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At least 1,531 records · Page 85
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Machine-learning-based automatic small-angle measurement between planar surfaces in interferometer images: A 2D multilayer Laue lenses case

Here, we report a new machine-learning-based approach to automatically measure the small angle between multiple planar surfaces characterized by white light interferometers. By applying an unsupervised clustering algorithm, DBSCAN (Density-Based Spatial Clustering of Applications with Noise), the multiple surfaces in an interferometer image are automatically identified as distinct surfaces. The angles between every two surfaces are then calculated through the surface fitting. This method can be applied to multiple surfaces regardless of their shapes and locations and significantly simplifies the angle measurement procedure. Using the developed method, we have demonstrated a quick and precise angle measurement for the alignment of 2D Multilayer Laue Lenses (MLLs) for the development of high-resolution x-ray microscopy. This automatic, accurate, and robust small-angle measurement method is compatible with widely used white light interferometers and can be further applied to other metrology applications of interferometer results.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Field emission microscopy of carbon nanotube fibers: Evaluating and interpreting spatial emission

In this work, the authors quantify field emission properties of cathodes made from carbon nanotube (CNT) fibers. The cathodes were arranged in different configurations to determine the effect of cathode geometry on the emission properties. Various geometries were investigated including (1) flat cut fiber tip, (2) folded fiber, (3) looped fiber, and (4) fibers wound around a cylinder. The authors employ a custom field emission microscope to quantify I-V characteristics in combination with laterally resolved field-dependent electron emission area. Additionally, they look at the very early emission stages, first when a CNT fiber is turned on for the first time, which is then followed by multiple ramp-up/down runs. Upon the first turn on, all fibers demonstrated limited and discrete emission area. During ramping runs, all CNT fibers underwent multiple (minor and/or major) breakdowns, which improved emission properties in that turn-on field decreased and field enhancement factor and emission area both increased. It is proposed that breakdowns are responsible for removing initially undesirable emission sites caused by stray fibers higher than average. This initial breakdown process gives way to a larger emission area that is created when the CNT fiber subcomponents unfold and align with the electric field. Overall, the authors' results form the basis for careful evaluation of CNT fiber cathodes for dc or low frequency pulsed power systems in which large uniform area emission is required or for narrow beam high frequency applications in which high brightness is a must.

Image processing↗
DOE OSTI2021

Assembly of Close–Packed Ferroelectric Polymer Nanowires via Interface–Epitaxy with ReS 2

The flexible, transparent, and low-weight nature of ferroelectric polymers makes them promising for wearable electronic and optical applications. To reach the full potential of the polarization-enabled device functionalities, large-scale fabrication of polymer thin films with well-controlled polar directions is called for, which remains a central challenge. The widely exploited Langmuir–Blodgett, spin-coating, and electrospinning methods only yield polymorphous or polycrystalline films, where the net polarization is compromised. Here, an easily scalable approach is reported to achieve poly(vinylidene fluoride-trifluoroethylene) P(VDF-TrFE) thin films composed of close-packed crystalline nanowires via interface-epitaxy with 1T'-ReS 2 . Upon controlled thermal treatment, uniform P(VDF-TrFE) films restructure into about 10 and 35 nm-wide (010)-oriented nanowires that are crystallographically aligned with the underlying ReS 2 , as revealed by high-resolution transmission electron microscopy. Piezoresponse force microscopy studies confirm the out-of-plane polar axis of the nanowire films and reveal coercive voltages as low as 0.1 V. Reversing the polarization can induce a conductance switching ratio of >10 8 in bilayer ReS 2 , over six orders of magnitude higher than that achieved by an untreated polymer gate. Lastly, this study points to a cost-effective route to large-scale processing of high-performance ferroelectric polymer thin films for flexible energy-efficient nanoelectronics.

crystalline nanowires↗
DOE OSTI2020

High Thermoelectric Performance and Defect Energetics of Multipocketed Full Heusler Compounds

