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DOE OSTI2014

Final Scientific and Technical Report - Practical Fiber Delivered Laser Ignition Systems for Vehicles

Research has characterized advanced kagome fiber optics for their use in laser ignition systems. In comparison to past fibers used in laser ignition, these fibers have the important advantage of being relatively bend-insensitivity, so that they can be bent and coiled without degradation of output energy or beam quality. The results are very promising for practical systems. For pulse durations of ~12 ns, the fibers could deliver >~10 mJ pulses before damage onset. A study of pulse duration showed that by using longer pulse duration (~20 – 30 ns), it is possible to carry even higher pulse energy (by factor of ~2-3) which also provides future opportunities to implement longer duration sources. Beam quality measurements showed nearly single-mode output from the kagome fibers (i.e. M2 close to 1) which is the optimum possible value and, combined with their high pulse energy, shows the suitability of the fibers for laser ignition. Research has also demonstrated laser ignition of an engine including reliable (100%) ignition of a single-cylinder gasoline engine using the laser ignition system with bent and coiled kagome fiber. The COV of IMEP was <2% which is favorable for stable engine operation. These research results, along with the continued reduction in cost of laser sources, support our commercial development of practical laser ignition systems.

ignition, laser ignition, vehicles, fiber optics↗

DOE OSTI2021

Dense Pair and Gamma-Ray Creation Using Ultra-Intense Lasers (Final Technical Report)

Lasers with intensity >1.4x10 18 W.cm -2 irradiating solid targets couple 10-50% of its energy to “hot electrons” near the critical surface, with temperature kT > mc 2 . When these hot electrons impact high-Z target ions (e.g. Au, Pt), they emit copious bremsstrahlung gamma-rays and create e + e - pairs via the Trident process. For targets thicker than ~0.1mm, the gamma-rays create secondary pairs via the Bethe-Heitler processes. The concept of using lasers to create pairs was first studied by Shearer et al (1973). Motivated by the rapid advance of short-pulse ultra-intense lasers based on chirped-pulse amplification, Liang (1994) first proposed irradiating solid Au targets with laser intensity ≥10 20 W.cm -2 to create dense e + e - pairs. Using particle-in-cell (PIC, Birdsall and Langdon, 1991) simulations, Liang et al (1998, 2002) estimated that high-energy PW lasers can in principle achieve ultra-high in-situ pair densities. Subsequent studies supported this idea and found that for gold foils thicker than ~50 μm, the pair yield is dominated by the Bethe-Heitler (BH, Heitler 1954) process. Cowan et al (1999, 2000) using the LLNL Nova PW-laser to irradiate 125μm gold foils first observed pair creation, followed by Chen et al (2009) who demonstrated copious BH pair creation using the Titan, Omega-EP and Orion lasers. However, the emerging e + /e - ratio of these experiments was ≤ few %, and the pair density was only 10 13 /cc so that the pair jet transverse size R(~mm) was < pair skin depth c/ω + (=8πn+e 2 /m) 1/2 ). This was insufficient to qualify as a bona fide ”pair plasma”.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2022

Non-Intrusive Measurements Using Femtosecond Laser in Atmospheric Pressure Plasma Jet

