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At least 1,531 records · Page 85

Instrumented nanoindentation and 3D mechanistic modeling of a shale at multiple scales

Nanoindentation tests, spanning various length scales ranging from 200 nanometers to 5 micrometers deep, were performed here on a sample of organic-rich Woodford shale in both the bedding plane normal and bedding plane parallel directions. Focused ion beam milling (FIB), scanning electron microscopy (SEM), and energy dispersive X-ray spectroscopy (EDX) were utilized to characterize the shale at the scale of the nanoindentation testing as being comprised predominantly of clay and other silicate minerals suspended in a mixed organic/clay matrix. The nanoindentation tests reveal the mechanical properties of the relatively homogeneous constituent materials as well as those of the highly heterogeneous composite material. Loads on the order of a few milliNewtons produced shallower indents and demonstrated the elastic-plastic deformation response of the constituent materials, whereas higher loads of as much as a few hundred milliNewtons produced deeper indents revealing the response of the composite matrix. In both cases, significant creep was observed. We use nonlinear finite element modeling utilizing an isotropic critical state theory with creep to capture the indentation response by calibrating plastic material parameters to the laboratory measurements. The simulations offer a means of extracting plastic material parameters from the nanoindentation measurements, and reveal the capabilities as well as limitations of an isotropic model in capturing the response of an inherently anisotropic material.

58 GEOSCIENCES↗

Nonlinear response of unidirectional boron/aluminum

Experimental results obtained for unidirectional boron/aluminum subjected to combined loading using off-axis tension, compression and Iosipescu shear specimens are correlated with a nonlinear micromechanics model. It is illustrated that the nonlinear response in the principal material directions is markedly influenced by the different loading modes and different ratios of the applied stress components. The observed nonlinear response under pure and combined loading is discussed in terms of initial yielding, subsequent hardening, stress-interaction effects and unloading-reloading characteristics. The micromechanics model is based on the concept of a repeating unit cell representative of the composite-at-large and employs the unified theory of Bodner and Partom to model the inelastic response of the matrix. It is shown that the employed micromechanics model is sufficiently general to predict the observed nonlinear response of unidirectional boron/aluminum with good accuracy.

Pindera, M.-J.↗

Transient motion of thick anisotropic plates

Analyses are developed for the response of anisotropic plate strips to a transient load. The load is taken in the form of a line load of normal stress on the surface or within the body of the strip. The characteristic free vibrational modes of the strip are derived and used to derive the secular equation for this case in closed form and to isolate the mathematical conditions for symmetric and antisymmetric wave mode propagation in completely separate terms. The applied loads are expanded in terms of these normal modes and the response of the plate is obtained by superposition of the appropriate components. Material systems of higher symmetry are contained implicitly in the analysis.

Nayfeh, Adnan H.↗

Inlet Flow Distortion and Unsteady Blade Response in a Transonic Axial-Compressor Rotor

This paper describes the unsteady blade surface pressures on the first-stage rotor blades of a two-stage transonic axial flow compressor experiencing inlet flow distortion. This study was conducted to demonstrate the ability of a full annulus unsteady Reynolds-averaged Navier-Stokes numerical technique to predict unsteady pressures on the rotor blades operating in a distorted inflow. A total pressure distortion produced by a variable mesh screen mounted near the inlet was used to excite the unsteady blade loading on the rotor. On-blade pressure transducers were used to measure the unsteady blade surface pressure. These pressures and the resulting transient load on the rotor blades were compared to the numerical prediction. It is important to develop numerical techniques to predict these transient loads to better understand the response of compressor blades to forcing functions. With this enhanced understanding and ability to predict these transient forces, more robust compressors can be developed. In the study, a high definition of the inlet flow distortion was achieved by rotating the distortion screens. In this manner the inlet flow distortion and the distortion at the first stage stator leading edge were measured at approximately every 0.7 degrees. This full annulus high definition of the inlet flow distortion was used as the inlet boundary condition for the numerical technique. The experimental measurements and numerical analyses are highly complementary in this study. Detailed comparisons between the measurements and the numerical analyses indicate that the current numerical procedure calculates the unsteady aerodynamic pressure on the blade surfaces reasonably well. Further, the agreement of the measured and predicted rotor exit flow distortion at the first stage stator leading edge provides verification of the numerical technique.