We report a first-principles density-functional study of electron-phonon interactions in and thermoelectric transport properties of the full Heusler compounds Sr 2 BiAu and Sr 2 SbAu. Our results show that ultrahigh intrinsic bulk thermoelectric performance across a wide range of temperatures is physically possible and point to the presence of multiply degenerate and highly dispersive carrier pockets as the key factor for achieving this. Sr 2 BiAu, which features ten energy-aligned low-effective-mass pockets (six along Γ-X and four at L), is predicted to deliver n-type zT=0.4-4.9 at T=100-700 K. Comparison with the previously investigated compound Ba 2 BiAu shows that the additional L pockets in Sr 2 BiAu significantly increase its low-temperature power factor to a maximum value of 12 mW m -1 K -2 near T=300 K. However, at high temperatures the power factor of Sr 2 BiAu drops below that of Ba 2 BiAu because the L states are heavier and subject to strong scattering by phonon deformation, as opposed to the lighter Γ-X states, which are limited by polar-optical scattering. Sr2SbAu is predicted to deliver a lower n-type zT=3.4 at T=750 K due to appreciable misalignment between the L and Γ-X carrier pockets, generally heavier scattering, and a slightly higher lattice thermal conductivity. Soft acoustic modes, which are responsible for the low lattice thermal conductivity, also increase the vibrational entropy and high-temperature stability of these Heusler compounds, suggesting that their experimental synthesis may be feasible. The dominant intrinsic defects are found to be Au vacancies, which drive the Fermi level towards the conduction band and work in favor of n-doping.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1990

Cloud atlas for the FIRE Cirrus Intensive Field Observation (IFO)

An Intensive Field Observation (IFO) of cirrus clouds was conducted over the mid-western U.S. during the period October 13 to November 2, 1986. This activity, part of the First ISCCP Regional Experiment (FIRE), included measurements made from specially deployed instruments on the ground, balloons, and aircraft as well as observations from existing operational and experimental satellites. One of the sets of satellite observations was the radiance measurements made with the 5-channel AVHRR radiometer on the NOAA 9 polar orbiting meteorological satellite. The ground resolution of the measurements at nadir is approx. 1 km. It is these measurements, made once each day at approximately 2:30 p.m. local time, that were used in determining the present cloud atlas. The area covered by the atlas is slightly larger than the area specified for the IFO, in order to be in alignment with the grid that will be used in a forthcoming atlas for the larger, ETO region. The atlas contains four pages of information for each satellite pass. The 1st page of each group shows the distribution of measured radiances in channel 1 (normalized to the incoming solar flux multiplied by the cosine of the solar zenith angle) and in channel 4 for the area as a whole and for each analysis box. The 2nd page shows the images in: channels 1 and 2, channel 3R; and channel 4. The 3rd page shows the retrieved parameters in graphical form for the region as a whole and for each analysis box, where cloud fraction appears as a contour plot with respect to optical thickness and cloudtop temperature. The 4th page provides a statistical summary of the retrieved parameters in numerical form for each analysis box.

Arking, Albert↗
NASA NTRS1993

Detection of Other Planetary Systems Using Photometry

Detection of extrasolar short-period planets, particularly if they are in the liquid-water zone, would be one of the most exciting discoveries of our lifetime. A well-planned space mission has the capability of making this discovery using the photometric method. An Earth-sized planet transiting a Sun-like star will cause a decrease in the apparent luminosity of the star by one part in 10,000 with a duration of about 12 hours and a period of about one year. Given a random orientation of orbital plane alignments with the line-of-sight to a star, and assuming our solar system to be typical, one would expect 1 percent of the stars monitored to exhibit planetary transits. A null result would also be significant and indicate that Earth-sized planets are rare. For the mission to be successful one needs a sensor system that can simultaneously monitor many thousands of stars with a photometric precision of one part in 30,000 per hour of integration. Confirmation of a detection will involve detection of a second transit that will yield a period and predict the time for a third and subsequent transits. The technology issues that need to be addressed are twofold: one is for an appropriate optical design; the other is for a detector system with the necessary photometric precision. Two candidates for the detector system are silicon diodes and CCD's.