Femto-second (fs) lasers offer state-of-the art non-intrusive diagnostic capabilities in plasma flow environments. The diagnostics in plasma flows using a fs-laser that are relevant to this proposal include Two-photon Absorption Laser Induced Fluorescence (TALIF) for measuring the number density of an atomic species, and Femto-second Laser Electronic Excitation Tagging (FLEET) for performing velocity measurements in plasma flows. Various aspects of these diagnostics using fs-lasers are still an active domain of research. The TALIF technique has been used to measure the number density of atomic species in various plasma flow environments like atmospheric pressure plasma jet (APPJ) and arc-jet flows. This technique utilizes a fs-laser to excite an atomic species and the subsequent relaxation process through fluorescence is recorded to make measurements. A narrow band-pass filter is used to isolate the fluorescence signal that is in the infra-red regime. However, broad-band background emissions can potentially pass through the filter and induce noise in the TALIF signal. Particularly, arc-jet plasma flows inherently contain background emissions. In such plasma flow environments, in addition to the filter, the background-subtraction technique will play an important role in reducing the noise that is induced in the number density measurements using TALIF. The proposed research focuses on evaluating the effectiveness of a background-subtraction technique by measuring atomic oxygen using a femtosecond (fs) TALIF in APPJ with induced background emissions and comparing measurements obtained without inducing the emissions. Therefore, by quantifying the changes in the signal-to-noise ratio caused by a background-subtraction technique applied for APPJ, it will enable a better understanding of the uncertainties in the background subtracted fs-TALIF measurements for arc-jet plasma flows. In addition to this, FLEET will be used to obtain velocity in the APPJ, and the impact of background emissions will be analyzed. Under this effort, the experimenters and research personnel will gain the technical know-how in the operational and theoretical aspects of the advanced fs-laser-based diagnostic techniques. The knowledge gained in this process will then also directly be applied to a separate ONR funded project at the Aerodynamics Research Center (ARC), UT Arlington, related to arc-jet flow characterization.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2022

Plasma Mirrors For High Power Lasers: A new approach for high repetition rates combined with realistic PIC simulations

We describe a research program to develop high quality plasma mirrors for use with high repetition rate, high power laser facilities to greatly facilitate experiments in high energy density physics, particularly when using solid density targets. A system delivering ultrathin, free standing liquid crystal films that could handle PW class laser pulses was developed that preserved the laser beam image quality and improved pulse contrast by over two orders of magnitude. The pulse contrast improvement was measured using a high dynamic range cross-correlation. The system operated at a repetition rate of several PMs formed in situ per minute. Extension to 1 Hz repetition rates should be possible. As a practical application, a PM system was used to separate laser accelerated electrons from the ultrashort pulse drive laser so that the electron beam emittance could be directly measured. The 20 nm thick PMs did not contribute significantly to emittance degradation. It was also demonstrated that the films could operate in the difficult plasma and laser environment present for GeV laser based electron acceleration. PM operation is still not well understood and much work with PMs is done empirically. Accordingly, we also demonstrated a particle-in-cell based simulation technique that would model PM operation, tracking the PM operation from cold, neutral atoms to a hot dense plasma by accounting for multiphoton ionization, plasma collisionality, and the dynamically changing index of refraction. Simulations in 3D were compared to a 2D based approach that was comparable. Finally, we developed a simpler model that can predict the intensity at which a plasma mirror will have its peak reflectivity.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2023

Laser Driven Hydrothermal Processing (LDHP) for Rapid Dissolution of Glassy Nuclear Debris

Discovered in 2009 on the SLAB laser system at LLNL, Laser-Driven Hydrothermal Processing (LDHP) both spalls and transiently dissolves a wetted surface (e.g., rock, concrete, paint) when that surface is struck by a laser beam pulse under specific conditions. Previous projects have explored the application of LDHP to expediting sample dissolution for post-detonation nuclear forensics. Early results were very promising, indicating that this method could decrease material dissolution time by a factor of 10 or more. However, the large and complicated lasers previously used are impractical for this application. Under the R^3 venture we aimed to benchmark the LDHP capabilities of turn-key commercial off-the-shelf (COTS) lasers, and to establish how this process could be integrated into an analytical workflow for nuclear forensic analysis. We demonstrated that geological rock standards could be quickly processed into fine powder by LDHP followed by complete acid digestion in 15 minutes, without elemental fractionation that would skew analytical results. We determined that the COTS laser can be used for LDHP that could potentially reduce dissolution time for solid nuclear debris samples in post detonation nuclear forensics. One downside to this approach, however, is that the laser interactions are different with every material, so extensive method validation would be required for all likely material compositions. The LDHP processing rates of several materials were tested and determined to be favorable in the beginning with significant slowdown due to particulate scattering. This could be mitigated either by stopping and centrifuging the sample at specific intervals, or through design of a continuous solvent flow through mechanism.

