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At least 1,495 records · Page 83

Quinoxaline polymers and copolymers derived from 1,4-bis(1'-naphthalenyloxalyl)benzene and their graphite composites

Experimental studies were performed with new polyquinoxalines and their graphite composites. Four polymers were synthesized, and then were characterized with respect to their inherent viscosity, elemental chemical analysis, mechanical, and thermodynamic properties. Structural formulas of the polymers and their precursors are given; methods of synthesis are described; and specifically examined was the preparation of polymers from 3,3' diamino-benzidine from 1,4- and 1,3- bis ((1'-napthalenyl) oxalyl) benzene respectively. Also considered was the preparation of polyquinoxalines from poly (p-benzil), and 1,2- aryldiamines.

Port, W. S.↗

Hardwall acoustical characteristics and measurement capabilities of the NASA Lewis 9 x 15 foot low speed wind tunnel

Experimental evaluations of the acoustical characteristics and source sound power and directionality measurement capabilities of the NASA Lewis 9 x 15 foot low speed wind tunnel in the untreated or hardwall configuration were performed. The results indicate that source sound power estimates can be made using only settling chamber sound pressure measurements. The accuracy of these estimates, expressed as one standard deviation, can be improved from + or - 4 db to + or - 1 db if sound pressure measurements in the preparation room and diffuser are also used and source directivity information is utilized. A simple procedure is presented. Acceptably accurate measurements of source direct field acoustic radiation were found to be limited by the test section reverberant characteristics to 3.0 feet for omni-directional and highly directional sources. Wind-on noise measurements in the test section, settling chamber and preparation room were found to depend on the sixth power of tunnel velocity. The levels were compared with various analytic models. Results are presented and discussed.

Rentz, P. E.↗

NASA/ESA CV-990 airborne simulation of Spacelab

The paper describes the joint NASA/ESA extensive Spacelab simulation using the NASA CV-990 airborne laboratory. The scientific payload was selected to conduct studies in upper atmospheric physics and infrared astronomy. Two experiment operators from Europe and two from the U.S. were selected to live aboard the aircraft along with a mission manager for a six-day period and operate the experiments in behalf of the principal scientists. The mission was successful and provided extensive data relevant to Spacelab objectives on overall management of a complex international payload; experiment preparation, testing, and integration; training for proxy operation in space; data handling; multiexperimenter use of common experimenter facilities (telescopes); and schedule requirements to prepare for such a Spacelab mission.

Mulholland, D.↗

Factors affecting the palmitoyl-coenzyme A desaturase of Saccharomyces cerevisiae

The activity and stability of the palmitoyl-coenzyme A (CoA) desaturase complex of Saccharomyces cerevisiae was influenced by several factors. Cells, grown nonaerobically and then incubated with glucose, either in air or under N2, showed a marked increase in desaturase activity. Cycloheximide, added during such incubations, prevented the increase in activity, suggesting de novo synthesis. The stability of the desaturase from cells grown nonaerobically was affected by subsequent treatment of the cells; enzyme from freshly harvested cells, or from cells that were then shaken under nitrogen, readily lost activity upon washing or during density gradient analysis, whereas aerated cells, in the presence or absence of glucose, yielded stable enzyme preparations. The loss of activity in nonaerobic preparations could be reversed by adding soluble supernatant from these homogenates and could be prevented by growing the cells in the presence of palmitoleic acid and ergosterol, but not with several other lipids tested.

Klein, H. P.↗

Properties of splat-quenched 7075 aluminum type alloys

The 7075 alloy belonging to the Al-Zn-Mg-Cu system, prepared by powder metallurgy techniques, was used in a study of alloys prepared from splat-quenched foils consolidated into bar material by hot extrusion. Ni and Fe were included in one alloy specimen, producing a fine dispersion of FeAl3 type particles which added to the strength of the aged alloy but did not coarsen upon heat treatment. Fine oxide films showing up on air-splatted foils induce finely dispersed oxide stringers (if the foils are not hot-worked subsequently) which in turn promote axial cracking (but longitudinal tensile strength is not seriously impaired). Splatting in a protective atmosphere, or thermomechanical processing, is recommended to compensate for this.

Durand, J. P. H. A.↗

Hierarchical resource analysis for land use planning through remote sensing

A hierarchical resource analysis was applied to remote sensing data to provide maps at Planning Levels I and III (Anderson et al., U.S. Geological Survey Circular 671) for Meade County, S. Dak. Level I land use and general soil maps were prepared by visual interpretation of imagery from a false color composite of Landsat MSS bands 4, 5, and 7 and single bands (5 and 7). A modified Level III land use map was prepared for the Black Hills area from RB-57 photography enlarged to a scale of 1:24,000. Level III land use data were used together with computer-generated interpretive soil maps to analyze relationships between developed and developing areas and soil criteria.

