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NASA NTRS2014

Near Infrared Cavity Ring-Down Spectroscopy for Isotopic Analyses of CH4 on Future Martian Surface Missions

A compact Near Infrared Continuous Wave Cavity Ring-Down Spectrometer (near-IR-cw-CRDS) was developed as a candidate for future planetary surface missions. The optical cavity was made of titanium with rugged quartz windows to protect the delicate super cavity from the harsh environmental changes that it would experience during space flight and a Martian surface mission. This design assured the long-term stability of the system. The system applied three distributed feedback laser diodes (DFB-LD), two of which were tuned to the absorption line peaks of (sup 12)CH4 and (sup 13)CH4 at 6046.954 inverse centimeters and 6049.121 inverse centimeters, respectively. The third laser was tuned to a spectral-lines-free region for measuring the baseline cavity loss. The multiple laser design compensated for typical baseline drift of a CRDS system and, thus, improved the overall precision. A semiconductor optical amplifier (SOA) was used instead of an Acousto-Optic Module (AOM) to initiate the cavity ring-down events. It maintained high acquisition rates such as AOM, but consumed less power. High data acquisition rates combined with improved long-term stability yielded precise isotopic measurements in this near-IR region even though the strongest CH4 absorption line in this region is 140 times weaker than that of the strongest mid-IR absorption band. The current system has a detection limit of 1.4 times 10( sup –12) inverse centimeters for (sup 13)CH4. This limit corresponds to approximately 7 parts per trillion volume of CH4 at 100 Torrs. With no further improvements the detection limit of our current near IR-cw-CRDS at an ambient Martian pressure of approximately 6 Torrs (8 millibars) would be 0.25 parts per billion volume for one 3.3 minute long analysis.

portable nir crds↗

DOE OSTI2020

High power edge-cum-surface emitting terahertz laser arrays phased locked by vacuum guided plasmon waves

Terahertz semiconductor quantum-cascade lasers (QCLs) are widely implemented with metallic cavities that support low-loss plasmonic optical modes at long wavelengths. However, resonant optical modes in such cavities suffer from poor radiative characteristics due to their subwavelength transverse dimensions. Consequently, single-mode terahertz QCLs with metallic cavities and large (>100 mW) output power have only been realized in the surface-emitting configuration that affords a large radiating surface. Here, we demonstrate a method to enhance radiative outcoupling from such plasmonic lasers for high-power emission in the edge-emitting (end-fire or longitudinal) direction. Single-sided plasmon waves propagating in vacuum are resonantly excited in surrounding medium of metallic cavities with the QCL semiconductor medium. The vacuum guided plasmon waves with a large wavefront phase-lock multiple metallic cavities longitudinally, which leads to intense radiation in multiple directions, including that in the longitudinal direction in a narrow single-lobed beam. The multicavity array radiates predominantly in a single spectral mode. A peak-power output of 260 mW and a slope efficiency of 303 mW/A are measured for the end-fire beam from a 3.3 THz QCL operating at 54 K in a Stirling cooler. Finally, single-mode operation and lithographic tuning across a bandwidth of ~150 GHz are demonstrated.

42 ENGINEERING↗

DOE OSTI2023

Non-Richtmyer–Meshkov instability ejecta production based on shallow bubble collapse

The study of shock-driven ejecta production has focused on Richtmyer–Meshkov instability (RMI) growth from geometric features of the material surface. Extensive study of this mechanism under both single- and multiple-shock conditions has found that the ejected mass tends to be closely associated with the shocked surface phase, and its temperature is not dramatically greater than the hydrodynamic shock temperature of the bulk. In this work, we propose and demonstrate a new ejecta production mechanism that can occur under multiple-shock conditions based on the collapse of bubbles near the free surface of the material. This mechanism produces ejected mass that is much greater in quantity than observed in the RMI case. The particles are much hotter than predicted by the shock Hugoniot state, and the ejected mass does not appear to be strongly dependent upon initial surface finish. The ejecta source extends into the material with no clear remaining free surface. We name this mechanism Shallow Bubble Collapse (SBC) and discuss the conditions under which it activates. We demonstrate resolved modeling methods that enable the calculation, design, and study of SBC as a mechanism and perform a series of experiments to compare with the models. Under some multiple-shock conditions, SBC ejection produces ten times more ejected mass than RMI growth.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