36 MATERIALS SCIENCE↗

DOE OSTI2024

Atmosphere Effects in Laser Powder Bed Fusion: A Review

The use of components fabricated by laser powder bed fusion (LPBF) requires the development of processing parameters that can produce high-quality material. Manipulating the most commonly identified critical build parameters (e.g., laser power, laser scan speed, and layer thickness) on LPBF equipment can generate acceptable parts for established materials and moderately intricate part geometries. The need to fabricate increasingly complex parts from unique materials drives the limited research into LPBF process control using underutilized parameters, such as atmosphere composition and pressure. As presented in this review, manipulating atmosphere composition and pressure in laser beam welding has been shown to expand processing windows and produce higher-quality welds. The similarities between laser beam welding and laser-based AM processes suggest that this atmosphere control research could be effectively adapted for LPBF, an area that has not been widely explored. Tailoring this research for LPBF has significant potential to reveal novel processing regimes. This review presents the current state of the art in atmosphere research for laser beam welding and LPBF, with a focus on studies exploring cover gas composition and pressure, and concludes with an outlook on future LPBF atmosphere control systems.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

NASA NTRS1996

The effect of nonablative laser energy on joint capsular properties. An in vitro histologic and biochemical study using a rabbit model

The purpose of this study was to evaluate the effect of laser energy at nonablative levels on joint capsular histologic and biochemical properties in an in vitro rabbit model. The medial and lateral portions of the femoropatellar joint capsule from both stifles of 12 mature New Zealand White rabbits were used. Specimens were divided into three treatment groups (5 watts, 10 watts, and 15 watt) and one control group using a randomized block design. Specimens were placed in a 37 degrees bath of lactated Ringer's solution and laser energy was applied using a holmium:yttrium-aluminum-garnet laser in four transverse passes across the tissue at a velocity of 2 mm/sec with the handpiece set 1.5 mm from the synovial surface. Histologic analysis revealed thermal alteration of collagen (fusion) and fibroblasts (pyknosis) at all energy densities, with higher laser energy causing significantly greater morphologic changes over a larger area (P < 0.05). Application of laser energy did not significantly alter the biochemical parameters evaluated, including type I collagen content and nonreducible crosslinks (P > 0.05). This study demonstrated that nonablative laser energy caused significant thermal damage to the joint capsular tissue in an energy-dependent fashion, but type I collagen content and nonreducible crosslinks (P > 0.05). This study demonstrated that nonablative laser energy caused significant thermal damage to the joint capsular tissue in an energy-dependent fashion, but type I Collagen content and nonreducible corsslinks were not significantly altered.

NASA Discipline Musculoskeletal↗

NASA NTRS2003

Development of a safe ground to space laser propagation system for the optical communications telescope laboratory

Furthering pursuits in high bandwidth communications to future NASA deep space and neat-Earth probes, the Jet Propulsion Laboratory (JPL) is building the Optical communications Telescope Laboratory (OCTL) atop Table Mountain in Southern California. This R&D optical antenna will be used to develop optical communication strategies for future optical ground stations. Initial experiments to be conducted include propagating high-powered, Q-switched laser beams to retro-reflecting satellites. Yet laser beam propagation from the ground to space is under the cognizance of various government agencies, namely: the Occupational Safety and Health Administration (ISHA) that is responsible for protecting workforce personnel; the Federal Aviation Administration (FAA) responsible for protecting pilots and aircraft; and the Laser Clearinghouse of Space Command responsible for protecting space assets. To ensure that laser beam propagation from the OCTL and future autonomously operated ground stations comply with the guidelines of these organizations, JPL is developing a multi-tiered safety system that will meet the coordination, monitoring, and reporting functions required by the agencies. At Tier 0, laser operators will meet OSHA safety standards for protection and access to the high power lasers area will be restricted and interlocked. Tier 1, the area defined from the telescope dome out to a range of 3.4-km, will utilize long wave infrared camera sensors to alert operators of at risk aircraft in the FAA controlled airspace. Tier 2, defined to extend from 3.4-km out to the aircraft service ceiling in FAA airspace, will detect at risk aircraft by radar. Lastly, beam propagation into space, defined as Tier 3, will require coordination with the Laser Clearinghouse. A detailed description of the four tiers is presented along with the design of the integrated monitoring and beam transmission control system.

