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All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Directed assembly of hybrid nanostructures using optically resonant nanotweezers

This represents the final report for this project. Over the course of the project we have made significant progress in photonically driven nano-assembly including: (1) demonstrating the first direct optical tweezer based manipulation of proteins, (2) the ability to apply optical angular torques to microtubuals and other rod-shaped microparticles, (3) direct assembly of hybrid nanostructures comprising of polymeric nanoparticles and carbon nanotubes and, (4) the ability to drive biological reactions (specifically protein aggregation) that are thermodynamically unfavorable by applying localized optical work. These advancements are described in the list of papers provided in section 2.0 of the below. Summary details are provided in prior year annual reports. We have two additional papers which will be submitted shortly based on the work done under this award. An updated publication list will be provided to the program manager when those are accepted. In this report, we report on a new advancement made in the final project year, which uses the nanotweezer technology to perform direct measurements of particle-surface interactions. Briefly, these measurements are important for characterizing the stability and behavior of colloidal and nanoparticle suspensions and current techniques are limited in their ability to measure piconewton scale interaction forces on sub-micrometer particles due to signal detection limits and thermal noise. In this project year we developed a new technique called “Nanophotonic Force Microscopy” which uses the localized region of exponentially decaying, near-field, light to confine small particles close to a surface. From the statistical distribution of the light intensity scattered by the particle the technique maps out the potential well of the trap and directly quantify the repulsive force between the nanoparticle and the surface. The major advantage of the technique is that it can measure forces and energy wells below the thermal noise limit, resolving interaction forces smaller than 1 pN on dielectric particles as small as 100 nm in diameter.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Exploration of Options for Ultra-Fast Mass Spectroscopy for Pulsed Power Applications

Mega-ampere class pulsed power machines drive intense currents into small volumes to study high energy and density environments. Power lost during these events is a difficult and paramount problem to solve. For example, facilities such as Sandia National Laboratories’ Z machine experience meaningful power loss, which can be linked to non-linear ohmic heating at high currents (i.e., 26 MA on Z) leading to thermal desorption of contaminants and subsequent shunt plasma formation. Characterizing and understanding this type of thermal desorption is key to design optimizations necessary to minimize current loss, which will be even more important for next generation pulsed power. This type of characterization requires the ability to identify and determine concentration of analytes with nanosecond resolution given the pulse width of Z is on the order of 100 ns. This report summarizes progress on a small exploratory project focused on investigating options to meet this challenge using mass spectrometry. The main focus of these efforts utilized an Energy and Velocity Analyzer for Distributions of Electric Rockets intending to determine how quickly transient data could be resolved. This probe combines an electrostatic analyzer with a Wien velocity filter (ExB) to obtain ion energy and velocity distributions. Primary results from this exploratory project indicate significant additional work is needed to demonstrate a nanosecond time scale mass spectrometer for this application and also highlight that alternative detection methods such as laser-based diagnostics should be considered to meet the need for ultra-fast detection.

42 ENGINEERING↗
DOE OSTI2019

Microscopic Structural and Dynamic Features in Triphilic Room Temperature Ionic Liquids

Here we report a thorough investigation of the microscopic and mesoscopic structural organization in a series of triphilic fluorinated room temperature ionic liquids, namely [1-alkyl,3-methylimidazolium][(trifluoromethanesulfonyl)(nonafluorobutylsulfonyl)imide], with alkyl=ethyl, butyl, octyl ([C n mim][IM 14 ], n = 2, 4, 8), based on the synergic exploitation of X-ray and Neutron Scattering and Molecular Dynamics simulations. This study reveals the strong complementarity between X-ray/neutron scattering in detecting the complex segregated morphology in these systems at mesoscopic spatial scales. The use of MD simulations delivering a very good agreement with experimental data allows us to gain a robust understanding of the segregated morphology. The structural scenario is completed with determination of dynamic properties accessing the diffusive behavior and a relaxation map is provided for [C 2 mim][IM 14 ] and [C 8 mim][IM 14 ], highlighting their natures as fragile glass formers.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2022