Rabe, D. C.↗

Nutrition and muscle loss in humans during spaceflight

The protein loss in humans during spaceflight is partly due to a normal adaptive response to a decreased work load on the muscles involved in weight bearing. The process is mediated by changes in prostaglandin release, secondary to the decrease in tension on the affected muscles. On missions, where there is a high level of physical demands on the astronauts, there tends to be an energy deficit, which adds to the muscle protein loss and depletes the body fat reserves. While the adaptive response is a normal part of homeostasis, the additional protein loss from an energy deficit can, in the long run, have a negative effect on health and capability of humans to live and work in space and afterward return to Earth.

NASA Program Biomedical Research and Countermeasur↗

Engineering endosomolytic nanocarriers of diverse morphologies using confined impingement jet mixing

The clinical translation of many biomolecular therapeutics has been hindered by undesirable pharmacokinetic (PK) properties, inadequate membrane permeability, poor endosomal escape and cytosolic delivery, and/or susceptibility to degradation. Overcoming these challenges merits the development of nanoscale drug carriers (nanocarriers) to improve the delivery of therapeutic cargo. Herein, we implement a flash nanoprecipitation (FNP) approach to produce nanocarriers of diverse vesicular morphologies by using various molecular weight PEG-bl-DEAEMA-co-BMA (PEG-DB) polymers. We demonstrated that FNP can produce uniform (PDI < 0.1) particles after 5 impingements, and that by varying the copolymer hydrophilic mass fraction, FNP enables access to a diverse variety of nanoarchitectures including micelles, unilamellar vesicles (polymersomes), and multi-compartment vesicles (MCVs). We synthesized a library of 2 kDa PEG block copolymers, with DEAEMA-co-BMA second block molecular weights of 3, 6, 12, 15, 20, and 30 kDa. All formulations were both pH responsive, endosomolytic, and capable of loading and cytosolically delivering small negatively charged molecules – albeit to different degrees. Using a B16.F10 melanoma model, we showcased the therapeutic potential of a lead FNP formulated PEG-DB nanocarrier, encapsulating the cyclic dinucleotide (CDN) cGAMP to activate the stimulator of interferon genes (STING) pathway in a therapeutically relevant context. Collectively, these data demonstrate that an FNP process can be used to formulate pH-responsive nanocarriers of diverse morphologies using a PEG-DB polymer system. As FNP is an industrially scalable process, these data address the critical translational challenge of producing PEG-DB nanoparticles at scale. Furthermore, the diverse morphologies produced may specialize in the delivery of distinct biomolecular cargos for other therapeutic applications, implicating the therapeutic potential of this platform in an array of disease applications.

36 MATERIALS SCIENCE↗

A test cassette for x-ray-exposure experiments at the National Ignition Facility

We present the design and operation of a test cassette for exposure of samples to radiation environments at the National Ignition Facility. The cassette provides options for square and round samples and exposure areas; the cassette provides for multiple levels of filtration on a single sample, which allows dynamic range in experiments. The samples had normal lines of sight to the x-ray source in order to have uniform x-ray illumination. The incident x-radiation onto the samples was determined by the choice of filter thicknesses and materials. The samples were held at precise locations, accurate to within a few hundred microns, in the target chamber in order to have a known fluence incident. In the cassette, the samples were held in place in such a way that a minimal ''line contact'' allows them to have the maximal mechanical response to the x-ray load. We present postshot images of the debris found on films used for filters, and pre- and postexposure specimens.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

A dissolution-precipitation mechanism is at the origin of concrete creep in moist environments