Koch, D.↗
DOE OSTI2024

Flashback Studies of High-Hydrogen Flames using High-Speed OH Planar Laser-Induced Fluorescence

Flame flashback is a crucial challenge during the application of high-hydrogen fuels for the development of next-generation lean premixed combustors. The fundamentals of stable flame configuration, flashback phenomena, and spatiotemporal information of flame dynamics in a premixed, swirl-stabilized burner are investigated experimentally at atmospheric pressure conditions using high-repetition-rate nanosecond (ns)-duration hydroxyl radical planar laser-induced fluorescence (OH-PLIF) measurements. The inlet conditions are varied systematically with respect to equivalence ratio (ϕ), hydrogen percentage in a hydrogen-methane mixture (50%–90%) and pre-mixer velocities and the experiments are performed on the burner modified to provide optical access to the premixing section. Signal interferences such as saturation effects, background chemiluminescence, and laser non-uniformity issues were minimized or corrected during data acquisition and subsequent data processing steps. A stable flame characterization was performed at 20 kHz-repetition-rate for varied pre-mixer velocities, hydrogen content and ϕ in the reactant mixture and lift-off length (L) investigation showed dependence on each of these parameters. Flame dynamics such as flame flashback events, local ignition, local extinction, flame curvature as well as the main reaction zone of the combustion mechanism are well characterized. Flashback ϕ showed an expected linearly increasing trend with increasing pre-mixer velocity and decreasing hydrogen content and the conclusions drawn aligned well with detailed L investigation. Such spatially and temporally resolved kHz-rate OH-PLIF is a promising technique to observe rapidly occurring flashback dynamics and can further validate turbulence-chemistry interaction models of swirling flames.

Parajuli, Pradeep↗
DOE OSTI2023

Recycling the Energy of Indoor Light: Highly Efficient Organic Photovoltaics via a Ternary Strategy

A ternary approach in organic photovoltaics (OPV) is simple and reliable to effectively tune the optical, electrical and morphological properties of the photoactive layer for high efficiency as well as long-term stability under 1 sun. However, there have been few papers reporting spectra and weak illumination compared to outdoor light. In this study, by using two compatible 16 structures, we demonstrate a simultaneous modulation of light absorption and molecular donor polymers (PM7 and PM7 D1) with slightly-different band gaps and similar chemical packing under ambient conditions, which resulted in efficient indoor OPVs exhibiting power conversion efficiency (PCE) over 20% under 1000 lux of warm white light-emitting diode (2900 K). From morphological analysis, we infer that PM7 serves to seed nucleation of PM7 D1 in the ternary blend, templating its crystallization and alignment along the PM7 backbone. Such templating effect leads to increased domain spacing and relative degree of crystallinity (rDoC) compared to those of each binary system. We further show that higher rDoC helps suppress both bimolecular and trap-assisted recombination of photogenerated charges in the ternary devices. As a result, the complementary absorption and synergistic molecular assembly of the two donor polymers enhance the short-circuit current density as to increase the average PCEs from 9.6 to 10.3% under 1 sun and from 18.7 to 20.0% under 1000 lux. We envision that our strategy of incorporating both a planar and a flexible donor polymer with similar chemical structures can be generally applicable to attain a high performance ternary OPV under both 1 sun and indoor light.

14 SOLAR ENERGY↗
NASA NTRS1973

Panoramic attitude sensor for Radio Astronomy Explorer B

An instrument system to acquire attitude determination data for the RAE-B spacecraft was designed and built. The system consists of an electronics module and two optical scanner heads. Each scanner head has an optical scanner with a field of view of 0.7 degrees diameter which scans the sky and measures the position of the moon, earth and sun relative to the spacecraft. This scanning is accomplished in either of two modes. When the spacecraft is spinning, the scanner operates in spherical mode, with the spacecraft spin providing the slow sweep of lattitude to scan the entire sky. After the spacecraft is placed in lunar orbit and despun, the scanner will operate in planar mode, advancing at a rate of 5.12 seconds per revolution in a fixed plane parallel to the spacecraft Z axis. This scan will cross and measure the moon horizons with every revolution. Each scanner head also has a sun slit which is aligned parallel to the spin axis of the spacecraft and which provides a sun pulse each revolution of the spacecraft. The electronics module provides the command and control, data processing and housekeeping functions.

