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At least 163 records · Page 9

Thermogravimetric study of reduction of oxides present in oxidized nickel-base alloy powders

Carbon, hydrogen, and hydrogen plus carbon reduction of three oxidized nickel-base alloy powders (a solid solution strengthened alloy both with and without the gamma prime formers aluminum and titanium and the solid solution strengthened alloy NiCrAlY) were evaluated by thermogravimetry. Hydrogen and hydrogen plus carbon were completely effective in reducing an alloy containing chromium, columbium, tantalum, molybdenum, and tungsten. However, with aluminum and titanium present the reduction was limited to a weight loss of about 81 percent. Carbon alone was not effective in reducing any of the alloys, and none of the reducing conditions were effective for use with NiCrAlY.

Herbell, T. P.↗

Blanch Resistant and Thermal Barrier NiAl Coating Systems for Advanced Copper Alloys

A method of forming an environmental resistant thermal barrier coating on a copper alloy is disclosed. The steps include cleansing a surface of a copper alloy, depositing a bond coat on the cleansed surface of the copper alloy, depositing a NiAl top coat on the bond coat and consolidating the bond coat and the NiAl top coat to form the thermal barrier coating. The bond coat may be a nickel layer or a layer composed of at least one of copper and chromium-copper alloy and either the bond coat or the NiAl top coat or both may be deposited using a low pressure or vacuum plasma spray.

Sai V Raj↗

High gas velocity oxidation and hot corrosion testing of oxide dispersion-strengthened nickel-base alloys

Several oxide dispersion strengthened (ODS) nickel-base alloys were tested in high velocity gases for cyclic oxidation resistance at temperatures to 1200 C and times to 500 hours and for hot corrosion resistance at 900 C for 200 hours. Nickel-chromium-aluminum ODS alloys were found to have superior resistance to oxidation and hot corrosion when compared to bare and coated nickel-chromium ODS alloys. The best of the alloys tested had compositions of nickel - 15.5 to 16 weight percent chromium with aluminum weight percents between 4.5 and 5.0. All of the nickel-chromium-aluminum ODS materials experienced small weight losses (less than 16 mg/sq cm).

Deadmore, D. L.↗

A Directionally Solidified Iron-chromium-aluminum-tantalum Carbide Eutectic Alloy

A eutectic alloy, Fe-13.6CR-3.7Al+9TaC, was directionally solidified in a high gradient furnace, producing a microstructure of alined TaC fibers in an oxidation resistant alpha-iron matrix. Tensile and stress rupture properties, thermal cycling resistance, and microstructures were evaluated. The alloy displays at 1000 C an ultimate tensile strength of 58 MPa and a 100-hour rupture life at a stress of 21 MPa. Thermal cycling to 1100 C induces faceting in the TaC fibers.

Harf, F. H.↗

Materials review for improved automotive gas turbine engine

The potential role of superalloys, refractory alloys, and ceramics in the hottest sections of engines operating with turbine inlet temperatures as high as 1370 C is examined. The convential superalloys, directionally solidified eutectics, oxide dispersion strenghened alloys, and tungsten fiber reinforced superalloys are reviewed and compared on the basis of maximum turbine blade temperature capability. Improved high temperature protective coatings and special fabrication techniques for these advanced alloys are discussed. Chromium, columbium, molybdenum, tantalum, and tungsten alloys are also reviewed. Molbdenum alloys are found to be the most suitable for mass produced turbine wheels. Various forms and fabrication processes for silicon nitride, silicon carbide, and SIALON's are investigated for use in highstress and medium stress high temperature environments.

Belleau, C.↗

Progress on a PdCr wire strain gage

The principal activity under the HOST effort to improve the state of the art in high temperature static strain measurement has been a contract under which a palladium-chromium (PdCr) alloy was developed. The contract effort is continuing with the goal of developing a thin film high temperature static strain gage system. In addition to this effort, researchers contracted with Battelle-Columbus Laboratories to draw the PdCr allow into wire while researchers at Lewis worked to gain experience with this alloy as a wire strain gage.

Englund, David R.↗

A resistance strain gage with repeatable and cancellable apparent strain for use to 800 C

A temperature compensated static strain gage, which is fabricated from palladium-13w/o chromium (Pd13Cr) alloy and a platinum (Pt) compensator, is being developed and was tested over a temperature range to 800 C at NASA-Lewis. The PdCr compensated strain gage has significantly lower apparent strain to 800 C than other high temperature strain gages. The PdCr compensated gage is protected from oxidation by a flame-sprayed alumina-4w/o zirconia overcoating. Test results to 800 C indicate apparent strain variations of less than 300 micro-epsilon and reproducibility between thermal cycles within 50 micro-epsilon. Apparent strain of the coated PdCr compensated gage can be predicted and cancelled due to its reproducibility and low value.

Lei, Jih-Fen↗

PdCr based high temperature static strain gage

The program at NASA Lewis Research Center to develop a high temperature static strain gage system for the hypersonic vehicle and turbine engine research has emphasized a palladium-13 wt pct chromium (PdCr) alloy. Gages made from this alloy are being developed in both fine wire and thin film form. The wire gage system had platinum wire as a temperature compensator and was coated with a special alumina and zirconia mixture overcoat. This PdCr compensated wire gage responded linearly to the imposed strain to at least 1000 microstrain. The apparent strain varied within 300 microstrain from room temperature to 800 C with a reproducibility within 50 microstrain between thermal cycles to 800 C. The sputtered thin film PdCr strain gage, whose size was 8 x 8 mm and 10 microns thick, has demonstrated the possibility of extending the use of the PdCr strain gage to a temperature of approximately 1000 C.

Lei, Jih-Fen↗

Friction Stir Welding of GR-Cop 84 for Combustion Chamber Liners

GRCop-84 is a copper-chromium-niobium alloy developed by the Glenn Research Center for liquid rocket engine combustion chamber liners. GRCop-84 exhibits superior properties over conventional copper-base alloys in a liquid hydrogen-oxygen operating environment. The Next Generation Launch Technology program has funded a program to demonstrate scale-up production capabilities of GR-Cop 84 to levels suitable for main combustion chamber production for the prototype rocket engine. This paper describes a novel method of manufacturing the main combustion chamber liner. The process consists of several steps: extrude the GR-Cop 84 powder into billets, roll the billets into plates, bump form the plates into cylinder halves and friction stir weld the halves into a cylinder. The cylinder is then metal spun formed to near net liner dimensions followed by finish machining to the final configuration. This paper describes the friction stir weld process development including tooling and non-destructive inspection techniques, culminating in the successful production of a liner preform completed through spin forming.

Russell, Carolyn K.↗