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At least 1,495 records · Page 83

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DOE OSTI2020

Comparison of woven and stitched out-of-autoclave E-glass/epoxy composites subjected to quasi-static and cyclic tensile loads

Tensile quasi-static and fatigue behaviors of out-of-autoclave, quasi-isotropic, E-glass/epoxy composites with woven and stitched fiber architectures are compared. Some specimens were cyclically loaded to failure, while others were tested for residual modulus and ultimate strength. Both laminates survived 10 7 cycles at a maximum stress of 94.8 MPa but failed prior to 10 7 cycles at a maximum stress greater than or equal to 124.1 MPa. For the stress-lifetime diagram and residual strength, the woven laminate had superior properties below 10 4 cycles and the stitched laminate had superior properties above 10 5 cycles. While intralaminar crack density was higher in the stitched laminate, the woven laminate demonstrated a higher percentage of delaminated area.

Materials Science↗

NASA NTRS1972

On fracture phenomena in advanced fiber composite materials.

The extension of linear elastic fracture mechanics (LEFM) from metallic alloys to advanced fiber composite laminates is considered. LEFM is shown to be valid for both isotropic and anisotropic homogeneous continua; the applicability of LEFM to advanced fiber composites is thus dependent on the validity of a homogeneous model of such materials. An experimental program to determine the validity of such a model for graphite/epoxy laminates is reviewed. Such laminates are found to have an apparent fracture toughness, from which it is inferred that a homogeneous material model is valid for the particular specimen geometry and composite laminates considered. Strain energy release rates are calculated from the experimentally determined fracture toughness of the various laminates. These strain energy release rates are found to lie in one of two groups, depending upon whether crack extension required fiber failure or matrix failure. The latter case is further investigated. It is concluded that matrix failure is governed by the tensile stress normal to the crack path.

Konish, H. J., Jr.↗

NASA NTRS1973

High temperature resistant composites from bismaleimide resin.

It is shown that bismaleimide/woven fiberglass composites molded at moderate pressures (100 psi) yield void-free laminates of good integrity. The strength of the laminates at room temperature compares favorably with epoxy/glass laminates; at 260 C, the laminates are far superior in oxidative aging to epoxy and silicon laminates. The synthesis, processing, and fabrication of a bismaleide polymer are discussed.

Gilwee, W. J.↗

NASA NTRS1974

Design, fabrication and test of graphite/epoxy metering truss structure components, phase 3

The design, materials, tooling, manufacturing processes, quality control, test procedures, and results associated with the fabrication and test of graphite/epoxy metering truss structure components exhibiting a near zero coefficient of thermal expansion are described. Analytical methods were utilized, with the aid of a computer program, to define the most efficient laminate configurations in terms of thermal behavior and structural requirements. This was followed by an extensive material characterization and selection program, conducted for several graphite/graphite/hybrid laminate systems to obtain experimental data in support of the analytical predictions. Mechanical property tests as well as the coefficient of thermal expansion tests were run on each laminate under study, the results of which were used as the selection criteria for the single most promising laminate. Further coefficient of thermal expansion measurement was successfully performed on three subcomponent tubes utilizing the selected laminate.

Source record↗

NASA NTRS1977

Tensile and compressive behavior of Borsic/aluminum

The results of an experimental investigation of the mechanical behavior of Borsic/aluminum are presented. Composite laminates were tested in tension and compression for monotonically increasing load and also for variable loading cycles in which the maximum load was increased in each successive cycle. It is shown that significant strain-hardening, and corresponding increase in yield stress, is exhibited by the metal matrix laminates. For matrix dominated laminates, the current yield stress is essentially identical to the previous maximum stress, and unloading is essentially linear with large permanent strains after unloading. For laminates with fiber dominated behavior, the yield stress increases with increase in the previous maximum stress, but the increase in yield stress does not keep pace with the previous maximum stress. These fiber dominated laminates exhibit smaller nonlinear strains, reversed nonlinear behavior during unloading, and smaller permanent strains after unloading. Compression results from sandwich beams and flat coupons are shown to differ considerably. Results from beam specimens tend to exhibit higher values for modulus, yield stress, and strength.

Herakovich, C. T.↗

NASA NTRS1978

A new experimental method for the accelerated characterization of composite materials

A method which permits the prediction of long-term properties of graphite/epoxy laminates on the basis of short-term (15 min) laboratory tests is described. Demonstration of delayed viscoelastic fracture in one laminate configuration, and data on the time and temperature response of a matrix-dominated unidirectional laminate contributed to a characterization of the viscoelastic process in the graphite/epoxy composites. Master curves from short-term tests of certain laminate configurations can be employed to generate long-term master curves. In addition, analytical predictions from short-term results can be used to predict long-term (25-hour) laminate properties.