DOE OSTI2021

Demonstration of a 20‐W membrane‐external‐cavity surface‐emitting laser for sodium guide star applications

Abstract We present a record 20‐W continuous‐wave output power membrane‐external‐cavity surface‐emitting laser (MECSEL) double‐bonded to silicon carbide (SiC) heat spreaders emitting around 1178 nm. We achieved a maximum slope efficiency of 27.7% and an optical‐to‐optical efficiency of 26.7%. By utilising an intracavity birefringent filtre, the wavelength was tuned over 75 nm and maximum output power of 12.7 W was recorded at 1178 nm. This study shows the potential of MECSELs to achieve high‐performance and cost‐effective optically pumped semiconductor disk lasers targeting applications in sodium guide stars.

Priante, D.↗

DOE OSTI2025

Unraveling the Surface Termination and Evolution of Surface States for Electrocatalyst PtSn 4 in Alkaline HER

Semimetal PtSn 4 has been experimentally demonstrated as a promising topological electrocatalyst for the hydrogen evolution reaction (HER) under both acidic and alkaline conditions. While two possible mechanisms have been proposed to explain its activity, the role of its surface states in HER remains unclear. It is indeed in question how the surface states of this alloy evolve as HER proceeds. In this study, we investigate the surface termination that sustains conducting surface states on PtSn 4 , and we track their evolution during HER catalysis. We show that a reconstructed surface with a Sn-poor termination reproduces the scanning tunneling microscopy pattern observed in experiments and sustains a conducting surface. Through phase diagram and geometric structure analysis, we outline the HER profile following the Volmer–Heyrovsky mechanism. As hydrogen atoms adsorb onto the surface, the structure undergoes further reconstruction to an equilibrium phase with a coverage of two hydrides per unit cell. Meanwhile, the surface electronic bands evolve in response to interactions with the adsorbed hydrogen atoms. A hybridization diagram is further proposed for understanding the surface state evolution based on wave function and chemical bonding analyses. While the Pt atoms serve as conventional sites for hydrogen binding, the surface states of PtSn 4 are essential for stabilizing the hydrogen antibonding states via in-phase electronic interactions with the Sn components. This stabilization results in frontier surface bands that are responsible for driving the HER catalysis. Here, our findings provide a detailed description for the direct involvement of surface states on PtSn4 when employed as a catalyst for HER.

catalysts↗

NASA NTRS2022

Mars Climate Sounder Observations of Gravity Wave Activity throughout Mars’s Lower Atmosphere

Gravity waves are one way Mars’s lower atmospheric weather can affect the circulation and even composition of Mars’s middle and upper atmosphere. A recent study showed how on-planet observations near the center of the 15 micron CO2band by the A3 channel(635–665 cm−1)of the Mars Climate Sounder on board Mars Reconnaissance Orbiter (MRO-MCS) could sense horizontally short, vertically broad gravity waves at≈25 km above the surface by looking at small-scale radiance variability in temperature-sensitive channels. This approach is extended here to two additional channels closer to the wings of the 15 micron CO2band,A1 (595–615 cm−1) and A2 (615–645 cm−1), to sense gravity waves throughout the lower atmosphere. Using information from all three channels demonstrates that gravity wave activity in Mars’s lowermost atmosphere is dominated by orographic sources, particularly over the extremely rough terrain of Valles Marineris. Much of this orographic population is either trapped or filtered in the lowest two scale heights, such that variations in filtering and non-orographic sources shape the gravity wave population observed at 25 km above the surface. During global dust storms, however, gravity wave activity in the first scale height decreases by approximately a factor of two, yet trapping/filtering of what activity remains in the tropics substantially weakens. Exceptionally high radiance variability at night in the tropics during the less dusty part of the year is the result of observing mesospheric clouds rather than gravity waves.