Single-Molecule Chemical Reactions Unveiled in Molecular Junctions

Understanding chemical processes at the single-molecule scale represents the ultimate limit of analytical chemistry. Single-molecule detection techniques allow one to reveal the detailed dynamics and kinetics of a chemical reaction with unprecedented accuracy. It has also enabled the discoveries of new reaction pathways or intermediates/transition states that are inaccessible in conventional ensemble experiments, which is critical to elucidating their intrinsic mechanisms. Thanks to the rapid development of single-molecule junction (SMJ) techniques, detecting chemical reactions via monitoring the electrical current through single molecules has received an increasing amount of attention and has witnessed tremendous advances in recent years. Research efforts in this direction have opened a new route for probing chemical and physical processes with single-molecule precision. This review presents detailed advancements in probing single-molecule chemical reactions using SMJ techniques. We specifically highlight recent progress in investigating electric-field-driven reactions, reaction dynamics and kinetics, host–guest interactions, and redox reactions of different molecular systems. Finally, we discuss the potential of single-molecule detection using SMJs across various future applications.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2019

Constraints on a Putative Planet Sculpting the V4046 Sagittarii Circumbinary Disk

We analyze the highest-resolution millimeter continuum and near-infrared (NIR) scattered-light images presented to date of the circumbinary disk orbiting V4046 Sgr, a ∼20-Myr-old actively accreting, close binary T Tauri star system located a mere 72.4 pc from Earth. We observed the disk with the Atacama Large Millimeter/submillimeter Array (ALMA) at 870 μm during Cycle 4, and we analyze these data in conjunction with archival NIR (H band) polarimetric images obtained with SPHERE/IRDIS on the ESO Very Large Telescope. At 0.″3 (20 au) resolution, the 870 μm image reveals a marginally resolved ring that peaks at ∼32 au and has an extension of ∼90 au. We infer a lower limit on a dust mass of ∼60.0 M {sub ⊕} within the 870 μm ring, and confirm that the ring is well aligned with the larger -scale gaseous disk. A second, inner dust ring is also tentatively detected in the ALMA observations; its position appears coincident with the inner (∼14 au radius) ring detected in scattered light. Using synthetic 870 μm and H-band images obtained from disk–planet interaction simulations, we attempt to constrain the mass of the putative planet orbiting at 20 au. Our trials suggest that a circumbinary Jovian-mass planet may be responsible for generating the dust ring and gap structures detected within the disk. We discuss the longevity of the gas-rich disk orbiting V4046 Sgr in the context of the binary nature of the system.

79 ASTRONOMY AND ASTROPHYSICS↗
NASA NTRS1973

Study of application of ERTS-A imagery to fracture related mine safety hazards in the coal mining industry

The author has identified the following significant results. The utility of ERTS-1/high altitude aircraft imagery to detect underground mine hazards is strongly suggested. A 1:250,000 scale mined lands map of the Vincennes Quadrangle, Indiana has been prepared. This map is a prototype for a national mined lands inventory and will be distributed to State and Federal offices.

Wier, C. E.↗
NASA NTRS1973

Geographic analysis of landscape change from ERTS-1 imagery

The author has identified the following significant results. Data from low altitude flights and ground truth observations confirm the existence of significant strip mining activity at the Cumberland Plateau, Tennessee Test Site. A map (1:120,000) depicting landscape changes associated with strip mining on the Cumberland Plateau has been completed. The map was prepared from NASA generated RB-57 imagery for April 1972 and ERTS imagery for October 1972. A second map shows the generalized forest cover for the state of Tennessee. The data were derived entirely from five ERTS-1 images and reduced to an original map scale of 1:2.4 million. The most significant discovery concerns the detection, identification, and mapping of plowed fields in northern Alabama, northern Georgia, and southeastern Tennessee. In an April ERTS observation, plowed ground and bare soil surfaces were easily detected and mapped from MSS Band 5.

