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At least 1,549 records · Page 86

Quantitative ultrasonic evaluation of engineering properties in metals, composites, and ceramics

Ultrasonic techniques that have demonstrated potential for material characterization are reviewed. These techniques rely on physical acoustic properties of materials and the interaction of elastic stress waves with morphological factors in the ultrasonic regime. The speed of wave propagation and energy loss by interaction with material microstructure and geometrical factors underlie ultrasonic determination of material properties. Two categories of ultrasonic measurements are discussed: those related to material strengths (e.g., elastic moduli, tensile strength, and fracture toughness) and those related to morphology and material conditions that govern strength and performance (e.g., microstructure, void content, residual stress, fatigue damage). It is shown that large-scale industrial application of ultrasonic NDE will depend on advancement in such areas as theory development, instrumentation, system automation, standardization, and coordination with design.

Vary, A.↗

F region above Kauai - Measurement, model, modification

Results of the Lagopedo II experiment conducted from Kauai, Hawaii to investigate the ionospheric modification that occurs when rocket combustion products are introduced into the O(+)-rich F region are presented. The experiment involved the detonation of a chemical explosion in the F2 peak accompanied by rocket-borne measurements of ion composition and electron content in the vicinity of the explosion. The experimental data is found to be in good agreement with the predictions of a model of the nighttime ion densities in the midlatitude laminar ionosphere, with the exception of N2(+) densities before the explosion. H2O(+) and H3O(+) currents produced by considerable H2O outgassing from the rocket are used to determine a H3O(+)/H2O(+) dissociative recombination rate averaging 1.6 to 1.08, depending on model assumptions. At the time of the explosion, an ionic void 1 km in radius is observed, the boundary of which is characterized by a steep gradient in ionic densities. Evidence of variations in the concentrations of ambient ion species, new reactant species and ionic depletion by sweeping is also obtained.

Johnson, C. Y.↗

Pulsed eddy current testing

Since a large number of the procedures used for inspecting the external tank are concerned with determining flaws in welds, there is a need to develop an inspection technique, which can be automated, to determine flaws in welds and structures with complex geometries. Techniques whereby an eddy current is generated in a metallic material and the changes in the circuit parameters due to material differences are observed, were chosen as one possible approach. Pulsed eddy current and its relationship to multifrequency techniques is discussed as well as some preliminary results obtained from observing pulsed waveforms with apparatus and algorithms currently in use for ultrasonic testing of welds. It can be shown the pulsed eddy current techniques can provide similar results, can eliminate some of the noncritical parameters affecting the eddy current signals, and can facilitate in the detection of critical parameter such as flaws, subsurface voids, and corrosion.

Workman, G. L.↗

Coal thickness guage using RRAS techniques, parts 2 and 3

Electron magnetic resonance was investigated as a sensing technique for use in measuring the thickness of the layer of coal overlying the rock substrate. The goal is development of a thickness gauge which will be usable for control of mining machinery to maintain the coal thickness within selected bounds. A sensor must be noncontracting, have a measurement range of 6 inches or more, and an accuracy of 1/2 inch or better. The sensor should be insensitive to variations in spacing between the sensor and the surface, the response speed should be adequate to permit use on continuous mining equipment, and the device should be rugged and otherwise suited for operation under conditions of high vibration, moisture, and dust. Finally, the sensor measurement must not be adversely affected by the natural effects occurring in coal such as impurities, voids, cracks, layering, high moisture level, and other conditions that are likely to be encountered.

King, J. D.↗

Evaluation of NESS soundings used in the FGGE special effort

A special effort to produce high quality edited and enhanced global data sets is being conducted for the two special observing periods of the first GARP global experiment. More than 60 cases were selected for enhancement on the basis of meteorological interest. These cases include situations of blocking, cut off low development, cyclogenesis, and tropical circulations. The sounding data enhancement process consists of supplementing the operational satellite sounding data set with higher resolution sounding in meteorologically active regions and with new soundings where data voids or soundings of questionable quality exist. After the enhancement process is completed, a final editing and quality assessment of the enhanced data are performed. The data is archived for further analyses. Subjective evaluation of the effects of sounding data enhancement indicate that: (1) enhanced and operational IR retrievals are similar in most situations; (2) large improvements in 1000 to 300 mb thickness and mandatory level temperature and intensification of atmospheric thermal gradients occasionally occur; (3) interactive processing can fill in major gaps in the TIROS-N coverage; and (4) assimilation of special effort soundings can result in major modifications to large scale analyses and prognoses.

Atlas, R.↗

Tackifier for addition polyimides containing monoethylphthalate

An improvement of addition polyimides wherein an essentially solventless, high viscosity laminating resin is synthesized from low cost liquid monomers is disclosed. The improved process takes advantage of a reactive, liquid plasticizer such as monoethylphthalate (MEP) which is used in lieu of an alcohol solvent, and helps solve a major problem of maintaining good prepreg tack and drape, or the ability of the prepreg to adhere to adjacent plies and conform to a desired shape during the layup process. This improvement results in both longer life of the polymer prepreg and the processing of low void laminate and appears to be applicable to all addition polyimide systems.