Brinson, H. F.↗

NASA NTRS1980

Effect of temperature on composite sandwich structures subjected to low velocity impact

The effect of low velocity projectile impact on sandwich-type structural components was investigated. The materials used in the fabrication of the impact surface were graphite-, Kevlar-, and boron-fibers with appropriate epoxy matrices. The testing of the specimens was performed at moderately low- and high-temperatures as well as at room temperature to assess the impact-initiated strength degradation of the laminates. Eleven laminates with different stacking sequences, orientations, and thicknesses were tested. The low energy projectile impact is considered to simulate the damage caused by runway debris, the dropping of the hand tools during servicing, etc., on the secondary aircraft structures fabricated with the composite materials. The results show the preload and the impact energy combinations necessary to cause catastrophic failure in the laminates tested. A set of faired curves indicating the failure thresholds is shown separately for the tension-and compression-loaded laminates. The specific-strengths and -modulii for the various laminates tested are also given.

Sharma, A. V.↗

NASA NTRS1980

Thermal expansion of composites using Moire interferometry

An experimental technique for precise measurement of the thermal response of fiber-reinforced composite materials uses moire interferometry with fringe multiplication which yield a sensitivity of 833 nm (32.8 mu in.) per fringe. Results from the technique are compared with those obtained from electrical resistance strain gages, and also those predicted from classical lamination theory. Temperature dependent coefficients of thermal expansion for composite materials subjected to thermal cycling in the temperature range of 297 K (75 F) to 422 K (300 F) were determined for four laminate configurations (0, 90, 0/ + or - 45/90 sub s and 0/90/ + or - 45 sub s) of T300/5208 graphite epoxy, and ranged from -0.107 mu epsilon K/1 (-0.059 mu epsilon deg F/-) for the 0 laminate to 32.18 mu epsilon K/1 (17.88 mu epsilon F/1) for the 90 laminate. Moisture was found to greatly influence the thermal response of a quasi-isotropic laminate, resulting in hysteresis and residual compressive strain as the moisture content was reduced. Comparisons between moire and strain gage measurements were inconclusive with both techniques giving consistent but systematically different results. Differences of as much as 29% were observed.

Bowles, D. E.↗

NASA NTRS1980

Finite element stress analysis of a notched coupon specimen for in-plane shear behaviour of composites

The results of a linear elastic, plane stress finite element investigation of the stress distribution in a double V-notched coupon specimen are presented for an isotropic material (steel) and five graphite/polyimide laminates: (0), (90), (0/90)s, (plus or minus 45)s and (0/90/plus or minus 45)s. Stress contours, stress profiles, and stress concentration factors are presented for specimens loaded through rigid fixtures. It is shown that the finite element analysis predicts a region of essentially uniform pure shear in the central portion of the specimen for all laminates considered. Stress concentrations vary considerably with laminate configuration. The influences of elastic fixtures and thermal stresses on the stress distribution in (0) laminates are also investigated. The (0) laminate is predicted to exhibit maximum pure shear in the center of the test section for both rigid and elastic fixtures. It is concluded that the specimen is a practicable candidate for use as a composite shear specimen.

Herakovich, C. T.↗

NASA NTRS1980

Mechanisms of fatigue damage in boron/aluminum composites

Tensile fatigue tests were conducted on several laminates of boron/aluminum (6061-0). In laminates with 0 deg fibers on the outside, an analysis that identifies "shakedown" conditions predicted the stress amplitude below which no fatigue damage accumulated. A fatigue damage accumulation model which relates matrix fatigue cracking and the overall laminate properties is described. A model for the saturation damage stage development is presented, that identical laminates, tested in directions 90 deg apart (such that one layup has 90 deg outer plies and the other 0 deg), have different fatigue behaviors due to the stacking sequence. The 90 deg plies on the surface develop cracks earlier than predicted by shakedown. An attempt was made to explain this stacking sequence effect. Variable load history effects on the fatigue damage response were investigated. Tests reveal that for a given stress ratio the specimen seeks the saturation damage state for the largest stress range to which it is subjected. It was also found that little damage is generated by shifting a given stress range down, whereas significant damage may be created by shifting it upward. The laminate stresses were always tensile.

Johnson, W. S.↗

NASA NTRS1981

Fillers for improved graphite fiber retention by polymer matrix composites

The results of a program designed to determine the extent to which elemental boron and boron containing fillers added to the matrix resin of graphite/epoxy composites prevent the release of graphite fibers when the composites are exposed to fire and impact conditions are described. The fillers evaluated were boron, boron carbide and aluminum boride. The conditions evaluated were laboratory simulations of those that could exist in the event of an aircraft crash and burn situation. The baseline (i.e., unfilled) laminates evaluated were prepared from commercially available graphite/epoxy. The baseline and filled laminates' mechanical properties, before and after isothermal and humidity aging, also were compared. It was found that a small amount of graphite fiber was released from the baseline graphite/epoxy laminates during the burn and impact conditions used in this program. However, the extent to which the fibers were released is not considered a severe enough problem to preclude the use of graphite reinforced composites in civil aircraft structure. It also was found that the addition of boron and boron containing fillers to the resin matrix eliminated this fiber release. Mechanical properties of laminates containing the boron and boron containing fillers were lower than those of the baseline laminates. These property degradations for two systems: boron (5 micron) at 2.5 percent filler loading, and boron (5 micron) at 5.0 percent filler loading do not appear severe enough to preclude their use in structural composite applications.