Rehder, J. B.↗
NASA NTRS1976

Thematic mapping, land use, geological structure and water resources in central Spain

The author has identified the following significant results. A method for a rapid updating of cartography at scale 1:200,000 was established. An annular tectonic structure was detected north of Madrid which was named Structural Halo of Guadalix, since its center is situated in the locality of Guadalix de la Sierra. This circular complex has from 30 to 40 km of radius and its influences at its most extreme edges reach Madrid.

Delascuevas, N.↗
NASA NTRS1981

Galaxy formation in an intergalactic medium dominated by explosions

The evolution of galaxies in an intergalactic medium dominated by explosions of star systems is considered analogously to star formation by nonlinearly interacting processes in the interstellar medium. Conditions for the existence of a hydrodynamic instability by which galaxy formation leads to more galaxy formation due to the propagation of the energy released at the death of massive stars are examined, and it is shown that such an explosive amplification is possible at redshifts less than about 5 and stellar system masses between 10 to the 8th and 10 to the 12th solar masses. Explosions before a redshift of about 5 are found to lead primarily to the formation of massive stars rather than galaxies, while those at a redshift close to 5 will result in objects of normal galactic scale. The model also predicts a dusty interstellar medium preventing the detection of objects of redshift greater than 3, numbers and luminosities of protogalaxies comparable to present observations, unvirialized groups of galaxies lying on two-dimensional surfaces, and a significant number of black holes in the mass range 1000-10,000 solar masses.

Ostriker, J. P.↗
NASA NTRS1987

A VLA gravitational lens survey

A VLA survey designed to detect gravitational lensing on sub-arc second and arc second scales is described, and preliminary results of radio data are presented. In particular, it is found that the density of matter in the form of a uniform comoving number density of 10 to the 11th - 10 to the 12th solar mass compact objects, luminous or dark, must be substantially less than the critical density. Data obtained for the radio source 1042+178 are briefly examined.

Hewitt, J. N.↗
NASA NTRS1990

The heliopause

A Pioneer or Voyager spacecraft will soon pass through one of the last major frontiers in the solar system - the heliospheric terminal shock. Some unknown, but perhaps small, distance beyond the terminal shock is the heliopause, marking the final boundary between solar-wind and Galactic plasmas and the final goal of these spacecraft. This occasion offers an opportunity to obtain a wealth of information on the properties of the Galaxy, the interstellar medium, and the large-scale interactions of that medium with stellar winds. Several tentative remote detections of the shock place it just beyond the present spacecraft locations. However, uncertainties in the physical processes and parameters that determine the location of the boundary lead to equal uncertainties in predicting which of the spacecraft will reach it first.

Suess, Steven T.↗
NASA NTRS1991

Probability of brittle failure

A methodology was developed for collecting statistically representative data for crack initiation and arrest from small number of test specimens. An epoxy (based on bisphenol A diglycidyl ether and polyglycol extended diglycyl ether and cured with diethylene triamine) is selected as a model material. A compact tension specimen with displacement controlled loading is used to observe multiple crack initiation and arrests. The energy release rate at crack initiation is significantly higher than that at a crack arrest, as has been observed elsewhere. The difference between these energy release rates is found to depend on specimen size (scale effect), and is quantitatively related to the fracture surface morphology. The scale effect, similar to that in statistical strength theory, is usually attributed to the statistics of defects which control the fracture process. Triangular shaped ripples (deltoids) are formed on the fracture surface during the slow subcritical crack growth, prior to the smooth mirror-like surface characteristic of fast cracks. The deltoids are complementary on the two crack faces which excludes any inelastic deformation from consideration. Presence of defects is also suggested by the observed scale effect. However, there are no defects at the deltoid apexes detectable down to the 0.1 micron level.