laser safety↗

NASA NTRS2016

Airborne Measurements of Atmospheric Methane Using Pulsed Laser Transmitters

Atmospheric methane (CH4) is the second most important anthropogenic greenhouse gas with approximately 25 times the radiative forcing of carbon dioxide (CO2) per molecule. At NASA Goddard Space Flight Center (GSFC) we have been developing a laser-based technology needed to remotely measure CH4 from orbit. We report on our development effort for the methane lidar, especially on our laser transmitters and recent airborne demonstration. Our lidar transmitter is based on an optical parametric process to generate near infrared laser radiation at 1651 nanometers, coincident with a CH4 absorption. In an airborne flight campaign in the fall of 2015, we tested two kinds of laser transmitters --- an optical parametric amplifier (OPA) and an optical parametric oscillator (OPO). The output wavelength of the lasers was rapidly tuned over the CH4 absorption by tuning the seed laser to sample the CH4 absorption line at several wavelengths. This approach uses the same Integrated Path Differential Absorption (IPDA) technique we have used for our CO2 lidar for ASCENDS. The two laser transmitters were successfully operated in the NASAs DC-8 aircraft, measuring methane from 3 to 13 kilometers with high precision.

optical radar↗

NASA NTRS2016

Development and Characterization of a Small Spacecraft Electro-Optic Scanner for Free-Space Laser Communications

Emergent data-intensive missions coupled with dramatic reductions in spacecraft size plus an increasing number of space-based missions necessitates new high performance, compact and low cost communications technology. Free space optical communications offer advantages including orders of magnitude increase for data rate performance, increased security, immunity to jamming and lack of frequency allocation requirements when compared with conventional radio frequency (RF) means. The spatial coherence and low divergence associated with the optical frequencies of laser communications lends themselves to superior performance, but this increased directionality also creates one of the primary technical challenges in establishing a laser communications link by repeatedly and reliably pointing the beam onto the receive aperture. Several solutions have emerged from wide angle (slow) mechanical articulation systems, fine (fast) steering mirrors and rotating prisms, inertial compensation gyros and vibration isolation cancellation systems, but each requires moving components and imparts a measured amount of burden on the host platform. The complexity, cost and size of current mechanically scanned solutions limits their platform applicability, and restricts the feasibility of deploying optical communications payloads on very compact spacecraft employing critical systems. A high speed, wide angle, non-mechanical solution is therefore desirable. The purpose of this work is to share the development, testing, and demonstration of a breadboard prototype electro-optic (EO) scanned laser-communication link (see Figure 1). This demonstration is a step toward realizing ultra-low Size, Weight and Power (SWaP) SmallSat/MicroSat EO non-mechanical laser beam steering modules for high bandwidth ( greater than Gbps) free-space data links operating in the 1550 nm wavelength bands. The elimination of all moving parts will dramatically reduce SWaP and cost, increase component lifetime and reliability, and simplify the system design of laser communication modules. This paper describes the target mission architectures and requirements (few cubic centimeters of volume, 10's of grams of weight with milliwatts of power) and design of the beam steering module. Laboratory metrology is used to determine the component performance including horizontal and vertical resolution (20urad) as a function of control voltage (see Figure 2), transition time (0.1-1ms), pointing repeatability and optic insertion loss. A test bed system demonstration, including a full laser communications link, is conducted. The capabilities of this new EO beam steerer provide an opportunity to dramatically improve space communications through increased utilization of laser technology on smaller platforms than were previously attainable.

