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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 163 records · Page 9

Failure of morphology of (0 deg)8 graphite/epoxy as influenced by environments and processing

Optical and scanning electron microscopy were used to investigate the failure morphology of graphite/epoxy specimens which had been tested until tensile failure. Failure morphology was studied as a function of the quality control variables of specimen preparation technique, prepreg batch, and cure condition, and also as a function of the environmental parameters of temperature and moisture content. Defective specimens were found to exhibit a low energy failure morphology. Poor specimen edge preparation and one batch of prepreg when tested at elevated temperature or moisture content also exhibited energy failure morphology. Postcuring had no effect on strength but did slightly alter failure morphology. Temperature or moisture appeared to decrease flaw sensitivity and thus increase strength; however, moisture also appeared to increase interfacial debonding between filament and matrix. When combined moisture and temperature increased interfacial debonding and made the epoxy matrix more prone to fracture.

Clements, L. L.↗

Outline of a fast hardware implementation of Winograd's DFT algorithm

The main characteristics of the discrete Fourier transform (DFT) algorithm considered by Winograd (1976) is a significant reduction in the number of multiplications. Its primary disadvantage is a higher structural complexity. It is, therefore, difficult to translate the reduced number of multiplications into faster execution of the DFT by means of a software implementation of the algorithm. For this reason, a hardware implementation is considered in the current study, taking into account a design based on the algorithm prescription discussed by Zohar (1979). The hardware implementation of a FORTRAN subroutine is proposed, giving attention to a pipelining scheme in which 5 consecutive data batches are being operated on simultaneously, each batch undergoing one of 5 processing phases.

Zohar, S.↗

Project Planning and Reporting

Project Planning Analysis and Reporting System (PPARS) is automated aid in monitoring and scheduling of activities within project. PPARS system consists of PPARS Batch Program, five preprocessor programs, and two post-processor programs. PPARS Batch program is full CPM (Critical Path Method) scheduling program with resource capabilities. Can process networks with up to 10,000 activities.

Source record↗

Coal desulfurization by low temperature chlorinolysis, phase 3

Laboratory scale, bench scale batch reactor, and minipilot plant tests were conducted on 22 bituminous, subbituminous, and lignite coals. Chemical pretreatment and post treatment of coals relative to the chlorination were tried as a means of enhancing desulfurization by the chlorinolysis process. Elevated temperature (500-700 C) hydrogen treatment of chlorinolysis-processed coal at atmospheric pressure was found to substantially increase coal desulfurization up to 90 percent. Sulfur forms, proximate and ultimate analyses of the processed coal are included. Minipilot plant operation indicates that the continuous flow reactor provides coal desulfurization results comparable to those obtained in the batch reactor. Seven runs were conducted at coal feed rates of 1.5 to 8.8 kg per hour using water and methylchloroform solvents, gaseous chlorine feed of 3 to 31.4 SCFH at 21 to 70 C, and atmospheric pressure for retention times of 20 to 120 minutes.

Kalvinskas, J. J.↗

Development and demonstration of manufacturing processes for fabricating graphite/Larc-160 polyimide structural elements, part 4, paragraph C

Progress in the development of processes for production of Celion/LARC-160 graphite-polyimide materials, quality control methods, and the fabrication of Space Shuttle composite structure components is reported. The formulation and processing limits for three batches of resin are presented. Process improvements for simplification of the imidizing and autoclave cure cycles are described. Imidized and autoclave cured test panels were prepared. Celion/LARC-160 cure process verification and the fabrication of honeycomb sandwich panel elements and skin/stringer panels are described. C-scans of laminates imidized at 163 C to 218 C for periods from 30 to 180 minutes, and of process verification laminates made from different batches of prepreg are presented. Failure modes and load/strain characteristics of sandwich elements and C-scans of stringer to skin bond joints are also given.

Source record↗

Synthesis of perfluoroalkylene dianilines

The objective of this contrast was to optimize and scale-up the synthesis of 2,2-bis(4-aminophenyl)-hexafluoropropane and 1,3-bis(4-aminophenyl)hexafluoropropane, as well as to explore avenues to other perfluoroalkyl-bridged dianilines. Routes other than Friedel-Crafts reaction leading to 2,2-bis(4-aminophenyl)hexafluoropropane were investigated. The processes utilizing bisphenol-AF were all unsuccessful; reactions aimed at the production of 4-(hexafluoro-2-halo-isopropyl)aniline from the hydroxyl intermediate failed to yield the desired products. Tailoring the conditions of the Friedel-Crafts reaction of 4-(hexafluoro-2-hydroxyisopropyl)aniline, aniline, and aluminum chloride by using hydrochloride salts and selecting optimum reagent ratios, reaction times, and temperature resulted in approx. 20% yield of pure crystallized 2,2-bis(4-aminophenyl)hexafluoropropane in 0.2 mole reaction batches. Yields up to approx. 40% were realized in small, approx. 0.01 mole, batches. The synthesis of 1,3-bis(4-aminophenyl)hexafluoropropane starting with perfluoroglutarimidine was reinvestigated. The yield of the 4-step reaction sequence giving 1,3-bis(4-acetamidophenyl)hexafluoropropane was raised to 44%. The yield of the subsequent hydrolysis process was improved by a factor of approx. 2. Approaches to prepare other perfluoroalkyl-bridged dianilines were unsuccessful. Reactions reported to proceed readily with trifluoromethyl substituents failed when longer chain perfluoroalkyl groups were employed.

