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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,585 records · Page 88
All sourcesNASA NTRSDOE OSTI
NASA NTRS1971

Development of conformal coating materials

New polymeric compositions appear useful as coatings on electronic circuitry operating in rigorous environments. Formulation of their compositions is based on nitrosofluorocarbon polymers having active cure sites.

Glickman, S. A.↗
NASA NTRS1974

Development of high temperature materials for solid propellant rocket nozzle applications

Evaluation of tantalum carbide-tungsten fiber composites has been completed as far as weight percent carbon additions and weight percent additions of tungsten fiber. Extensive studies were undertaken concerning Young's Modulus and fracture strength of this material. Also, in-depth analysis of the embrittling effects of the extra carbon additions on the tungsten fibers has been completed. The complete fabrication procedure for the tantalum carbide-tungsten fiber composites with extra carbon additions is given. Microprobe and metallographic studies showed the effect of extra carbon on the tungsten fibers, and evaluation of the thermal shock parameter fracture strength/Young's Modulus is included.

Manning, C. R., Jr.↗
NASA NTRS1974

High purity silica reflective heat shield development

Progress is reported on the development of a high purity reflective heat shield material. Silicon dioxide was selected as the material because it is highly reflective in the correct wavelength band, has good ablation characteristics, is thermal shock resistant, and is readily fabricated to full size at reasonable cost. Conclusions indicate that: reflectance is affected by purity and morphology; the pure material is readily available; required purity and morphology can be maintained with reasonable care; high reflectances are determined (0.99 from 0.4 to 1.2 microns); major processing steps are defined; and the material appears to be cost effective. It is indicated that the materials are developed to the point of readiness for full scale fabrication and characterization.

Blome, J.↗
NASA NTRS1974

Development of improved amorphous materials for laser systems

Crystallization calculations were performed in order to determine the possibility of forming a particular type of laser glass with the avoidance of devitrification in an outer space laboratory. It was demonstrated that under the homogenuous nucleating conditions obtainable in a zero gravity laboratory this laser glass may be easily quenched to a virtually crystal-free product. Experimental evidence is provided that use of this material as a host in a neodymium glass laser would result in more than a 10 percent increase in efficiency when compared to laser glass rods of a similar composition currently commercially available. Differential thermal analysis, thermal gradient oven, X-ray diffraction, and liquidus determination experiments were carried out to determine the basics of the crystallization behavior of the glass, and small-angle X-ray scattering and splat-cooling experiments were performed in order to provide additional evidence for the feasibility of producing this laser glass material, crystal free, in an outer space environment.

Neilson, G. F.↗
NASA NTRS1976

Slicing of silicon into sheet material: Silicon sheet growth development for the large area silicon sheet task of the low cost silicon solar array project

Multiblade slurry sawing is used to slice 10 cm diameter silicon ingots into wafers 0.024 cm thick using 0.050 cm of silicon per slice (0.026 cm kerf loss). Total slicing time is less than twenty hours, and 143 slices are produced simultaneously. Productivity (slice area per hour per blade) is shown as a function or blade load and thickness, and abrasive size. Finer abrasive slurries cause a reduction in slice productivity, and thin blades cause a reduction of wafer accuracy. Sawing induced surface damage is found to extend 18 microns into the wafer.

Holden, S. C.↗
NASA NTRS1978

Slicing of silicon into sheet material. Silicon sheet growth development for the large area silicon sheet task of the low cost silicon solar array project

Fabrication of a prototype large capacity multiple blade slurry saw is considered. Design of the bladehead which will tension up to 1000 blades, and cut a 45 cm long silicon ingot as large as 12 cm in diameter is given. The large blade tensioning force of 270,000 kg is applied through two bolts acting on a pair of scissor toggles, significantly reducing operator set-up time. Tests with an upside-down cutting technique resulted in 100% wafering yields and the highest wafer accuracy yet experienced with MS slicing. Variations in oil and abrasives resulted only in degraded slicing results. A technique of continuous abrasive slurry separation to remove silicon debris is described.

