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At least 163 records · Page 9

Method of making a distributed optical fiber sensor having enhanced Rayleigh scattering and enhanced temperature stability, and monitoring systems employing same

A method of making an optical fiber sensor device for distributed sensing includes generating a laser beam comprising a plurality of ultrafast pulses, and focusing the laser beam into a core of an optical fiber to form a nanograting structure within the core, wherein the nanograting structure includes a plurality of spaced nanograting elements each extending substantially parallel to a longitudinal axis of optical fiber. Also, an optical fiber sensor device for distributed sensing includes an optical fiber having a longitudinal axis, a core, and a nanograting structure within the core, wherein the nanograting structure includes a plurality of spaced nanograting elements each extending substantially parallel to the longitudinal axis of the optical fiber. Also, a distributed sensing method and system and an energy production system that employs such an optical fiber sensor device.

42 ENGINEERING↗

Method of making a distributed optical fiber sensor having enhanced Rayleigh scattering and enhanced temperature stability, and monitoring systems employing same

A method of making an optical fiber sensor device for distributed sensing includes generating a laser beam comprising a plurality of ultrafast pulses, and focusing the laser beam into a core of an optical fiber to form a nanograting structure within the core, wherein the nanograting structure includes a plurality of spaced nanograting elements each extending substantially parallel to a longitudinal axis of optical fiber. Also, an optical fiber sensor device for distributed sensing includes an optical fiber having a longitudinal axis, a core, and a nanograting structure within the core, wherein the nanograting structure includes a plurality of spaced nanograting elements each extending substantially parallel to the longitudinal axis of the optical fiber. Also, a distributed sensing method and system and an energy production system that employs such an optical fiber sensor device.

Chen, Peng Kevin↗

Dual wavelength negative imaging DLP-SLA system and method

The present disclosure relates to a method for forming a three dimensional (3D) component from a photopolymer resin. The method may involve generating a first optical beam at a first wavelength, with the first optical beam causing polymerization of a photopolymerizable resist. A second optical beam is generated at a second wavelength, different from the first wavelength, which inhibits polymerization of the photopolymerizable resist. A device is used to receive the first and second optical beams and to generate therefrom corresponding separate first and second light patterns, respectively, where the first light pattern forms a first image on the photopolymerizable resist to cause polymerization of a first portion of the photopolymerizable resist, while the second light pattern forms a second image on the photopolymerizable resist and inhibits polymerization of a second portion of the photopolymerizable resist.

Moran, Bryan D.↗

System and method for stimulated emission depletion projection stereolithography

The present disclosure relates to a system for forming a three dimensional (3D) part. The system may incorporate a beam delivery subsystem for generating optical signals, and a mask subsystem that receives the optical signals and generates optical images therefrom. A first one of the optical images activates a polymerization species of a photo-sensitive resin in accordance with illuminated areas thereof, to thus cause polymerization of select portions of the photo-sensitive resin to help form a layer of the 3D part. A second one of the optical images causes stimulated emission depletion of subportions of the polymerization species, simultaneously, over various areas of the layer, to enhance resolution of at least one subportion of the select portions of the photo-sensitive resin.

Hensleigh, Ryan↗

System and method for laser system having non-planar thin disc gain media

The present disclosure relates to a laser system. The laser system may have at least non-flat gain media disc. At least one pump source may be configured to generate a beam that pumps the non-flat gain media disc. A laser cavity may be formed by the pump source and the non-flat gain media disc. An output coupler may be included for receiving and directing the output beam toward an external component.

Dawson, Jay W.↗

New Septum Dump Quadrupole Magnet Design

The purpose of the septum dump quadrupole (SDQ) magnet is to expand the beam size on the septum dump of the DARHT Axis 2 downstream transport in the same manner as the S2 magnet expands the beam on the beam stop for mode 1 operations of DARHT Axis 2. This is necessary in order to minimize the heating of the carbon beam dump and suppress desorption of ions. Initially, ions are generated through stimulated desorption and ionization of the monolayers of water vapor stuck to the beam dump surface. These ions propagate upstream at high speeds and act as an electrostatic focusing lens by reducing the beam space charge. As the beam size on the dump decreases, the dump is sufficiently heated so that a surface plasma is formed and much greater quantities of ions are generated through space charge limited emission. The interaction of these ions with the beam causes significant disruption of the beam.