Long-term creep (i.e., deformation under sustained load) is a significant material response that needs to be accounted for in concrete structural design. However, the nature and origin of concrete creep remain poorly understood and controversial. Here, we propose that concrete creep at relative humidity ≥ 50%, but fixed moisture content (i.e., basic creep), arises from a dissolution-precipitation mechanism, active at nanoscale grain contacts, as has been extensively observed in a geological context, e.g., when rocks are exposed to sustained loads, in liquid-bearing environments. Based on micro-indentation and vertical scanning interferometry data and molecular dynamics simulations carried out on calcium–silicate–hydrate (C–S–H), the major binding phase in concrete, of different compositions, we show that creep rates are correlated with dissolution rates—an observation which suggests a dissolution-precipitation mechanism as being at the origin of concrete creep. C–S–H compositions featuring high resistance to dissolution, and, hence, creep are identified. Analyses of the atomic networks of such C–S–H compositions using topological constraint theory indicate that these compositions present limited relaxation modes on account of their optimally connected (i.e., constrained) atomic networks.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Active control of tiltrotor blade in-plane loads during maneuvers

The origin of one/rev rotor aerodynamic loads which arise in tiltrotor aircraft during airplane-mode high speed pull-up and push-over maneuvers is examined using a coupled rotor/fuselage dynamic simulation. A modified eigenstructure assignment technique is used to design a controller which alleviates the in-plane loads during high pitch rate maneuvers. The controller utilizes rotor cyclic pitch inputs to restructure the aircraft short period and phugoid responses in order to achieve the coupling between pitch rate and rotor flapping responses which minimizes the rotor aerodynamic loading. Realistic time delays in the feedback path are considered during the controller design. Stability robustness in the presence of high frequency modeling errors is ensured through the use of singular value analysis.

Miller, David G.↗

Determination of Radiative Forcing of Saharan Dust using Combined TOMS and ERBE Data

The direct radiative forcing of Saharan dust aerosols has been determined by combining aerosol information derived from Nimbus-7 TOMS with radiation measurements observed at the top of atmosphere (TOA) by NOAA-9 ERBE made during February-July 1985. Cloud parameters and precipitable water derived from the NOAA-9 HIRS2 instrument were used to aid in screening for clouds and water vapor in the analyses. Our results indicate that under "cloud-free" and "dry" conditions there is a good correlation between the ERBE TOA outgoing longwave fluxes and the TOMS aerosol index measurements over both land and ocean in areas under the influence of airborne Saharan dust. The ERBE TOA outgoing shortwave fluxes were also found to correlate well with the dust loading derived from TOMS over ocean. However, the calculated shortwave forcing of Saharan dust aerosols is very weak and noisy over land for the range of solar zenith angle viewed by the NOAA-9 ERBE in 1985. Sensitivity factors of the TOA outgoing fluxes to changes in aerosol index were estimated using a linear regression fit to the ERBE and TOMS measurements. The ratio of the shortwave-to-longwave response to changes in dust loading over the ocean is found to be roughly 2 to 3, but opposite in sign. The monthly averaged "clear-sky" TOA direct forcing of airborne Saharan dust was also calculated by multiplying these sensitivity factors by the TOMS monthly averaged "clear-sky" aerosol index. Both the observational and theoretical analyses indicate that the dust layer height, ambient moisture content as well as the presence of cloud all play an important role in determining the TOA direct radiative forcing due to mineral aerosols.