Byrnes, B. H.↗

Apollo Soyuz mission planning and operations

The paper describes the Apollo Soyuz project from the points of view of working group organization, mission plan definition, joint operations concept, and mission preparation. The concept for joint operations considered contingency situations as well as nominal operations. Preparations for the joint flight included cooperative tracking tests and combined training of the flight crews and mission control personnel.

Frank, M. P., III↗

Apollo 12 Mission Report

The Apollo 12 mission was the twelfth in a series of flights using Apollo flight hardware and was the second lunar landing. The purpose of the mission was to perform a precise lunar landing and to conduct a specific scientific exploration of a designated landing site in the Ocean of Storms. Since the performance of the entire spacecraft was excellent, this report discusses only the systems performance that significantly differed from that of previous missions. Because they were unique to Apollo 12, the lunar surface experiments, the precision landing operation, and lunar dust contamination are reported in sections 3, 4, and 6, respectively. A complete analysis of all flight data is not possible within the time allowed for preparation of this report. Therefore, report supple­ments will be published for certain Apollo 12 systems analyses, as shown in appendix E. This appendix also lists the current status of all Apollo mission supplements, either published or in preparation. Other supplements will be published as the need is identified. In this report, all actual times prior to earth landing are elapsed time from range zero, established as the integral second before lift-off. Range zero for this mission was 16:22:00 G.m.t., November 14, 1969. Greenwich mean time is used for all times after earth landing as well as for the discussions of the experiments left on the lunar surface. All references to mileage distance are in nautical miles.

Source record↗

Orbiter description document for Jupiter Orbiter Probe 1981/1982 Mission

The Jupiter Orbiter as it is presently understood is documented. Because the Jupiter Orbiter Probe 1981/1982 (JOP 81/82) Project will be severely cost constrained, the Orbiter design and capabilities described herein are not subject to major change or modification as a result of instrument selection. The JOP science payload should conform to this defined capability and the specified interfaces. A description and discussion of any science instrument complement is excluded, except the imaging science subsystem and the radio science capability which are provided by the project as Orbiter facilities. The environmental design requirements and the mission operations description are studied. This document has been prepared specifically for the JOP Announcement of Opportunity proposal preparation package and describes the Jupiter Orbiter in sufficient detail to allow the science community to propose scientific instrumentation consistent with its capabilities and limitations.

Source record↗

Flame retardant polyphosphazenes

Three processes for the preparation of polyphosphazenes were investigated: (1) the reaction of bisphosphines with diazides, (2) the condensation of bisdichlorophosphoranes with diamines; and (3) the treatment of bisphosphines with diamines in the presence of carbon tetrachloride followed by base dehydrohalogenation. All products obtained were of low molecular weight; the degree of polymerization did not exceed twelve repeating units. However, several compositions exhibited good thermal stability. No weight loss was observed up to 390 C when heated in air at 5 C/min. Treatment of bisphosphines with either an excess of a diazide or an excess of a diamine in the presence of carbon tetrachloride resulted in the production of difunctional phosphazenes which were respectively, azido and amino terminated. The reaction of these azido terminated extended monomers with bisphosphines did not produce high molecular weight materials. The bis-aminophosphazene prepared for the first time under this contract was successfully incorporated into a polyimide.

Paciorek, K. L.↗

The NASA Space Processing Program

The program is intended to initiate utilization of spaceflight for economically beneficial activities in all branches of materials science and technology. In view of the prospect they offer for reducing the costs of space operations, the Spacelab and Space Shuttle are expected to become widely used for work on materials early in the 1980's. At first they will be employed for space experiments and for services, such as sample preparation, that support research and development activities on the ground. Orbital manufacturing operations are expected to develop as well when research has prepared an adequate basis for them. During the past year, NASA has initiated a series of rocket flights on which prospective participants in the Shuttle/Spacelab program can perform preliminary experiments. Participation in these flights is open to investigators from all countries, and experiments are being solicited from private sponsors also. NASA is performing concurrent definition studies of Shuttle/Spacelab payloads, and design work on equipment for the first two years of operations is planned to begin early in 1977. The Office of Applications currently plans to fly two space processing payloads on Orbital Flight Test missions in 1980 and two on operational Spacelab missions in 1981.