Nicholas G Heavens↗

DOE OSTI2024

Emergence of two distinct phase transitions in monolayer CoSe2 on graphene

Abstract Dimensional modifications play a crucial role in various applications, especially in the context of device miniaturization, giving rise to novel quantum phenomena. The many-body dynamics induced by dimensional modifications, including electron-electron, electron-phonon, electron-magnon and electron-plasmon coupling, are known to significantly affect the atomic and electronic properties of the materials. By reducing the dimensionality of orthorhombic CoSe 2 and forming heterostructure with bilayer graphene using molecular beam epitaxy, we unveil the emergence of two types of phase transitions through angle-resolved photoemission spectroscopy and scanning tunneling microscopy measurements. We disclose that the 2 × 1 superstructure is associated with charge density wave induced by Fermi surface nesting, characterized by a transition temperature of 340 K. Additionally, another phase transition at temperature of 160 K based on temperature dependent gap evolution are observed with renormalized electronic structure induced by electron-boson coupling. These discoveries of the electronic and atomic modifications, influenced by electron-electron and electron-boson interactions, underscore that many-body physics play significant roles in understanding low-dimensional properties of non-van der Waals Co-chalcogenides and related heterostructures. Graphical Abstract

36 MATERIALS SCIENCE↗

NASA NTRS2012

Polarimetric Retrievals of Surface and Cirrus Clouds Properties in the Region Affected by the Deepwater Horizon Oil Spill

In 2010, the Goddard Institute for Space Studies (GISS) Research Scanning Polarimeter (RSP) performed several aerial surveys over the region affected by the oil spill caused by the explosion of the Deepwater Horizon offshore platform. The instrument was deployed on the NASA Langley B200 aircraft together with the High Spectral Resolution Lidar (HSRL), which provides information on the distribution of the aerosol layers beneath the aircraft, including an accurate estimate of aerosol optical depth. This work illustrates the merits of polarization measurements in detecting variations of ocean surface properties linked to the presence of an oil slick. In particular, we make use of the degree of linear polarization in the glint region, which is severely affected by variations in the refractive index but insensitive to the waviness of the water surface. Alterations in the surface optical properties are therefore expected to directly affect the polarization response of the RSP channel at 2264 nm, where both molecular and aerosol scattering are negligible and virtually all of the observed signal is generated via Fresnel reflection at the surface. The glint profile at this wavelength is fitted with a model which can optimally estimate refractive index, wind speed and direction, together with aircraft attitude variations affecting the viewing geometry. The retrieved refractive index markedly increases over oil-contaminated waters, while the apparent wind speed is significantly lower than in adjacent uncontaminated areas, suggesting that the slick dampens high-frequency components of the ocean wave spectrum. The constraint on surface reflectance provided by the short-wave infrared channels is a cornerstone of established procedures to retrieve atmospheric aerosol microphysical parameters based on the inversion of the RSP multispectral measurements. This retrieval, which benefits from the ancillary information provided by the HSRL, was in this specific case hampered by prohibitive variability in atmospheric conditions (very inhomogeneous aerosol distribution and cloud cover). Although the results presented for the surface are essentially unaffected, we discuss the results obtained by typing algorithms in sorting the complex mix of aerosol types, and show evidence of oriented ice in cirrus clouds present in the area. In this context, polarization measurements at 1880 nm were used to infer ice habit and cirrus optical depth, which was found in the subvisual/threshold-visible regime, confirming the utility of the aforementioned RSP channel for the remote sensing of even thin cold clouds.

Polarization↗

NASA NTRS1974

A uniform geometrical theory of diffraction for an edge in a perfectly conducting surface

A compact dyadic diffraction coefficient for electromagnetic waves obliquely incident on a curved edge formed by perfectly conducting curved or plane surfaces is obtained. This diffraction coefficient remains valid in the transition regions adjacent to shadow and reflection boundaries, where the diffraction coefficients of Keller's original theory fail. Our method is based on Keller's method of the canonical problem, which in this case is the perfectly conducting wedge illuminated by plane, cylindrical, conical, and spherical waves. When the proper ray-fixed coordinate system is introduced, the dyadic diffraction coefficient for the wedge is found to be the sum of only two dyads, and it is shown that this is also true for the dyadic diffraction coefficients of higher order edges. One dyad contains the acoustic soft diffraction coefficient; the other dyad contains the acoustic hard diffraction coefficient. The expressions for the acoustic wedge diffraction coefficients contain Fresnel integrals, which ensure that the total field is continuous at shadow and reflection boundaries.