Paciorek, K. L.↗

Interactive computer modeling of combustion chemistry and coalescence-dispersion modeling of turbulent combustion

An interactive computer code for simulation of a high-intensity turbulent combustor as a single point inhomogeneous stirred reactor was developed from an existing batch processing computer code CDPSR. The interactive CDPSR code was used as a guide for interpretation and direction of DOE-sponsored companion experiments utilizing Xenon tracer with optical laser diagnostic techniques to experimentally determine the appropriate mixing frequency, and for validation of CDPSR as a mixing-chemistry model for a laboratory jet-stirred reactor. The coalescence-dispersion model for finite rate mixing was incorporated into an existing interactive code AVCO-MARK I, to enable simulation of a combustor as a modular array of stirred flow and plug flow elements, each having a prescribed finite mixing frequency, or axial distribution of mixing frequency, as appropriate. Further increase the speed and reliability of the batch kinetics integrator code CREKID was increased by rewriting in vectorized form for execution on a vector or parallel processor, and by incorporating numerical techniques which enhance execution speed by permitting specification of a very low accuracy tolerance.

Pratt, D. T.↗

Data distribution in the NBS Automated Manufacturing Research Facility

The Automated Manufacturing Research Facility (AMRF) at the National Bureau of Standards was constructed as a testbed for research in the automation of small batch maufacturing, in particular for systems producing machined parts in lots of 1000 or less. Potential standard interfaces between existing and future components of small batch of factory floor metrology in an automated environment, delivering proven measurement techniques and standard reference materails industry to are identified. Commercially available product are used to construct the facility to expedite transfer of research results into the private sector.

Mitchell, M. J.↗

Interactive digital signal processor

The Interactive Digital Signal Processor (IDSP) is examined. It consists of a set of time series analysis Operators each of which operates on an input file to produce an output file. The operators can be executed in any order that makes sense and recursively, if desired. The operators are the various algorithms used in digital time series analysis work. User written operators can be easily interfaced to the sysatem. The system can be operated both interactively and in batch mode. In IDSP a file can consist of up to n (currently n=8) simultaneous time series. IDSP currently includes over thirty standard operators that range from Fourier transform operations, design and application of digital filters, eigenvalue analysis, to operators that provide graphical output, allow batch operation, editing and display information.

Mish, W. H.↗

Aging properties of Kodak type 101 emulsions

Aging tests for several batches of Kodak type 101 emulsion show that storage conditions significantly influence how well the film will maintain its sensitometric properties, with sensitivity and density increasing to a maximum during this period. Any further aging may result in higher fog levels and sensitivity loss. It is noted that storage in an environment free of photographically active compounds allows film property optimization, and that film batches with different sensitivities age differently. Emulsions with maximum 1700-A sensitivity are 2.5 times faster than those at the low end of the sensitivity scale. These sensitive emulsions exhibit significantly accelerated changes in aging properties. Their use in space applications requires careful consideration of time and temperature profiles, encouraging the use of less sensitive emulsions when the controllability of these factors is limited.

Dohne, B.↗

Microbial colonization and growth on metal sulfides and other mineral surfaces

To determine whether a bacterial film forms on sulfur minerals in situ, various sulfur containing and other minerals were incubated in Penitencia Creek. The rate of cell growth and attachment within the surface microenvironment of mineral surfaces was also determined. To determine whether surfaces enriched with soluble sulfur substrates (cysteine, glutathione, thioglycolate, sulfite, and thiosulfate) increased the rate of growth or attachment of natural communities, membrane enrichments were incubated. These rates were determined as described by Caldwell et al. (1981, 1983). The growth of Pseudomonas fluorescens, a heterotrophic sulfur oxidizer, was studied in batch cell suspensions and in continuous culture. In batch culture the cells were oxygen limited (growth rate 0.33 per hour under oxygen limitations and 0.52 per hour when vigorously aerated). Growth within the film was glucose limited. Several behavioral phenomena were observed for cells growing within the hydrodynamic boundary layer. Despite a flow of 10 cm per second in the environment, the bacteria were able to move freely in both directions within the hydrodynamic boundary layer.