Hsu, N. Christina↗

Dynamic Behavior of Sand: Annual Report FY 11

Currently, design of earth-penetrating munitions relies heavily on empirical relationships to estimate behavior, making it difficult to design novel munitions or address novel target situations without expensive and time-consuming full-scale testing with relevant system and target characteristics. Enhancing design through numerical studies and modeling could help reduce the extent and duration of full-scale testing if the models have enough fidelity to capture all of the relevant parameters. This can be separated into three distinct problems: that of the penetrator structural and component response, that of the target response, and that of the coupling between the two. This project focuses on enhancing understanding of the target response, specifically granular geomaterials, where the temporal and spatial multi-scale nature of the material controls its response. As part of the overarching goal of developing computational capabilities to predict the performance of conventional earth-penetrating weapons, this project focuses specifically on developing new models and numerical capabilities for modeling sand response in ALE3D. There is general recognition that granular materials behave in a manner that defies conventional continuum approaches which rely on response locality and which degrade in the presence of strong response nonlinearities, localization, and phase gradients. There are many numerical tools available to address parts of the problem. However, to enhance modeling capability, this project is pursuing a bottom-up approach of building constitutive models from higher fidelity, smaller spatial scale simulations (rather than from macro-scale observations of physical behavior as is traditionally employed) that are being augmented to address the unique challenges of mesoscale modeling of dynamically loaded granular materials. Through understanding response and sensitivity at the grain-scale, it is expected that better reduced order representations of response can be formulated at the continuum scale as illustrated in Figure 1 and Figure 2. The final result of this project is to implement such reduced order models in the ALE3D material library for general use.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗

Fracture of Charring Avcoat With Meshfree Material Response-Coupled Fracture Approach

Fracture of thermal protection systems (TPS) is typically unfavorable, but often unavoidable. TPS can fracture during entry, manufacturing or from impact. Many NASA missions use ablative materials for TPS, including the fore-body for Dragonfly (PICA) and Orion for Artemis-I (Avcoat). The material response to thermal and mechanical loads during entry is integral to TPS sizing, design and analysis. The fracture of TPS also depends, and can be caused by, the change of material properties during entry. Simulations that resolve fracture of TPS due to thermo-mechanical forces can identify TPS failure mechanisms and be applied to conditions inaccessible to ground testing. We present simulation work using a mesh-free/Lagrangian approach to solving continuum mechanics, coupled to material response. Two different materials are simulated under different model entry-like boundary conditions. The dynamic crack structure is analyzed and compared across simulations. Crack analyses inform the role of design features, such as entry trajectories and manufacturing-influenced material properties, play in TPS fracture.

Andrew P Santos↗

Constraining the Venus Interior Structure With Future VERITAS Measurements of the Gravitational Atmospheric Loading

The complex dynamics of the Venus atmosphere produces a periodic mass redistribution pattern that creates a time-variable modulation of the gravity field of Venus. This gravity signal depends on the net transport of mass across the globe and on the response of the solid body to the normal loading of its crust imparted by the atmosphere. In this work, we explore the possibility of measuring this phenomenon with VERITAS, a NASA Discovery-class mission. By simulating the gravity science experiment, we explore the possibility of measuring the response of Venus to the atmospheric loading, parametrized by the loading Love numbers ( 𝑘 𝑙 ' ), and assess the dependence of these parameters on fundamental interior structure properties. Using the most recent models of Venus' interior, we compute the Venus Love numbers in a compressible viscoelastic setting and compare them with the predicted uncertainty of the VERITAS measurements. We show that VERITAS will measure 𝑘 2 ' at the 4% level and that this measurement could possibly help to distinguish between different equally plausible interior structure models, especially allowing us to distinguish different rheological laws. We also show that a measurement campaign such as the VERITAS gravity science investigation has the potential of measuring 𝑘 2 ' not only at the loading forcing frequency, but also at the tidal frequency, ultimately providing a way to probe the response of the planet at different forcing periods.