43 PARTICLE ACCELERATORS↗

Modeling and Analysis Support for Acceleratro-based Production of Mo-99

NorthStar Medical Radioisotopes, LLC, is in the process of commissioning a medical isotope production facility, which will use high-power electron accelerators to produce molybdenum-99 (Mo-99), the parent of technetium-99m (Tc-99m), through photonuclear reactions in molybdenum-100 (Mo-100). In this approach, a target comprising multiple thin disks of enriched molybdenum metal is bombarded with a 40-MeV electron beam. Electrons that impinge on the molybdenum target produce bremsstrahlung x-rays that cause the nuclear reaction. Because enriched Mo-100 is expensive, there is a desire to use as much beam power as possible to achieve maximum production yield and minimize the size of the target. This requirement leads to very high beam power density (heat deposition in the target), which creates challenging requirements for target cooling. In the latest concept developed by NorthStar, a stack of target (sintered molybdenum) disks is irradiated from two sides by a 40-MeV electron beam, with a total power of 250 kW (125 kW from each side). The target disks are cooled by pressurized helium gas flowing through channels between the disks. Inconel windows in the target housing form a pressure boundary between the helium within the housing and the evacuated beam tube.

07 ISOTOPE AND RADIATION SOURCES↗

Photonic ring resonator notch filters for astronomical OH line suppression

Photonic ring resonator arrays used as notch filters are a promising novel solution to improve the signal-to-noise ratio of ground-based astronomical observations by suppressing OH emission lines in the near-infrared (NIR) wavelength range (0.9-2.5 μm). We aim to fabricate a series of ring resonators connected by a waveguide, each with its resonance wavelength and full-width-half-maximum (FWHM) matched with one of the OH emission lines. The fundamental structure of ring resonator-based notch filters is a ring resonator evanescently coupled to a waveguide. Due to the optical loss of the ring resonator, the transmission of light through the waveguide will be suppressed at the resonance wavelength of the ring resonator. The degree of suppression can be controlled by varying the coupling strength between the waveguide and the ring resonator, while the resonance wavelength can be controlled by the geometry and size of the ring. However, since a single ring resonator has multiple modes each with a different wavelength separated by its free spectral range (FSR), the additional suppression at other wavelengths may undermine the signal. Therefore, the ideal FSR off the ring resonators needs to be larger than the measurement window. For this application, we aim the FSR to be 1 larger than 30 nm . Our initial measurement results revealed two major challenges for this application. First, the FSR of the ring resonators is limited by the bending loss of ring resonators. In a standard 220 nm silicon-on-insulator material platform, the FSR of ring resonators cannot exceed 30 nm; Second, due to the wafer thickness variation and fabrication inaccuracy, the achievable accuracy in the resonance wavelength of a fabricated single ring resonator is only ~1.5 nm. In this work, we report our novel solutions to the above two challenges. For the first one, we have developed a novel structure based on the Vernier effect to greatly raise the FSR of ring resonators. Serially coupled Vernier ring structures is a typical approach to increase the FSR without encountering bending loss, but it requires restrictive matching of the coupling and optical loss of the rings and any imperfect matching can result in even noisier signals. On the contrary, our structure, as shown in shown in Fig. 1, does not require the restrictive matching. The signals of two output ports in our structure marked in Fig. 1 will be added together to form the final output signal, and Fig. 2 shows the finite-difference time-domain (FDTD) simulation results of the final output signal. As can be seen, the FSR of the entire structure is well-beyond 60 nm with little noise at other wavelengths. For the second one, we have developed an easy-to-implement method to permanently tune the resonance wavelengths of ring resonators within 0.1 nm accuracy. The tuning mechanism is based on the property of hydrogen silsesquioxane (HSQ) resist. As a negative tone electron beam resist, HSQ upon exposure will cross-link and eventually form SiO2. The refractive 2 index of HSQ resist and formed SiO2 are slightly different , enabling the tuning. By having a thin layer of HSQ resist on top of ring resonator structures followed by SiO2 cladding, the resonance wavelengths of ring resonators can be post-tuned Advances in Optical Astronomical Instrumentation 2019, edited by Simon Ellis, Céline d'Orgeville, Downloaded From: https://www.spiedigitallibrary.org/conference-proceedings-of-spie on 23 Sep 2020 Terms of Use: https://www.spiedigitallibrary.org/terms-of-use through electron beam exposure. We have found that, within 5 nm tuning range, the resonance wavelength shift and dosage applied obeys a linear relationship. So a simple calibration beforehand can result in resonance wavelength tuning within 0.1 nm accuracy. The transmission spectra of a 3-ring device before and after tuning is shown in Fig. 3.