Thomsen, R.↗
NASA NTRS1995

Flow-aligned jets in the magnetospheric cusp: Results from the Geospace Environment Modeling Pilot program

The extended flight of the Airborne Ionospheric Observatory during the Geospace Environment Modeling (GEM) Pilot program on January 16, 1990, allowed continuous all-sky monitoring of the two-dimensional ionospheric footprint of the northward interplanetary magnetic field (IMF) cusp in several wavelengths. Especially important in determining the locus of magnetosheath electron precipitation was the 630.0-nm red line emission. The most striking morphological change in the images was the transient appearance of zonally elongated regions of enhanced 630.0-nm emission which resembled 'rays' emanating from the centroid of the precipitation. The appearance of these rays was strongly correlated with the Y component of the IMF: when the magnitude of B(sub y) was large compared to B(sub z), the rays appeared; otherwise, the distribution was relatively unstructured. Late in the flight the field of view of the imager included the field of view of flow measurements from the European incoherent scatter radar (EISCAT). The rays visible in 630.0-nm emission exactly aligned with the position of strong flow jets observed by EISCAT. We attribute this correspondence to the requirement of quasi-neutrality; namely, the soft electrons have their largest precipitating fluxes where the bulk of the ions precipitate. The ions, in regions of strong convective flow, are spread out farther along the flow path than in regions of weaker flow. The occurrence and direction of these flow bursts are controlled by the IMF in a manner consistent with newly opened flux tubes; i.e., when absolute value of B(sub y) greater than absolute value of B(sub z), tension in the reconnected field lines produce east-west flow regions downstream of the ionospheric projection of the x line. We interpret the optical rays (flow bursts), which typically last between 5 and 15 min, as evidence of periods of enhanced dayside (or lobe) reconnection when absolute value of B(sub y) greater than absolute value of B(sub z). The length of the reconnection pulse is difficult to determine, however, since strong zonal flows would be expected to persist until the tension force in the field line has decayed, even if the duration of the enhanced reconnection was relatively short.

Weiss, L. A.↗
NASA NTRSDate not supplied

Model Validation of Phase-Induced Amplitude Apodization Complex Mask Coronagraph for LUVOIR-A in Vacuum

The Phase-Induced Amplitude Apodization Complex Mask Coronagraph (PIAACMC) is a coronagraph architecture for the next generation of large space telescopes optimized for habitable exoplanet imaging that can achieve attractive theoretical performance with high throughput at small inner working angles (IWA). PIAACMC designs are compatible with large, on-axis, segmented apertures such as the Large UV / Optical/ Infrared A (LUVOIR-A) concept currently being considered by the decadal survey review which would greatly enhance the possibility to achieve statistically significant scientific yields and signal quality for direct imaging exoplanet surveys. PIAACMC has been recently implemented for LUVOIR-A and is currently being tested in vacuum at JPL’s High-Contrast Imaging Testbed (HCIT). In this work, we review the theoretical performance of the PIAACMC instrument designed to meet a 1e-9 raw contrast goal in 10% broadband light in a region from 2-8 L/D both before and after the wavefront control loop. We use empirical measurements from the vacuum testbed to verify the instrument model and its performance including line-of-sight errors, instrument alignment, and fabricated components. In particular, the model verification includes measured sags of the manufactured PIAA mirrors by NuTek. The CMC mask was manufactured at JPL’s Microdevices Laboratory and we include surface profile characterization measurement. We assess the impact on performance of the different manufacturing and alignment errors.