Atmospheric tides↗

Detailed Modeling and Response of Demand Response Enabled Appliances

Proper modeling of end use loads is very important in order to predict their behavior, and how they interact with the power system, including voltage and temperature dependencies, power system and load control functions, and the complex interactions that occur between devices in such an interconnected system. This paper develops multi-state time variant residential appliance models with demand response enabled capabilities in the GridLAB-DTM simulation environment. These models represent not only the baseline instantaneous power demand and energy consumption, but the control systems developed by GE Appliances to enable response to demand response signals and the change in behavior of the appliance in response to the signal. These DR enabled appliances are simulated to estimate their capability to reduce peak demand and energy consumption.

demand response↗

Comprehensive Forced Response Analysis of J2X Turbine Bladed-Discs with 36- Degree Variation in CFD Loading

At NASA/MSFC, Structural Dynamics personnel continue to perform advanced analysis for the turbomachinery in the J2X Rocket Engine, which is under consideration for the new Space Launch System. One of the most challenging analyses in the program is predicting turbine blade structural capability. Resonance was predicted by modal analysis, so comprehensive forced response analyses using high fidelity cyclic symmetric finite element models were initiated as required. Analysis methodologies up to this point have assumed the flow field could be fully described by a sector, so the loading on every blade would be identical as it travelled through it. However, in the J2X the CFD flow field varied over the 360 deg of a revolution because of the flow speeds and tortuous axial path. MSFC therefore developed a complex procedure using Nastran Dmap's and Matlab scripts to apply this circumferentially varying loading onto the cyclically symmetric structural models to produce accurate dynamic stresses for every blade on the disk. This procedure is coupled with static, spin, and thermal loading to produce high cycle fatigue safety factors resulting in much more accurate analytical assessments of the blades.

Elrod, David↗

Nonlinear Analysis of the Space Shuttle Superlightweight LO2 Tank: Bahavior Under Booster Ascent Loads - Part 1

Results of linear bifurcation and nonlinear analyses of the Space Shuttle superlightweight (SLWT) external liquid-oxygen (LO2) tank for an important early booster ascent loading condition are presented. These results for thin-walled linear elastic shells that are subjected to combined mechanical and thermal loads illustrate an important type of response mode that may be encountered in the design of other liquid-fuel launch vehicles. Linear bifurcation analyses are presented that predict several nearly equal eigenvalues that correspond to local buckling modes in the forward ogive section of the LO2 tank. In contrast, the nonlinear response phenomenon is shown to consist of short-wavelength bending deformations in the forward ogive and barrel sections of the LO2 tank that growing amplitude in a stable manner increasing load. Imperfection sensitivity analyses are presented that show that the presence of several nearly equal eigenvalues does not lead to a premature general instability mode for the forward ogive section. For the linear bifurcation and nonlinear analyses, the results show that accurate predictions of the response of the shield generally require a large-scale, high-fidelity finite-element model. Results are also presented that show that the SLWT LO2 tank can support loads in excess of approximately 2.6 times the values of the operational loads considered.

Young, Richard D.↗

On the pore-scale mechanisms leading to brittle and ductile deformation behavior of crystalline rocks

Deformation mechanisms found at the pore scale are responsible for producing large strains in porous rocks. Furthermore, they include cataclastic flow, dislocation creep, dynamic recrystallization, diffusive mass transfer, and grain boundary sliding, among others. Here, we focus on two dominant pore-scale mechanisms resulting from purely mechanical, isothermal loading: crystal plasticity and micro-fracturing. We examine the contributions of each mechanism to the overall behavior at a scale larger than the grains but smaller than the specimen, which is commonly referred to as the mesoscale. Crystal plasticity is assumed to occur as dislocations along the many crystallographic slip planes, whereas micro-fracturing entails slip and frictional sliding on microcracks. It is observed that under combined shear and tensile loading, micro-fracturing generates a softer response compared to crystal plasticity alone, which is attributed to slip weakening where the shear stress drops to a residual level determined by the frictional strength. For compressive loading, however, micro-fracturing produces a stiffer response than crystal plasticity due to the presence of frictional resistance on the slip surface. Behaviors under tensile, compressive, and shear loading invariably show that porosity plays a critical role in the initiation of the deformation mechanisms. Both crystal plasticity and micro-fracturing are observed to initiate at the peripheries of the pores, consistent with results of experimental studies.

58 GEOSCIENCES↗