Holden, S. C.↗
NASA NTRS1979

Slicing of Silicon into Sheet Material. Silicon Sheet Growth Development for the Large Area Silicon Sheet Task of the Low Cost Silicon Solar Array Project

Tests on mineral oil slurries show that the potential for workability and low cost is present. However, slurries tested to date which had sufficient lubricity exhibited wafer breakage problems near the end of the run for as-yet unknown reasons. The first test of the large prototype saw under cutting force control was largely successful in that the controller worked perfectly. Unfortunately a technique error (excessive stroke shortening) caused blade breakage and low yield. The latest run of the large saw pointed up the fact that an indication of end-of-stoke vertical motion, or bounce, is necessary. A circuit to provide such indication was fabricated and installed. Preliminary tests show it to be excessively noise sensitive; therefore, work on grounding and shielding to reduce this sensitivity is in progress.

Fleming, J. R.↗
NASA NTRS1979

Slicing of Silicon into Sheet Material: Silicon Sheet Growth Development for the Large Area Silicon Sheet Task of the Low Cost Silicon Solar Array Project

Testing of low cost low suspension power slurry vehicles is presented. Cutting oils are unlikely to work, but a mineral oil with additives should be workable. Two different abrasives were tested. A cheaper silicon carbide from Norton gave excellent results except for excessive kerf loss: the particles were too big. An abrasive treated for lubricity showed no lubricity improvement in mineral oil vehicle. The bounce fixture was tested for the first time under constant cut rate conditions (rather than constant force). Although the cut was not completed before the blades broke, the blade lifetime of thin (100 micrometer) blades was 120 times the lifetime without the fixture. The large prototype saw completed a successful run, producing 90% cutting yield (849 wafers) at 20 wafers/cm. Although inexperience with large numbers of wafers caused cleaning breakage to reduce this yield to 74%, the yield was high enough that the concept of the large saw is proven workable.

Fleming, J. R.↗
NASA NTRS1980

Development of advanced thermoelectric materials, phase A

Work performed on the chemical system characterized by chrome sulfide, chrome selenide, lanthanum selenide, and lanthanum sulfide is described. Most materials within the chemical systems possess the requisites for attractive thermoelectric materials. The preparation of the alloys is discussed. Graphs show the Seebeck coefficient, electrical resistivity, and thermal conductivity of various materials within the chemical systems. The results of selected doping are included.

Source record↗
NASA NTRS1981

Development of low modulus material for use in ceramic gas path seal applications

Three candidate materials were examined: Brunsbond (R) Pad; plasma sprayed porous NiCrAlY; and plasma sprayed low modulus microcracked zirconia. Evaluation consisted of mechanical, thermophysical, and oxidation resistance testing along with optical microscopy and a feasibility demonstration of attaching the material to a suitable substrate. The goals of the program were the following: feasibility of fastening or depositing the low modulus system onto a broad range of substrate alloys; feasibility of depositing or forming the low modulus system to a thickness of 0.19 cm to 0.38 cm; potential to attain a modulus of elasticity in the range of 3.4 to 6.9 GPa (0.5 to 1.0 MSI), and an ultimate strength of 17.2 MPa (2.5 ksi); suitable thermal conductivity; and static oxidation life of at least 1000 hours at 1311 K. The results of the program indicate that all three systems offer attractive properties as a strain isolator material.

Eaton, H. E.↗
NASA NTRS1987

Performance analysis of advanced spacecraft TPS

For the Space Shuttle several types of ceramic heat shield materials were developed, both flexible and rigid. Improvements on the materials are continuously evolving. Material properties that have been studied and improved are high temperature limits, material strength, surface ruggedness, and surface catalycity. The results are presented of preliminary analyses concerning the thermal protection systems of future spacecraft and their sensitivity to the above material properties.

Pitts, William C.↗
NASA NTRS1991

Development of improved ablative materials for ASRM

A program to improve ablative materials for the Advanced Solid Rocket Motor (ASRM) is briefly discussed. The main concerns with the baseline material are summarized along with the measures being undertaken to obtain improvements. The materials involved in the program, all of which have been manufactured and are now being evaluated, are mentioned.

Canfield, A.↗