Laser Optical Communications↗

NASA NTRSDate not supplied

Estimation of Timing Performance with Pulsed Laser Links for Small Satellite PNT

Satellite constellations are growing in size and in utility for applications as diverse as providing reliable, low-latency internet service to rural areas orEarth science missions.This expansion of satellite constellations brings attention to the need for responsive and reliable satellite communication.Current research in the PrecisionSpace Systems Laboratory at the University of Florida focuses on using pulsed laser communications as the method of relaying time signals instead of the radio frequency (RF)signals.The upcoming CLICK (CubeSat Laser Infrared CrosslinK) missions (Massachusetts Institute of Technology, University of Florida, NASA Ames Research Center) will demonstrate a spacecraft-to-spacecraft laser communication link and time-transfer.For pre-flight technology assessment of missions such as CLICK, a simulation of a spacecraft constellation in Earth orbit has been created to estimate clock synchronization and precision orbit determination based on measured instrumentation performance.We have developed a novel MATLAB-based numerical simulator to model spacecraft-to-spacecraft laser time-transfer and estimate the offset between the spacecraft clocks over time.This simulation includes timing errors associated with laser pulse generation and detection, as well as non-Gaussian clock drift models.The two on-board clocks modeled are a cesium-based Chip-Scale Atomic Clock (CSAC) and a rubidium-based Miniature Atomic Clock (MAC), both produced by Microchip.An example case of two spacecraft in a circular, low-Earth orbit receiving GPS position, GPS timing, and laser pulse time-of-flight measurements is simulated.The positions and velocities of the two spacecraft at a reference epoch and the constant clock model coefficients are estimated.Polynomial models of different orders were used as clock models. The effect of clock model order on the root-mean-square (RMS) of the clock error is apparent in the case using GPS and lasing measurements, showing that the clock model improves with increasing clock model order. Results compare the estimated clock model of a mission operation that only uses GPS measurements and a mission operation that uses both GPS and laser pulse time-of-flight measurements between spacecraft referenced to their on-board CSACs or on-board MACs. Including lasing measurements reduces the RMS clock model error by approximately 80% of the RMS of the cases with only GPS measurements.This simulation tool can be used to optimize the lasing operations schedule based on mission timing performance objectives. During this presentation, I will discuss the details of the simulation and clock model estimation, as well as discuss the results.I will compare the results of incorporating lasing timing measurements to using only GPS measurements and the outcomes of using different orders of polynomials.

Timing Performance↗

NASA NTRSDate not supplied

Independent Reliability Assessment and Progress Review of the NASA GSFC Laser Transmitter for the LISA Program

NASA Goddard Space Flight Center (GSFC) has been actively developing the laser transmitter for the Laser Interferometer Space Antenna (LISA) program since the late 2017. In 2021 we delivered a prototype laser transmitter to the LISA program for performance evaluation as well as performed an independent technology assessment on the laser design supported by the NASA Engineering and Safety Center (NESC). We continued to further develop the LISA laser with a goal of advancing the technology readiness level (TRL) of the laser to 6 by the end of 2023. In this paper, we report on the progress we made on the laser development for the LISA program as well as the technology assessment findings by the NESC.