Astronomical optics↗

Excitation of surface waves in 3D ion beam neutralization

Neutralization of beams with 2D and 3D geometries by the electrons emitted from an external source is studied using particle-in-cell simulations. Our work reveals that the high-energy electrons excite Trivelpiece–Gould (TG) surface waves in the beams with 3D axisymmetric geometries. These high-energy electrons are generated because of a large amplitude electrostatic solitary wave (ESW) that forms near the electron source and has an electric potential amplitude more than three times the electron thermal energy. Here, we also find that surface wave excitation only happens when the beam radius is large enough at the ion source to attract enough electrons that could form the large amplitude ESW. A comparison of the 3D TG surface wave dispersion relation with an expression for 2D surface waves reveals that they become excited in 3D axisymmetric but not in 2D planar beam because of a higher phase speed requirement in the latter case.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Direct TPE measurement via $e^+p/e^-p$ scattering at low $\varepsilon$ in Hall A

The proton elastic form factor ratio can be measured either via Rosenbluth separation in an experiment with unpolarized beam and target, or via the use of polarization degrees of freedom. However, data produced by these two approaches show a discrepancy, increasing with $Q^2$. The proposed explanation of this discrepancy - two-photon exchange - has been tested recently by three experiments. The results support the existence of a small two-photon exchange effect but cannot establish that theoretical treatments at the measured momentum transfers are valid. At larger momentum transfers, theory remains untested, and without further data, it is impossible to resolve the discrepancy. Additionally, a positron beam at Jefferson Lab allows us to directly measure two-photon exchange over an extended $Q^2$ and $\epsilon$ range with high precision. With this, we can validate whether the effect reconciles the form factor ratio measurements, and test several theoretical approaches, valid in different parts of the tested $Q^2$ range. In this proposal, we describe a measurement program in Hall A that combines the Super BigBite, BigBite, and High Resolution Spectrometers to directly measure the two-photon effect. Though the limited beam current of the positron beam will restrict the kinematic reach, this measurement will have very small systematic uncertainties, making it a clean probe of two photon exchange.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

Tuning of the electronic and vibrational properties of epitaxial MoS 2 through He-ion beam modification

Abstract Atomically thin transition metal dichalcogenides (TMDs), like MoS 2 with high carrier mobilities and tunable electron dispersions, are unique active material candidates for next generation opto-electronic devices. Previous studies on ion irradiation show great potential applications when applied to two-dimensional (2D) materials, yet have been limited to micron size exfoliated flakes or smaller. To demonstrate the scalability of this method for industrial applications, we report the application of relatively low power (50 keV) 4 He + ion irradiation towards tuning the optoelectronic properties of an epitaxially grown continuous film of MoS 2 at the wafer scale, and demonstrate that precise manipulation of atomistic defects can be achieved in TMD films using ion implanters. The effect of 4 He + ion fluence on the PL and Raman signatures of the irradiated film provides new insights into the type and concentration of defects formed in the MoS 2 lattice, which are quantified through ion beam analysis. PL and Raman spectroscopy indicate that point defects are generated without causing disruption to the underlying lattice structure of the 2D films and hence, this technique can prove to be an effective way to achieve defect-mediated control over the opto-electronic properties of MoS 2 and other 2D materials.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