Kouyoumjian, R. G.↗

NASA NTRS1995

Acoustic receptivity due to weak surface inhomogeneities in adverse pressure gradient boundary layers

The boundary layer receptivity to free-stream acoustic waves in the presence of localized surface disturbances is studied for the case of incompressible Falkner-Skan flows with adverse pressure gradients. These boundary layers are unstable to both viscous and inviscid (i.e., inflectional) modes, and the finite Reynolds number extension of the Goldstein-Ruban theory provides a convenient method to compare the efficiency of the localized receptivity processes in these two cases. The value of the efficiency function related to the receptivity caused by localized distortions in surface geometry is relatively insensitive to the type of instability mechanism, provided that the same reference length scale is used to normalize the efficiency function for each type of instability. In contrast, when the receptivity is induced by variations in wall suction velocity or in wall admittance distribution, the magnitudes of the related efficiency functions, as well as the resulting coupling coefficients, are smaller for inflectional (i.e., Rayleigh) modes than for the viscous Tollmien-Schlichting waves. The reduced levels of receptivity can be attributed mainly to the shorter wavelengths and higher frequencies of the inflectional modes. Because the most critical band of frequencies shifts toward higher values, the overall efficiency of the wall suction- and the wall admittance-induced receptivity decreases with an increase in the adverse pressure gradient.

Choudhari, Meelan↗

NASA NTRS2004

A Study of Supersonic Surface Sources: The Ffowcs Williams-Hawkings Equation and the Kirchhoff Formula

In this paper we address the mathematical problem of noise generation from high speed moving surfaces. The problem we are solving is the linear wave equation with sources on a moving surface. The Ffowcs Williams-Hawkings (FW-H) equation as well as the govern- ing equation for deriving the Kirchhoff formula for moving surfaces are both this type of partial differential equation. We give a new exact solution of this problem here in closed form which is valid for subsonic and supersonic motion of the surface but it is particularly suitable for supersonically moving surfaces. This new solution is the simplest of all high speed formulations of Langley and is denoted formulation 4 following the tradition of numbering of our major results for the prediction of the noise of rotating blades. We show that for a smooth surface moving at supersonic speed, our solution has only removable singularities. Thus it can be used for numerical work.

Farassat, F.↗

NASA NTRS1989

Scatterometer azimuthal response and wind wave directionality

Azimuthal response of a scatterometer to radiation scattered by the sea surface was studied in a wind-wave tank. The variation of the normalized radar cross section with the azimuth angle is fitted by a three-term series. Results show that the upwind-downwind asymmetry decreases as the wind speed increases. The crosswind modulation depends on the wind velocity. The results show that the evolution of the long-wind-crosswind ratio evolves with wind speed in a manner similar to the evolution of the isotropy of short capillary-gravity waves. The maximum of the isotropy of the short wind waves is obtained for wind velocities close to 4 m/s. For the same value of the velocity, the variations of radar response between long-wind and crosswind directions is minimum. For lower or higher values of wind velocities the directional accuracy of the radar increases, since the wind-wave field tends to align in the wind direction.

Giovanangeli, J. P.↗

NASA NTRS1983

Remote sensing with spaceborne synthetic aperture imaging radars: A review

A review is given of remote sensing with Spaceborne Synthetic Aperture Radars (SAR's). In 1978, a spaceborne SA was flown on the SEASAT satellite. It acquired high resulution images over many regions in North America and the North Pacific. The acquired data clearly demonstrate the capability of spaceborne SARs to: image and track polar ice floes; image ocean surface patterns including swells, internal waves, current boundaries, weather boundaries and vessels; and image land features which are used to acquire information about the surface geology and land cover. In 1981, another SAR was flown on the second shuttle flight. This Shuttle Imaging Radar (SIR-A) acquired land and ocean images over many areas around the world. The emphasis of the SIR-A experiment was mainly toward geologic mapping. Some of the key results of the SIR-A experiment are given.