High-Contrast Imaging↗
DOE OSTI2022

Reflectance of rhenium as a function of pressure in a diamond anvil cell

We have measured the reflectance of rhenium in the visible region to pressures up to 100 GPa in a diamond anvil cell (DAC). By photographing the reflecting surface, we visually show that there are challenges to obtaining accurate values in a DAC for several reasons, including cupping of the diamonds and roughening of the surface with the increase in pressure. We propose some useful procedures, such as careful alignment of the incident light and using thin gaskets to minimize cupping of the diamonds as well as measurement in the central region of the diamond culet. We also show that knowledge of the reflectance of rhenium can overcome the problem of absorption of light by diamonds when studying the reflectance of materials at high pressure in a DAC.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2024

In situ estimation of ice crystal properties at the South Pole using LED calibration data from the IceCube Neutrino Observatory

The IceCube Neutrino Observatory instruments about 1 km 3 of deep, glacial ice at the geographic South Pole. It uses 5160 photomultipliers to detect Cherenkov light emitted by charged relativistic particles. An unexpected light propagation effect observed by the experiment is an anisotropic attenuation, which is aligned with the local flow direction of the ice. We examine birefringent light propagation through the polycrystalline ice microstructure as a possible explanation for this effect. The predictions of a first-principles model developed for this purpose, in particular curved light trajectories resulting from asymmetric diffusion, provide a qualitatively good match to the main features of the data. This in turn allows us to deduce ice crystal properties. Since the wavelength of the detected light is short compared to the crystal size, these crystal properties include not only the crystal orientation fabric, but also the average crystal size and shape, as a function of depth. By adding small empirical corrections to this first-principles model, a quantitatively accurate description of the optical properties of the IceCube glacial ice is obtained. In this paper, we present the experimental signature of ice optical anisotropy observed in IceCube light-emitting diode (LED) calibration data, the theory and parameterization of the birefringence effect, the fitting procedures of these parameterizations to experimental data, and the inferred crystal properties.

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS2002

Correlations among the Optical Properties of Cirrus-Cloud Particles: Microphysical Interpretation

Cirrus measurements obtained with a ground-based polarization Raman lidar at 67.9 deg N in January 1997 reveal a strong positive correlation between the particle optical properties, specifically depolarization ratio delta(sub par) and extinction- to-backscatter (lidar) ratio S, for delta(sub par) less than approximately 40%, and an anti-correlation for delta(sub par) greater than approximately 40%. Over the length of the measurements the particle properties vary systematically. Initially, delta (sub par) approximately equals 60% and S approximately equals 10sr are observed. Then, with decreasing delta(sub par), S first increases to approximately 27sr (delta(sub par) approximately equals 40%) before decreasing to values around 10sr again (delta(sub par) approximately equals 20%). The analysis of lidar humidity and radiosonde temperature data shows that the measured optical properties stem from scattering by dry solid ice particles, while scattering by supercooled droplets, or by wetted or subliming ice particles can be excluded. For the microphysical interpretation of the lidar measurements, ray-tracing computations of particle scattering properties have been used. The comparison with the theoretical data suggests that the observed cirrus data can be interpreted in terms of size, shape, and, under the assumption that the lidar measurements of consecutive cloud segments can be mapped on the temporal development of a single cloud parcel moving along its trajectory, growth of the cirrus particles: Near the cloud top in the early stage of cirrus development, light scattering by nearly isometric particles that have the optical characteristics of hexagonal columns (short, column-like particles) is dominant. Over time the ice particles grow, and as the cloud base height extends to lower altitudes characterized by warmer temperatures they become morphologically diverse. For large S and depolarization values of approximately 40%, the scattering contributions of column- and plate-like particles are roughly the same. In the lower ranges of the cirrus clouds, light scattering is predominantly by plate-like ice particles. This interpretation assumes random orientation of the cirrus particles. Simulations with a simple model suggest, however, that the positive correlation between S and delta(sub par) which is observed for depolarization ratios less than 40% mainly at low cloud altitudes, can be alternatively explained by horizontal alignment of a fraction of the cirrus particle population.