Overview of H- radio frequency ion sources for particle accelerators

Particle accelerators are among the most important scientific tools of the modern era. Large accelerator complexes have supported scientific user facilities which have had an enormous societal impact spanning many decades and enabling the work of thousands of scientific users worldwide contributing to many Nobel prizes in physics, biology and chemistry [1]. Many of the large hadron facilities employ accelerator complexes which include cyclotrons, synchrotrons, storage rings, linear or tandem accelerators and deliver ion beams of very high-intensity and/or very high-energy to their user facilities. These accelerator complexes require the injection of high-intensity beams of ions which are produced within an ion source and formed within a plasma or by bombardment of a surface [2]. Increasingly, RF systems are being utilized, to generate these ion-rich plasmas due to their high reliability and minimal use of consumable components. This report will first discuss the basic mechanisms of ion formation and plasma generation as well as some specifics of RF/microwave generators, matching circuits and plasma coupling structures typically employed. A detailed discussion will then be given of the RF-driven negative ion source systems employed by US Spallation Neutron Source as well as those used in similar facilities located around the globe. REFERENCES [1]Vladimir Shiltsev, “Particle beams behind physics discoveries”, Physics Today 73, Issue 4, 32 (2020) [2]Robert Welton et al, “Negative hydrogen ion sources for particle accelerators: Sustainability issues and recent improvements in long-term operations”, Journal of Physics Conf Series, 2244 012045

Welton, Robert F.↗

Additive Manufacturing of Pure Mo and Mo + TiC MMC Alloy by Electron Beam Powder Bed Fusion

A metal matrix composite powder of molybdenum (Mo) + TiC was produced by mechanical alloying (MA) and used in additive manufacturing by electron beam powder bed fusion along with pure Mo powder to form sandwich structures. The Mo + TiC solid layers formed mixed structures of Mo with discrete TiC particles, eutectic Mo + TiC, and Mo dendrites. Thermodynamic modeling showed that the system contained an invariant eutectic reaction in the composition range used and indicated that the system was highly sensitive to changes in composition and temperature.

36 MATERIALS SCIENCE↗

Assessment of Blocking Contacts in Suppressing Polarization Effects in CsPbBr 3 Perovskite Detectors

The CsPbBr 3 perovskite has garnered significant attention as a room-temperature semiconductor for hard radiation detection due to straightforward synthesis, scalable crystal growth, low cost, and excellent energy resolution. However, despite these advantages, at ambient temperature, CsPbBr 3 devices may experience performance deterioration and irreversible failure due to “polarization” induced by electromigration of ions to electrical connections on the device. In this study, we tested several contact materials and their optimization deposition techniques to assess the stability of high-performance CsPbBr 3 γ-ray detectors. Metals, with low work functions (Ti, In, Sn, Sb, Pb, Bi, Al, Au, and TiC) and high-work-function (Au or Pt) contacts, were used to form different Schottky junctions using vacuum thermal evaporation, electron-beam evaporation, and sputtering methods. These detectors were tested in intermittent and continuous modes to assess their stability. Among the tested detectors, the Bi/CLB/Pt electrode configuration demonstrated superior stability, operating effectively for 11 months under periodic testing and 16 days under continuous testing. In contrast, other configurations functioned only for a few months under intermittent conditions. Upon incorporating a ~40-nm-thick TiC passivation layer on the anode side (Bi/TiC/CLB/Pt), the CLB device operated continuously for 36 days without degradation. In many cases, the failure mode of the devices was due to the degradation of the anode. Here, the chemical changes in the fresh and deteriorated anodes were characterized using scanning electron microscopy and energydispersive X-ray spectroscopy

CsPbBr3 perovskite↗

Tailoring the Physicochemical Properties of Nb Thin Films via Surface Engineering Methods