Cimino, J. B.↗

DOE OSTI2021

Some aspects of the five-dimensional Lovelock black hole spacetime: Strong homotopy retract, perihelion precession and quasistationary levels

Highlights: • Some topological aspects are explored. • The perihelion precession is calculated. • The general Heun functions are applied to obtain analytical solutions. • The quasibound states and the radial wave eigenfunctions are obtained. In this work we explore some mathematical physics aspects of the spherically symmetric Lovelock black hole in high dimensions. Intended for this aim, we thoroughly consider the metric corresponding to the five-dimensional Lovelock black hole spacetime. We construct the strong retractions by the geodesic equations on the background under consideration. As a result, from the topological point of view, we construct the theory of strong homotopy retract, which will allow us, in principle, to better understand some of its suitable applications on astrophysics and cosmology, in particular, in the analysis of the spacetime singularities. We find the solutions of the equation of motion for both radial and angular coordinates, and then we describe the outer (“exterior”) and lower (“interior”) apparent horizons. Indeed, the outer apparent horizon is the last surface from which the light waves could still escape from the black hole. Thus, it is meaningful to analyze some physical phenomena related to quantum particles propagating outside the exterior apparent horizon, in particular, we discuss the quasistationary levels of scalar fields and their radial wave functions, which are given in terms of the general Heun functions. We also calculate the perihelion precession in this background.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

NASA NTRS1977

The tropospheric-stratospheric polar vortex breakdown of January 1977

An extraordinary warming of the stratosphere in December-January 1976-77 was followed by tropospheric warming in the polar region and cooling in middle latitudes. During January 10-20, the associated polar anticyclone extended from the surface to 10 mb. Antecedents of the polar vortex breakdown are reviewed with the aid of results of zonal-harmonic analyses of planetary waves, for heights of the pressure surfaces (700-10 mb), temperature, and mean stratospheric temperature (the latter determined from satellite radiation measurements). Wave 1 in height and temperature played a dominant role in the stratosphere, attaining amplitudes of 1600 gpm and 25 C, respectively, at 10 mb. On the other hand, superposition of retrogressing wave 1 and quasi-stationary wave 2 in the height of the 300-mb surface, with individual amplitudes exceeding 300 gpm, is judged to have been an important factor in the overall development.

Quiroz, R. S.↗

NASA NTRS2002

Containerless Ripple Turbulence

One of the longest standing unsolved problems in physics relates to the behavior of fluids that are driven far from equilibrium such as occurs when they become turbulent due to fast flow through a grid or tidal motions. In turbulent flows the distribution of vortex energy as a function of the inverse length scale [or wavenumber 'k'] of motion is proportional to 1/k(sup 5/3) which is the celebrated law of Kolmogorov. Although this law gives a good description of the average motion, fluctuations around the average are huge. This stands in contrast with thermally activated motion where large fluctuations around thermal equilibrium are highly unfavorable. The problem of turbulence is the problem of understanding why large fluctuations are so prevalent which is also called the problem of 'intermittency'. Turbulence is a remarkable problem in that its solution sits simultaneously at the forefront of physics, mathematics, engineering and computer science. A recent conference [March 2002] on 'Statistical Hydrodynamics' organized by the Los Alamos Laboratory Center for Nonlinear Studies brought together researchers in all of these fields. Although turbulence is generally thought to be described by the Navier-Stokes Equations of fluid mechanics the solution as well as its existence has eluded researchers for over 100 years. In fact proof of the existence of such a solution qualifies for a 1 M$ millennium prize. As part of our NASA funded research we have proposed building a bridge between vortex turbulence and wave turbulence. The latter occurs when high amplitude waves of various wavelengths are allowed to mutually interact in a fluid. In particular we have proposed measuring the interaction of ripples [capillary waves] that run around on the surface of a fluid sphere suspended in a microgravity environment. The problem of ripple turbulence poses similar mathematical challenges to the problem of vortex turbulence. The waves can have a high amplitude and a strong nonlinear interaction. Furthermore, the steady state distribution of energy again follows a Kolmogorov scaling law; in this case the ripple energy is distributed according to 1/k (sup 7/4). Again, in parallel with vortex turbulence ripple turbulence exhibits intermittency. The problem of ripple turbulence presents an experimental opportunity to generate data in a controlled, benchmarked system. In particular the surface of a sphere is an ideal environment to study ripple turbulence. Waves run around the sphere and interact with each other, and the effect of walls is eliminated. In microgravity this state can be realized for over 2 decades of frequency. Wave turbulence is a physically relevant problem in its own right. It has been studied on the surface of liquid hydrogen and its application to Alfven waves in space is a source of debate. Of course, application of wave turbulence perspectives to ocean waves has been a major success. The experiment which we plan to run in microgravity is conceptually straightforward. Ripples are excited on the surface of a spherical drop of fluid and then their amplitude is recorded with appropriate photography. A key challenge is posed by the need to stably position a 10cm diameter sphere of water in microgravity. Two methods are being developed. Orbitec is using controlled puffs of air from at least 6 independent directions to provided the positioning force. This approach has actually succeeded to position and stabilize a 4cm sphere during a KC 135 segment. Guigne International is using the radiation pressure of high frequency sound. These transducers have been organized into a device in the shape of a dodecahedron. This apparatus 'SPACE DRUMS' has already been approved for use for combustion synthesis experiments on the International Space Station. A key opportunity presented by the ripple turbulence data is its use in driving the development of codes to simulate its properties.