Reichardt, J.↗
DOE OSTI2026

Flame Characterization and Flashback Studies of Hydrogen-Enriched Low-Swirl Flames Using High-Speed OH-PLIF

Here, this paper reports the flashback mechanism observed in hydrogen-enriched flames stabilized in a low-swirl burner (LSB) at atmospheric temperature and pressure. The fundamentals of hydrogen-rich stable flames and spatiotemporal information of flashback phenomena were observed experimentally using a high-repetition-rate nanosecond (ns)-duration hydroxyl planar laser-induced fluorescence (OH-PLIF) diagnostic. Testing was conducted for methane and hydrogen (50–90%H 2 , by mole) blends in an optically accessible LSB premixer with measured swirl numbers varying from 0.43 to 0.49. The flashback propensity showed dependence on liftoff length, which was dependent on premixer velocity (𝑉), hydrogen content (𝑋 H 2 ), and equivalence ratio (𝜙) at constant temperature and pressure. High-speed OH-PLIF images revealed that lifted flames were first observed at low 𝜙/𝑋 H 2 conditions, which were changed to an M-shaped flame attached to the burner rim with an increase in 𝜙/𝑋 H 2 . A further increase in 𝜙/𝑋 H 2 triggered the flame flashback into the premixer. Flame 𝜙 at flashback (𝜙 FB ) showed an expected linearly increasing trend with increasing 𝑉 and decreasing 𝑋 H 2 , and the conclusions drawn aligned well with detailed liftoff length investigations. The 𝜙 FB increased with increasing perforated plate hole diameter and increasing swirler vane angle. The vane angle had little effect on flashback tendency at high premixer velocity.

combustion↗
NASA NTRS1972

Microscopic observations of X-ray and gamma-ray induced decomposition of ammonium perchlorate crystals

The X-ray and gamma-ray induced decomposition of ammonium perchlorate was studied by optical, transmission, and scanning electron microscopy. This material is a commonly used oxidizer in solid propellents which could be employed in deep-space probes, and where they will be subjected to a variety of radiations for as long as ten years. In some respects the radiation-induced damage closely resembles the effects produced by thermal decomposition, but in other respects the results differ markedly. Similar radiation and thermal effects include the following: (1) irregular or ill-defined circular etch pits are formed in both cases; (2) approximately the same size pits are produced; (3) the pit density is similar; (4) the c face is considerably more reactive than the m face; and (5) most importantly, many of the etch pits are aligned in crystallographic directions which are the same for thermal or radiolytic decomposition. Thus, dislocations play an important role in the radiolytic decomposition process.

Herley, P. J.↗
NASA NTRSDate not supplied

Ground to Air Testing of a Fused Optical-Radar Aircraft Detection and Tracking System

Onboard detection and tracking capability are integral to the sensing component in collision avoidance systems needed to safely operate autonomous urban air taxis and small Unmanned Aircraft Systems. Ground-based validation of detection and tracking systems is an important milestone towards the end goal of real-time collision avoidance using onboard sensors and algorithms. In this work, we evaluate three Extended Kalman Filter(EKF)based fusion trackers with radar and vision detection inputs, and compare them with baseline trackers for each sensor type. Performance is assessed using field collected data of ground to air test flights with the sensors co-located on a stable platform with an instrumented multirotor acting as the intruder performing a waypoint pattern at a distance of1.1km to 0.3km to simulate a head-on collision geometry. Fusing an image-based morphological detector with a radar detector using an EKF covered 74% of the ground truth position updates logged by the flight controller on the multirotor within 50 meters after accounting for alignment offsets while covering 15% more ground truth updates relative to radar only. Removing timestamps when the intruder aircraft is occluded by trees and only considering timestamps where the radar has an update, the EKF image-based morphological detector combined with the radar detector covered 90% of the of the ground truth position updates within 50metersand 97% within 100 meters.

Chester V Dolph↗
NASA NTRS1986

Operation of the CCD/Transit Instrument (CTI)

The fully automated imaging survey telescope at Kitt Peak known as the CCD/Transit Instrument (CTI) has no moving parts, and employs two CCDs aligned east-west in the focal plane that are operated in the time delay and integrate mode, at the apparent sidereal rate, in order to produce a strip image of the sky. This image is 8.25-arcmin wide in declination and 8 hr in duration, to yield about 15 sq deg of sky from each night's survey; this, over the course of a year, represents more than 40 sq deg in a continuous strip. The CTI is addressing such astronomical tasks as the determination of the supernova production rate by counting, galactic structure investigations, and the definition of a complete sample of quasars. Attention is given to the CTI's bimetallic, thermally self-compensating structure and three-mirror wide-field optical system.

Mcgraw, J. T.↗