The modification of surface oxide layers formed on niobium (Nb) thin films via chemical mechanical planarization (CMP) and accelerated neutral atom beam (ANAB) processing provides a promising route toward tailoring their emergent properties and performance when used as superconducting qubits. Here, in this study, we show that CMP- and ANAB-formed Nb oxides are significantly thinner and smoother than the native oxide, as revealed by transmission electron microscopy (TEM) and atomic force microscopy. Scanning TEM and energy-dispersive X-ray spectroscopy along with X-ray photoelectron spectroscopy identified an oxidation gradient within the native and surface-engineered oxides. The topside layer is dominated by Nb 5+ (Nb 2 O 5 ), with various Nb suboxides present closer to the oxide/metal interface. Time-of-flight secondary ion mass spectrometry (ToF-SIMS) depth profiling confirmed the presence of an oxygen content gradient and demonstrated the enhanced resistance of the CMP- and ANAB-formed oxides to oxygen surface exchange and subsequent diffusion via 18 O 2 isotopic labeling experiments. ToF-SIMS also identified an interfacial layer containing trapped hydrogen (H)-containing species at the Nb oxide/metal interface. In situ ToF-SIMS and TEM revealed migration of the H/OH interfacial layer coinciding with decomposition of the surface oxide. Furthermore, our density functional theory calculations indicated that both H from moisture present in ambient air and bulk H in Nb films tend to segregate at the interface. These findings underscore the importance of understanding surface oxidation mechanisms, hydrogen incorporation, and their impact on the designed functionalities of Nb-based devices.

36 MATERIALS SCIENCE↗

Explainable physics-based constraints on reinforcement learning for accelerator optimization

We present a reinforcement learning (RL) framework for optimizing particle accelerator experiments that builds explainable physics-based constraints on agent behavior. The goal is to increase transparency and trust by letting users verify that the agent’s decision-making process incorporates suitable physics. Our algorithm uses a learnable surrogate function for physical observables, such as energy, and uses them to fine-tune how actions are chosen. This surrogate can be represented by a neural network or by an interpretable sparse dictionary model. We test our algorithm on a range of particle accelerator optimization environments designed to emulate the Continuous Electron Beam Accelerator Facility at Jefferson Lab. By examining the mathematical form of the learned constraint function, we are able to confirm the agent has learned to use the established physics of each environment. In addition, we find that the introduction of a physics-based surrogate enables our RL algorithms to reliably converge for difficult high-dimensional accelerator optimization environments.

explainability↗

Synthesis and electronic properties of Nd n +1 NinO 3 n +1 Ruddlesden-Popper nickelate thin films

The rare-earth nickelates possess a diverse set of collective phenomena including metal-to-insulator transitions, magnetic phase transitions, and, upon chemical reduction, superconductivity. In this work, we demonstrate epitaxial stabilization of layered nickelates in the Ruddlesden-Popper form, Nd n +1 NinO 3 n +1 , using molecular beam epitaxy. By optimizing the stoichiometry of the parent perovskite NdNiO 3 , we can reproducibly synthesize the n = 1–5 member compounds. X-ray absorption spectroscopy at the O K and Ni L edges indicate systematic changes in both the nickel-oxygen hybridization level and nominal nickel filling from 3$d^8$ to 3$d^7$ as we move across the series from n = 1 to n = ∞. The n = 3 – 5 compounds exhibit weakly hysteretic metal-to-insulator transitions with transition temperatures that depress with increasing order toward NdNiO 3 ( n = ∞).

36 MATERIALS SCIENCE↗

Scoping study of detecting high harmonic fast waves in NSTX-U hot core plasma directly using beam emission spectroscopy

In this paper, we used radio frequency (RF) full wave simulation to explore the feasibility of generating a density beat oscillation formed by high harmonic fast waves (HHFWs) in the National Spherical Tokamak Experiment-Upgrade (NSTX-U) and of measuring it numerically with 2D beam emission spectroscopy (BES). This oscillation is of interest as it can be used to determine the injected RF fields. We began by computing HHFW fields in NSTX-U under a variety of experimental conditions and antenna configurations with Petra-M, a 3D RF wavefield solver. These fields were then used to evaluate the amplitude of δne,beat/ne0 in the volume of measurement, which we predict to be between 5 × 10−10 and 10−9, although it is highly dependent on plasma parameters. Trends in magnetic field, core temperature, core density, and antenna phasing are presented, and the parameters most suitable to this measurement are identified. Finally, we developed a synthetic BES diagnostic to compare the experimental BES signal against.

Rutherford, Grant (ORCID:0000000163620037)↗