Putterman, Seth↗

DOE OSTI2020

Imaging how thermal capillary waves and anisotropic interfacial stiffness shape nanoparticle supracrystals

Abstract Development of the surface morphology and shape of crystalline nanostructures governs the functionality of various materials, ranging from phonon transport to biocompatibility. However, the kinetic pathways, following which such development occurs, have been largely unexplored due to the lack of real-space imaging at single particle resolution. Here, we use colloidal nanoparticles assembling into supracrystals as a model system, and pinpoint the key role of surface fluctuation in shaping supracrystals. Utilizing liquid-phase transmission electron microscopy, we map the spatiotemporal surface profiles of supracrystals, which follow a capillary wave theory. Based on this theory, we measure otherwise elusive interfacial properties such as interfacial stiffness and mobility, the former of which demonstrates a remarkable dependence on the exposed facet of the supracrystal. The facet of lower surface energy is favored, consistent with the Wulff construction rule. Our imaging–analysis framework can be applicable to other phenomena, such as electrodeposition, nucleation, and membrane deformation.

77 NANOSCIENCE AND NANOTECHNOLOGY↗

DOE OSTI2026

Adsorption-based direct air capture using hierarchical porous composites prepared via confined-space crystallization

Capturing CO₂ at trace concentration remains a critical challenge in sustainable carbon management via adsorption, as conventional adsorbents suffer from low CO₂ selectivity, poor moisture tolerance, and energy-intensive regeneration requirements. Here, we report a hierarchical Ba²⁺-exchanged silicoaluminophosphate (Ba²⁺-CSAPO-34) composite synthesized via confined-space crystallization within an activated carbon matrix. Comprehensive characterization revealed a confined nucleation mechanism and the successful incorporation of Ba²⁺ active sites within the SAPO-34 framework, achieved via a two-step liquid ion-exchange protocol. The core-shell architecture combines the selective CO₂ binding of Ba²⁺-functionalized SAPO-34 with the hydrophobic protection of the carbon shell. Fixed-bed adsorption tests demonstrated strong CO₂ binding (at 500-2500 ppm), no roll-up, and effective suppression of water affinity, while maintaining high selectivity even at 90% relative humidity. A phenomenological adsorption model, validated against dynamic breakthrough data, accurately predicted dynamic adsorption behavior under real-world operating conditions, enabling rational process design for direct air capture (DAC) and closed-loop life support systems. Furthermore, these results establish Ba²⁺-CSAPO-34 as a scalable, moisture-resistant adsorbent that addresses key limitations in trace CO₂ capture, advancing practical implementation of carbon removal technologies.

77 NANOSCIENCE AND NANOTECHNOLOGY↗