St.clair, T. L.↗

Bodies in flowing plasmas - Laboratory studies

A brief review of early rudimentary laboratory studies of bodies in flowing, rarefied plasmas is presented (e.g., Birkeland, 1908), along with a discussion of more recent parametric studies conducted in steady plasma wind tunnels, which includes the study by Hall et al. (1964), in which a strong ion density enhancement in the center of the ion void created downstream from the body was observed. Good agreement was found between the experimental results and theoretical calculations which omit ion thermal motion. Examples in which in situ data on the interaction between satellites and the ionospheric plasma have been elucidated by the laboratory results are presented, and include evidence for a midwake axial ion peak, and ion current density in the near-wake region. The application of the ionospheric laboratory to basic space plasma physics is discussed, and its application to some types of solar system plasma phenomena is illustrated.

Stone, N. H.↗

Screening of high temperature adhesives for large area bonding

High temperature-resistant adhesive systems were screened for processability, mechanical and physical properties, operational capability at 589 K (600 F), and the ability to produce large area bonds of high quality in fabricating Space Shuttle components. The adhesives consisted primarily of polyimide systems, including FM34B-18, NR-150B2 (DuPont), PMR-15, LARC-13, LARC-160, Thermid 600, and AI-1130L (AMOCA). The processing studies included preparation of polyimide resins, fabrication of film adhesives, development of lay-up and cure procedures, fabrication of honeycomb sandwich panels, and fabrication of mid-plane bonded panels in joints up to 30.5 cm (12 in.) wide. The screening program included tests for tack and drape properties, reticulation and filleting characteristics, ability to produce void-free or low porosity bonds in mid-plane bonded panels, out-time stability, lap shear strength, climbing drum peel strength, and glass transition temperature (Tg). This paper describes the processing methods developed and the test results.

Stenersen, A. A.↗

A multi-purpose thermoplastic polyimide

A linear thermoplastic polyimide, LARC-TPI, has been characterized and developed for a variety of high-temperature applications. In its fully imidized form, this new material can be used as an adhesive for bonding metals such as titanium, aluminum, copper, brass, and stainless steel. LARC-TPI is being evaluated as a thermoplastic for bonding large pieces of polyimide film to produce flexible, 100% void-free laminates for flexible circuit applications. The further development of LARC-TPI as a potential molding powder, composite matrix resin, high-temperature film and fiber will also be discussed.

Saint Clair, A. K.↗

Preliminary results on the development of vacuum brazed joints for cryogenic wind tunnel aerofoil models

The results of initial experiments show that high-strength void-free bonds can be formed by vacuum brazing of stainless steels using copper and nickel-based filler metals. In Nitronic 40, brazed joints have been formed with strengths in excess of the yield strength of the parent metal, and even at liquid nitrogen temperatures the excellent mechanical properties of the parent metal are only slightly degraded. The poor toughness of 15-5 P.H. stainless steel at cryogenic temperatures is lowered even further by the presence of the brazed bonds investigated. It is highly unlikely that the technique would be used for any critical areas of aerofoil models intended for low-temperature service. Nevertheless, the potential advantages of this simplified method of construction still have attractions for use at ambient temperatures.

Wigley, D. A.↗

Spine Immobilizer for Accident Victims

Proposed conformal bladder filled with tiny spheres called "microballoons," enables spine of accident victim to be rapidly immobilized and restrained and permit victim to be safely removed from accident scene in extremely short time after help arrives. Microballoons expand to form rigid mass when pressure within bladder is less than ambient. Bladder strapped to victim is also strapped to rescue chair. Void between bladder and chair is filled with cloth wedges.

Vykukal, H. C.↗

Laminating Polyimide Films

Thermoplastic polyimide adhesive is used to bond polyimide sheets into flexible laminates. Films are first primed with polyimide adhesive, then bonded together under heat and pressure. Adhesive is cast on separate surface, then sandwiched between polyimide and/or metal films for final assembly. Objectives of process are to improve bonding of high-temperature polyimide film, prepare flexible, large-area, void-free laminates from polyimide film, and laminate polyimide film not only to itself but to metal surfaces.

St. Clair, A. K.↗

Solventless Fabrication of Reinforced Composites

Heat and pressure melt thermoplastic fibers, causing them to flow into voids around graphite reinforcement. On cooling, fiber bundle has been transformed into structural composite. Required temperature and pressure depend on properties of particular thermoplastic used.