Independent Reliability Assessment↗

NASA NTRSDate not supplied

Laser Beam Welding Advancements for In-Space Servicing, Assembly, and Manufacturing

NASA is currently working to develop in-space servicing, assembly, and manufacturing (ISAM) capabilities for low Earth orbit and the lunar surface. One crucial technology for this effort is laser beam welding. Laser systems can perform joining, cleaning, cutting, and repair activities, which will enable the construction of large in-space structures that could not fit on a single launch vehicle, such as trusses for solar panels, radiators, or communications infrastructure. Multiple projects studying laser welding for space applications are currently underway at NASA Marshall Space Flight Center. One of these, the DIsk-Shaped Configurable and Modular vAcuum uNit (DISCMAN), is a compact vacuum chamber designed to support parameter development for laser welding in microgravity. It contains a rotating platen with weld samples made from aluminum, steel, and titanium, a high-power infrared laser, and integrated pumps for pulling vacuum inside the sample cartridge. The DISCMAN payload is planned to launch to the International Space Station, where welds will be performed under sustained microgravity inside the Bishop Airlock. Another effort underway at Marshall is the Lunar Assembly and Servicing by Autonomous Robotics (LASAR) initiative. This project uses a space-rated robotic arm equipped with a laser weld head, wire feeder, and multiple cameras to perform welds in a thermal vacuum chamber simulating the lunar surface environment. Some of these welds are done on snowflake joints, which are specially designed to slot together to join segments of trussN structures, allowing for the construction of tall surface infrastructure. DISCMAN, LASAR, and other projects are being carried out to advance the technological maturity of in-space laser beam welding, collect data to inform computational models, and learn reliable processes for creating weld joints in space. This work supports NASA’s greater goals to expand humanity’s presence in low Earth orbit, establish a permanent moon base, and eventually send crewed missions to Mars and beyond.

Manufacturing↗

NASA NTRSDate not supplied

Laser Beam Welding Advancements for In-Space Servicing, Assembly, and Manufacturing

Robotics↗

DOE OSTI2018

Study on high-flux laser ion source with applying magnetic field

The laser ion source is a technology where by irradiating a solid target with a pulsed laser of high intensity (10 8 W/cm 2 ~), ablation plasma is generated, and by applying there an external electric field for extracting and accelerating ions, high brightness ion beams are produced. This paper introduced the basic features of laser ion source and recent movement of the control of laser ion source using magnetic field. In the development of heavy ion inertial fusion (HIF) driver, engineers are challenging new tasks of supplying low valence, large current, and low emittance beams. In order to respond to the requirements of large current beams in HIF driver, attempts have been made to control the plasma via magnetic field to further increase the flux. The current of the laser ion source with application of solenoid magnetic field is dramatically improved and its amplification magnification can be adjusted by changing the position, length, and magnetic flux density of the solenoid. In order to further control the laser ion source toward HIF, the authors propose the guiding of plasma via multiple cusp magnetic field, and the guiding effect is being demonstrated through examination. According to the studies so far, the laser ion source can supply ion beams using a simple configuration, so it is suitable for miniaturization and may be adopted at many accelerator facilities. (A.O.)

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

DOE OSTI2020

Hollow fiber mid-ID spectrometer with UV laser ablation sampling for fine spatial reoslution of isotope ratios in solids

We describe a system that combines isotope ratio analysis via mid-infrared (Mid-IR) laser absorption spectroscopy with fine spatial resolution sampling using a UV pulsed laser. The UV laser ablates a pit in a solid on the order of 10 microns in diameter. The sample-derived particulates resulting from laser ablation pass through a micro-combustor, and the resulting gas is analyzed using Mid-IR laser absorption spectroscopy in a capillary absorption spectrometer (CAS). The CAS uses a hollow fiber optic waveguide with a reflective inner coating and a small internal volume on the order of 1ml. The hollow fiber both guides the laser light from source to detector and contains the gas sample at reduced pressure. Near unity overlap between the laser beam and sample enables sensitive analysis with ultra-small sample size. A prototype system has been demonstrated to enable stable carbon isotopic analysis (d13C) with 1 per mil precision using <1 picomole of carbon and is currently being used to study nutrient exchange in soil/root/microbial rhizosphere studies. The smaller sample size of this system is enabling fine spatial resolution analysis (on the order of 10 microns), which is roughly an order of magnitude smaller than was possible with an isotope ratio mass spectrometer (IRMS). In addition to rhizosphere studies, the system can provide a useful tool for fine scale isotope analysis with applications in biological, forensic, and environmental science.