Kim, A.↗
NASA NTRS1992

One Year of Rayleigh Lidar Measurements at Toronto

The Rayleigh lidar technique is being used at York University to study middle atmospheric thermal structure with particular emphasis on the properties and influence of internal gravity waves. These measurements are now carried out on a routine basis (every clear night) in order to determine seasonal variability and, eventually, long term trends. The transmitter consists of a doubled Nd:YAG laser with an output of 0.4 Joules per pulse at 20Hz (8 Watts) which is expanded to obtain a divergence of 0.4 milliradians. Backscattered photons are collected by a half meter cassegrain telescope, filtered to a bandwidth of 1nm, detected by a PMT, and counted with a multi-channel scaling averager. Strong backscatter from lower altitudes is blocked using a rotating chopper (25000rpm) which triggers the laser. The range gate and hardware averaging interval are variable but typically 300m and 5 minutes. Relative density profiles are obtained by simply normalizing to a model (eg. CIRA) at some altitude. Absolute temperature is derived using the hydrostatic equation, ideal gas law, and a model pressure value at the altitude where the photocount statistical uncertainty is about 15 percent - typically 90km for the entire night's average. The lower limit is currently about 30-35km due the presence aerosol from the volcanic eruption of Mt. Pinatubo.

Whiteway, James A.↗
NASA NTRS1994

The phenomenological status of late time phase transition models after cosmic background radiation anisotropy measurements

Some relatively model-independent results for structure formation via late time phase transitions (LTPT) are discussed. In particular, generic LTPT power spectra are presented. The implication of the recent Cosmic Background Explorer (COBE) detection of the cosmic background radiation (CBR) anisotropy at large angular scales (greater than or approximately equal to 7 deg) and the tight upper limits from small angular scales (approximately 1 deg) to LTPT models are discussed. Special attention is focused on the observational constraints and possible non-Gaussian signatures of CBR temperature anisotropies from LTPT and other non-Gaussian models. It is shown that while LTPT have been seriously constrained by the recent data, viable models do remain which provide more power on the 100-200 Mpc scales than do more traditional primordial Gaussian density fluctuation models. Tests for such models are presented, including possible anisotropies on angular scales less than 8 min.

Luo, Xiaochun↗
NASA NTRS2001

Subsurface Sounding of Mars: The Effects of Surface Roughness

The Mars Advanced Radar for Subsurface and Ionospheric Sounding (MARSIS) will conduct a global survey of Mars from the Mars Express Orbiter starting in 2004. The primary objective of the subsurface observations is to detect material interfaces in the upper several kilometers of the crust of Mars, with a particular emphasis on mapping the 3D distribution of water and ice in that portion of the crust. In order to detect subsurface interfaces, the returned echo from the subsurface must be distinguished from noise and clutter, which can arise from a variety of sources. One source of clutter is surface topography that generates backscattered energy at the same time delay as the subsurface region of interest. Surface topography can affect the detectability of subsurface features in several other ways. Surface roughness at scales comparable or somewhat smaller than the radar wavelength reduces the coherency of the wave as it passes the upper interface. Also, surface slope (tilt) at scales of the radar footprint and larger (> 5 km) affects the apparent Doppler signature of the echoes, and effectively disperses the wave transmitted into the subsurface, making processing and interpretation difficult. In this paper, we report on the roughness characteristics of Mars at these various scales as measured by the Mars Global Surveyor Laser Altimeter (MOLA), and consider the implications for achieving the subsurface sounding goals of MARSIS. Additional information is contained in the original extended abstract.

Plaut, J. J.↗
NASA NTRS2001

Determining Biosignatures by Complexity Analysis in Antarctic Cryptoendolithic Communities