Baucom, R. M.↗

Glass shell manufacturing in space

Highly-uniform, hollow glass spheres (shells), which are used for inertial confinement fusion targets, were formed from metal-organic gel powder feedstock in a vertical furnace. As a result of the rapid pyrolysis caused by the furnace, the gel is transformed to a shell in five distinct stages: (a) surface closure of the porous gel; (b) generation of a closed-cell foam structure in the gel; (c) spheridization of the gel and further expansion of the foam; (d) coalescence of the closed-cell foam to a single-void shell; and (e) fining of the glass shell. The heat transfer from the furnace to the falling gel particle was modeled to determine the effective heating rate of the gel. The model predicts the temperature history for a particle as a function of mass, dimensions, specific heat, and absorptance as well as furnace temperature profile and thermal conductivity of the furnace gas. A model was developed that predicts the gravity-induced degradation of shell concentricity in falling molten shells as a function of shell characteristics and time.

Downs, R. L.↗

Design, analysis, and test verification of advanced encapsulation systems

Thermal, optical, structural, and electrical isolation analyses are decribed. Major factors in the design of terrestrial photovoltaic modules are discussed. Mechanical defects in the different layers of an encapsulation system, it was found, would strongly influence the minimum pottant thickness required for electrical isolation. Structural, optical, and electrical properties, a literature survey indicated, are hevily influenced by the presence of moisture. These items, identified as technology voids, are discussed. Analyses were based upon a 1.2 meter square module using 10.2 cm (4-inch) square cells placed 1.3 mm apart as shown in Figure 2-2. Sizing of the structural support member of a module was determined for a uniform, normal pressure load of 50 psf, corresponding to the pressure difference generated between the front and back surface of a module by a 100 mph wind. Thermal and optical calculations were performed for a wind velocity of 1 meter/sec parallel to the ground and for module tilt (relative to the local horizontal) of 37 deg. Placement of a module in a typical array field is illustrated.

Garcia, A.↗

Thermal degradation of the tensile properties of undirectionally reinforced FP-AI203/EZ 33 magnesium composites

The effects of isothermal and cyclic exposure on the room temperature axial and transverse tensile strength and dynamic flexural modulus of 35 volume percent and 55 volume percent FP-Al2O3/EZ 33 magnesium composites were studied. The composite specimens were continuously heated in a sand bath maintained at 350 C for up to 150 hours or thermally cycled between 50 and 250 C or 50 and 350 C for up to 3000 cycles. Each thermal cycle lasted for a total of six minutes with a hold time of two minutes at the maximum temperature. Results indicate to significant loss in the room temperature axial tensile strength and dynamic flexural modulus of composites thermally cycled between 50 and 250 C or of composites isothermally heated at 350 C for up to 150 hours from the strength and modulus data for the untreated, as fabricated composites. In contrast, thermal cycling between 50 and 350 C caused considerable loss in both room temperature strength and modulus. Fractographic analysis and measurement of composite transverse strength and matrix hardness of thermally cycled and isothermally heated composites indicated matrix softening and fiber/matrix debonding due to void growth at the interface and matrix cracking as the likely causes of the strength and modulus loss behavior.

Bhatt, R. T.↗

Effect of aluminum phosphate additions on composition of three-component plasma-sprayed solid lubricant

Image analysis (IA) and electron microprobe X-ray analysis (EMXA) were used to characterize a plasma-sprayed, self-lubricating coating, NASA LUBE PS106, specified by weight percent as 35NiCr-35Ag-30CaF2. To minimize segregation of the powder mixture during the plasma-spraying procedure, monoaluminum phosphate was added to form agglomerate particles. Three concentrations of AlPO4 were added to the mixtures: 1.25, 2.5, and 6.25 percent by weight. Analysis showed that 1.25 wt% AlPO4 yielded a CaF2 deficiency, 2.5 wt% kept the coating closest to specification, and 6.25 wt% yielded excess CaF2 as well as more impurities and voids and a deficiency in silver. Photomicrographs and X-ray maps are presented. The methods of IA and EMXA complement each other, and the reasonable agreement in the results increases the confidence in determining the coating composition.

Jacobson, T. P.↗

An Assessment of Alternate Thermal Protection Systems for the Space Shuttle Orbiter: Executive Summary - Volume 1

Alternate thermal protection system (TPS) concepts to the Space Shuttle Orbiter were assessed. Metallic, ablator, and carbon-carbon concepts which are the result of some previous design, manufacturing and testing effort were considered. Emphasis was placed on improved TPS durability, which could potentially reduce life cycle costs and improve Orbiter operational characteristics. Integrated concept/orbiter point designs were generated and analyzed on the basis of Shuttle design environments and criteria. A merit function evaluation methodology based on mission impact, life cycle costs, and risk was developed to compare the candidate concepts and to identify the best alternate. Voids and deficiencies in the technology were identified, along with recommended activities to overcome them. Finally, programmatic plans, including ROM costs and schedules, were developed for all activities required to bring the selected alternate system up to operational readiness.

Hays, D.↗