Bredt, J. H.↗

Electrophoresis for biological production

Preparative electrophoresis may provide a unique method for meeting ever more stringent purity requirements. Prolonged near zero gravity in space may permit the operation of preparative electrophoresis equipment with 100 times greater throughput than is currently available. Some experiments with influenza Virus Antigen, Erythropoietin and Antihemophaliac Factor, along with process and economic projections, are briefly reviewed.

Mccreight, L. R.↗

Superconductivity in sputtered CuMO6S8

Samples were prepared by melting the metals, followed by annealing to various temperatures. The result was a structurally weak material. Sputtered films on sapphire substrates were prepared and studied. The substrates give the films mechanical strength and permit easy attachment of electrical leads. Materials were characterized by X-ray diffraction, electron microscopy, electrical resistance vs. temperature, and critical current measurements. Some of the results on CuMo6S8 are presented.

Alterovitz, S.↗

Application of remote sensor data to geologic analysis of the Bonanza test site, Colorado

The author has identified the following significant results. The Hayden Pass (Orient mine area) includes 60 sq miles of the northern Sangre de Cristo Mountains and San Luis Valley in south-central Colorado. Based on interpretation of the remote sensor data, a geologic map was prepared and compared with a second geologic map, prepared from interpretation of both remote sensor data and field data. Comparison of the two maps gives an indication of the usefulness and reliability of the remote sensor data. The relative utility of color and color infrared photography was tested. The photography was used successfully to locate 75% of all faults in a portion of the geologically complex Bonanza volcanic center and to map and correctly identify 93% of all quaternary deposits and 62% of all areas of tertiary volcanic outcrop. Using a filter wheel photometer, more than 8,600 measurements of band reflectance of several sedimentary rocks were performed. The following conclusions were drawn: (1) the typical spectral reflectance curve shows a gradual increase with increasing wavelength; (2) the average band reflectance is about 0.20; and (3) within a formation, the minimum natural variation is about 0.04, or about 20% of the mean band reflectance.

Lee, K.↗

Carbon distribution profiles in lunar fines

Radial distribution profiles of elemental carbon in lunar soils consisting of particles in the size range of 50 to 150 microns were investigated. Initial experiments on specimen preparation and the analysis of prepared specimens by Auger electron spectrometry (AES) and scanning electron microscopy (SEM) are described. Results from splits of samples 61501,84 and 64421,11, which were mounted various ways in several specimen holders, are presented. A low carbon content was observed in AES spectra from soil particles that were subjected to sputter-ion cleaning with 960eV argon ions for periods of time up to a total exposure for one hour. This ion charge was sufficient to remove approximately 70 nm of material from the surface. All of the physically adsorbed carbon (as well as water vapor, etc.) would normally be removed in the first few minutes, leaving only carbon in the specimen, and metal support structure, to be detected thereafter.

Hart, R. K.↗

Extension of surface data by use of meteorological satellites

Ways of using meteorological satellite data to extend surface data are summarized. Temperature models are prepared from infrared data from ITOS/NOAA, NIMBUS, SMS/GOES, or future LANDSAT satellites. Using temperatures for surface meteorological stations as anchors, an adjustment is made to temperature values for each pixel in the model. The result is an image with an estimated temperature for each pixel. This provides an economical way of producing detailed temperature information for data-sparse areas, such as are found in underdeveloped countries. Related uses of these satellite data are also given, including the use of computer prepared cloud-free composites to extend climatic zones, and their use in discrimination of reflectivity-thermal regime zones.

Giddings, L. E.↗

Method for fabricating a mass spectrometer inlet leak

A method of fabricating an inlet leak for measuring chemically reactive gases is proposed. The method involves the steps of preparing a selected internal surface of a high melting point metal tubing for sealing to a glass tubing. A portion of the glass tubing is inserted into the prepared portion of the metal tubing, the glass tubing having an outer diameter substantially the same as the inner diameter of the metal tubing. The inserted glass tubing is sealed to the internal surface of the metal tubing; the glass tubing is drawn under a magnifying device to reduce the entire interior diameter thereof to substantially two microns; and an end portion of the drawing glass tubing is broken away.

Harris, R. F.↗

A preliminary training guide for utilizing high-altitude, color-infrared photography in compiling soil maps

Instruction for acquiring and analytically processing small-scale color-infrared photography to perform a soil resources inventory over forests of the southern U.S. is provided. Planning the project; acquiring aerial photography, materials, equipment and supplemental data; and preparing the photography for analysis are discussed. The procedures for preparing ancillary and primary component overlays are discussed. The use of correlation charts and dichotomous keys for mountain landforms, water regime, and vegetation is explained.

Weaver, J. E.↗