Caldwell, D.↗

Investigation of porous polymer gas chromatographic packings for atmospheric analysis of extraterrestrial bodies

Measurement of the permanent gases in the atmospheres of mission targets is a major objective. A 16 meter long Porapak N column was used on the Venus probe and required a rather high carrier gas flow rate. The researchers have, therefore, surveyed commercial porous polymer types which had some ability to resolve nitrogen, oxygen, argon and carbon monoxide gases. Porapaks N and Q appeared superior to most. Batch to batch variation, however, was quite wide, so the researchers learned how to synthesize porous polymer and investigated some of the factors affecting the separations. A polymer was synthesized which was superior to all commercial products and allowed at least a 50% reduction in length and flow rate of carrier gas. Similar studies were made concerning the separation of hydrocarbons and new porous polymers have been synthesized which represent significant improvements in time of analysis, column, and carrier gas flow rate.

Pollock, G. E.↗

The network queueing system

Described is the implementation of a networked, UNIX based queueing system developed on contract for NASA. The system discussed supports both batch and device requests, and provides the facilities of remote queueing, request routing, remote status, queue access controls, batch request resource quota limits, and remote output return.

Kingsbury, Brent K.↗

Inflight estimation of gyro noise

A method is described and demonstrated for estimating single-axis gyro noise levels in terms of the Farrenkopf model parameters. This is accomplished for the Cosmic Background Explorer (COBE) by comparing gyro-propagated attitudes with less accurate single-frame solutions and fitting the squared differences to a third-order polynomial in time. Initial results are consistent with the gyro specifications, and these results are used to determine limits on the duration of batches used to determine attitude. Sources of error are discussed, and guidelines for a more elegant implementation, as part of a batch estimator or filter, are included for future work.

Filla, O. H.↗

Hot-bench simulation of the active flexible wing wind-tunnel model

Two simulations, one batch and one real-time, of an aeroelastically-scaled wind-tunnel model were developed. The wind-tunnel model was a full-span, free-to-roll model of an advanced fighter concept. The batch simulation was used to generate and verify the real-time simulation and to test candidate control laws prior to implementation. The real-time simulation supported hot-bench testing of a digital controller, which was developed to actively control the elastic deformation of the wind-tunnel model. Time scaling was required for hot-bench testing. The wind-tunnel model, the mathematical models for the simulations, the techniques employed to reduce the hot-bench time-scale factors, and the verification procedures are described.

Buttrill, Carey S.↗

Geomagnetic model investigations for 1980 - 1989: A model for strategic defense initiative particle beam experiments and a study in the effects of data types and observatory bias solutions

Two suites of geomagnetic field models were generated at the request of Los Alamos National Lab. concerning Strategic Defense Initiative (SDI) research. The first is a progression of five models incorporating MAGSAT data and data from a sequence of batches as a priori information. The batch sequence is: post 1979.5 observatory data, post 1980 land survey and selected aeromagnetic and marine survey data, a special White Sands (NM) area survey by Project Magnet with some additional post 1980 marine survey data, and finally DE-2 satellite data. These models are of 13th deg and order in their main field terms, and deg and order 10 in their first derivative temporal terms. The second suite consists of four models based solely upon post 1983.5 observatory and survey data. They are of deg and order 10 in main field and 8 in a first deg Taylor series. A comprehensive error analysis was applied to both series, which accounted for error sources such as the truncated core and crustal fields, and the neglected Sq and low deg crustal fields. Comparison of the power spectrum of the MGST (10/81) model with those of this series show good agreement.

Langel, Robert A.↗

Hot-bench simulation of the active flexible wing wind-tunnel model

Two simulations, one batch and one real-time, of an aeroelastically-scaled wind-tunnel model were developed. The wind-tunnel model was a full-span, free-to-roll model of an advanced fighter concept. The batch simulation was used to generate and verify the real-time simulation and to test candidate control laws prior to implementation. The real-time simulation supported hot-bench testing of a digital controller, which was developed to actively control the elastic deformation of the wind tunnel model. Time scaling was required for hot-bench testing. The wind-tunnel model, the math models for the simulations, the techniques employed to reduce the hot-bench time-scale factor, and the verification procedures are described.

Buttrill, Carey S.↗

Fault detection and isolation for multisensor navigation systems

Increasing attention is being given to the problem of erroneous measurement data for multisensor navigation systems. A recursive estimator can be used in conjunction with a 'snapshot' batch estimator to provide fault detection and isolation (FDI) for these systems. A recursive estimator uses past system states to form a new state estimate and compares it to the calculated state based on a new set of measurements. A 'snapshot' batch estimator uses a set of measurements collected simultaneously and compares solutions based on subsets of measurements. The 'snapshot' approach requires redundant measurements in order to detect and isolate faults. FDI is also referred to as Receiver Autonomous Integrity Monitoring (RAIM).

Kline, Paul A.↗