One of the most difficult problems of life detection is that of identifying biosignatures across a wide range of scales using multiple co-registered probes. The technique should be of equal utility across a wide range of search spaces from remote sensors probing volumes of space or planetary surfaces, visual eye or camera searches across the surface of a rock in Antarctica, low resolution microscopic scanning of a rock or a space craft in situ, or high resolution electron microscope and computerized tomography scanning of geobiological samples. We describe here an approach to this problem which derives in large part from past work done in the area of astrophysics - namely the analysis of complexity in galactic signals by data compression methods. This approach is a radically new one for geobiology and astrobiology, and allows us to assess the complexity (and thus potential biogenicity) of an object being examined. This is done by considering the information within pixels of an image (regardless the sensor used to gather the information) as an energetic system capable of description in terms of classical thermodynamics. The image data space is searched by an algorithm that judges complexity via data compression (e.g., the more compressible it is, the less complex, and vice versa) and maximum entropy as originally outlined by Shannon. At present we are implementing methods to utilize images from multiple sensors gathering different kinds of information (e.g., visible gray-scale data, color analyses, UV fluorescence, chemical information, etc). We present here preliminary data from deep UV fluorescence and ESEM (Environmental Scanning Electron Microscope) images from a layered cryptoendolithic community of an Antarctic rock.

Storrie-Lombardi, M. C.↗
NASA NTRS2004

Decelerating Flows in the TeV Blazars

TeV emission from a class of BL Lacertae (BL) objects is commonly modeled as radiation from relativistically moving homogeneous plasma blobs. In the context of these models, the blob Lorentz factors needed to reproduce the (corrected for absorption by the IR background) TeV emission are large ($\delta \gtrsim 50$) are required to reproduce via Synchrotron-Self Compton (SSC) the observed TeV emission. The main reason for this is that stronger beaming eases the problem of the lack of $\sim$ IR-UV synchrotron seed photons needed to produce the de-absorbed $\sim$ few TeV peak of the spectral energy distribution (SED). However, such high Doppler factors are in strong disagreement with the unified scheme, according to which BLs are FR I radio galaxies with their jets closely aligned to the line of sight. Here, motivated by the detection of sub-luminal velocities in the sub-pc scale jets of the best studied TeV blazars, MKN 421 and MKN 501. we examine the possibility that the relativistic flow in the TeV BLs is longitudinally decelerating. In this case, the problem of the missing seed photons is solved due to Upstream Compton (UC) scattering, a process in which the upstream energetic electrons from the fast base of the flow 'see' the synchrotron seed photons produced in the slow part of the flow relativistically beamed. Modest Lorentz factors ($\Gamma kim 15s). decelerating down to values compatible with the recent radio interferometric observations, reproduce the $\sim$ few TeV peak energy of these sources. Furthermore, such decelerating flows are shown to be in agreement with the BL - FR I unification.

Kazanas, Demosthenes↗
NASA NTRS2005

Decelerating Flows in TeV Blazars: A Resolution to the BL Lac -- FR I Unification Problem

TeV emission from BL Lacertae (BL) objects i s commonly modeled as Synchrotron-Self Compton (SSC) radiation from relativistically moving homogeneous plasma blobs. In the context of these models, the blob Lorentz factors needed to reproduce the corrected for absorption by the diffuse IR background (DIRB) TeV emission are large ($\delta \gtrsim 50$). The main reason for this is that stronger beaming eases the problem of the lack of $\sim$ IR-UV synchrotron seed photons needed to produce the de-absorbed $\sim $ few TeV peak of the spectral energy distribution (SED). However, such high Doppler factors are in strong disagreement with the unified scheme, according to which BLs are FR I radio galaxies with their jets closely aligned to the line of sight. Here, motivated by the detection of sub-luminal velocities in the sub-pc scale jets of the best studied TeV blazars, MKN 421 and MKN 501, we examine the possibility that the relativistic flows in the TeV BLs decelerate. In this case, the problem of the missing seed photons is solved because of Upstream Compton (UC) scattering, a process in which the upstream energetic electrons from the fast base of the flow 'see' the synchrotron seed photons produced in the slow part of the flow relativistically beamed. Modest Lorentz factors ($\Gamma \sim 15$), decelerating down to values compatible with the recent radio interferometric observations, reproduce the $\sim $ few TeV peak energy of these sources. Furthermore, such decelerating flows are shown to be in agreement with the BL - FR I unification, naturally reproducing the observed BL/FR I broadband luminosity ratios.

Kazanas, Demosthenes↗