capillary absorption spectroscopy, laser ablation,↗

DOE OSTI2023

High Throughput Laser Processing for Enhanced Battery Performance and Manufacturing

For widespread adoption of electric vehicles, lithium-ion batteries (LiBs) need to achieve energy densities of >275 Wh/kg, cell costs less than $100/kWh, and charge to more than 80% capacity within 15 minutes. Recently, it has been shown that introducing a secondary pore network in thick battery electrodes enables higher extracted capacity without a severe reduction in charge/discharge rate performance. Secondary pore networks consisting of ordered arrays of microstructures reduce tortuosity of Li+-ion transport deep into the thick electrodes, diminishing detrimental concentration gradients within the cell. Ultrafast (femtosecond)-pulsed laser ablation is a promising method to introduce such micro pores or channels in thick battery electrodes as it allows for precise control of pattern geometries, results in minimal damage to the electrode, and can be introduced into existing roll-to-roll electrode manufacturing lines. We have explored laser patterning to create secondary pore networks in a variety of battery electrode materials for both anode and cathode applications and characterized the laser-material interaction parameters. In addition, advanced materials characterization techniques (SEM-EDS, XRD) were used to explore whether ultrafast laser ablation affects the remaining electrode materials' morphology and structure. Furthermore, we have translated lab-scale laser ablation to high-throughput roll-to-roll processing at industrially relevant scales. Finally, we worked with Argonne National Laboratory, developers of the battery cost-analysis package BatPac, to estimate the additional manufacturing costs (CapEx and OpEx) for incorporation of laser-ablation processing to current battery electrode manufacturing. We estimate that ultrafast laser processing will add only -$1kWh, which for considerable improvements in cell performance, creates a compelling case for industry adoption.

battery↗

DOE OSTI2018

Assessing High-energy, Laser-driven, X-ray Sources as a Technique to Analyse ILW Containers - 18242

The principle concern regarding intermediate level waste (ILW) containers is the internal volumetric expansion due to the formation of corrosion products. To tackle this (via non-destructive testing) the development of a new technique to identify problematic containers was initiated by radiographic imaging and neutron assay of small scale, simulated, nuclear waste packages. This was achieved using a high-energy laser pulse to produce a bright burst of high-energy Bremsstrahlung radiation for imaging and a pulse of thermal energy neutrons for isotopic quantification. The small scale, simulated, nuclear waste packages (typically a quarter of a 28 mm natural uranium penny encased in grout) were produced with corrosion from oxygen and hydrogen rich environments to simulate the potential effects of long term storage. These samples were characterised using electron and ion beam techniques prior to encapsulation to establish the extent of corrosion and sample morphology. The small-scale samples were analysed using high-resolution x-ray tomography (XRT). These 3D pictures identified the corrosion state of the material and the effect on the surrounding grout matrix. These data sets were used as a baseline to compare with the 2D images obtained from the high-energy radiography to ascertain the imaging quality and potential capability of a laser driven inspection system. The study established the non-destructive imaging capability of a high-energy laser driven x-ray source for identifying fine features such as corrosion products on uranium samples encased in grout and cracks, and for penetrative imaging through large thicknesses of grout. In addition, generation of laser-driven neutrons of thermal energy required for active interrogation of uranium isotopes is demonstrated experimentally and simulations of the neutron inspection method are presented, thus paving the way for criticality testing of ILW containers. This current study is single pulse exposure acquisition, but the data can be used to predict the potential capability of a diode-pumped laser-driven system operating at, or above, 10 Hz by utilising, for example, the Dipole laser technology recently delivered by the STFC Central Laser Facility. Such a system will enable 3D tomography of nuclear waste containers and also greatly reduced signal to noise ratio via multiple acquisition and image stacking. (authors)

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