House, E. E.↗

NASA NTRS1981

Mechanical characterization of PMR-15 graphite/polyimide bolted joints

Data are presented for the static and viscoelastic performance of Celion 6000/PMR-15 graphite/polyimide composite belted joints over the 21 to 315 C temperature range. Two laminate configurations were obtained by sectioning a panel into subpanels oriented parallel and perpendicular to the laminate principal direction. Three replicates of each specimen geometry were tested at each of the test temperatures for the two laminate configurations, and failure load was defined as the maximum load attained as indicated by the load/deflection curve. Effects of strain-rate on strength and failure mode behavior were assessed at room temperature for strain rates of 0.002, 0.01, 0.10, and 1.00/s, and creep behavior was examined for the case of bearing deformations at temperatures of 21 and 177 C. Results are presented, including: (1) two distinct mechanisms were responsible for bearing failure and related to laminate configuration, (2) the + or - 45 deg plies carried the shearing load in composite bolted joints, and (3) the material exhibited strain-rate sensitivity which varied with laminate configuration.

Wilson, D. W.↗

NASA NTRS1981

Environmental effects on composite fracture behavior

An experimental program was carried out to investigate the effects of temperature and moisture on the damage development and fracture response of graphite/epoxy composites. Fracture response data were obtained for 20-ply laminates of different layup patterns for both room temperature and immediately after the application of a temperature transient causing the specimen to attain 150 C. It is found that elevated temperature degrades the notched strength of some laminates while not degrading others. The unnotched strength of all laminates tested at elevated temperatures was degraded. The effect of preloading on damage growth and moisture absorption, the effect of autoclave pressure during the laminate cure on fracture, and the variation of interlaminar shear properties with layup, moisture exposure, laminate material, and cure pressure are also discussed.

Porter, T. R.↗

NASA NTRS1982

Accelerated fatigue durability of a high performance composite

The fatigue behavior of multidirectional graphite-epoxy laminates was analyzed theoretically and experimentally in an effort to establish an accelerated testing methodology. Analysis of the failure mechanism in fatigue of the laminates led to the determination of the failure mode governing fracture. The nonlinear, cyclic-dependent shear modulus was used to calculate the changing stress field in the laminate during the fatigue loading. Fatigue tests were performed at three different temperatures: 25 C, 74 C, and 114 C. The prediction of the S-N curves was made based on the artificial static strength artificial static strength at a reference temperature and the fatigue functions associated with them. The prediction of an S-N curve at other temperatures was performed using shifting factors determined for the specific failure mode. For multidirectional laminates, different S-N curves at different temperatures could be predicted using these shifting factors. Different S-N curves at different temperatures occur only when the fatigue failure mode is matrix dominated. It was found that whenever the fatigue failure mode is fiber dominated, temperature, over the range investigated, had no influence on the fatigue life. These results permit the prediction of long-time, low temperature fatigue behavior from data obtained in short time, high temperature testing, for laminates governed by a matrix failure mode.

Rotem, A.↗

NASA NTRS1980

Impact-initiated damage thresholds in composites

An experimental investigation was conducted to study the effect of low velocity projectile impact on the sandwich-type structural components. The materials used in the fabrication of the impact surface were graphite-, Kevlar-, and boron-fibers with appropriate epoxy matrices. The testing of the specimens was performed at moderately low- and high-temperatures as well as at room temperature to assess the impact-initiated strength degradation of the laminates. Eleven laminates with different stacking sequences, orientations, and thicknesses were tested. The low energy projectile impact is considered to simulate the damage caused by runway debris, dropping of the hand tools during servicing, etc., on the secondary aircraft structures fabricated with the composite materials. The results show the preload and the impact energy combinations necessary to cause catastrophic failures in the laminates tested. A set of faired curves indicating the failure thresholds is shown separately for the tension- and compression-loaded laminates. The specific-strengths and -moduli for the various laminates tested are also given.

Sharma, A. V.↗

NASA NTRS1983

Notch strength of composites

The notch strength of composites is discussed. The point stress and average stress criteria relate the notched strength of a laminate to the average strength of a relatively long tensile coupon. Tests of notched specimens in which microstrain gages have been placed at or near the edges of the holes have measured strains much larger that those measured in an unnotched tensile coupon. Orthotropic stress concentration analyses of failed notched laminates have also indicated that failure occurred at strains much larger than those experienced on tensile coupons with normal gage lengths. This suggests that the high strains at the edge of a hole can be related to the very short length of fiber subjected to these strains. Lockheed has attempted to correlate a series of tests of several laminates with holes ranging from 0.19 to 0.50 in. Although the average stress criterion correlated well with test results for hole sizes equal to or greater than 0.50 in., it over-estimated the laminate strength in the range of hole sizes from 0.19 to 0.38 in. It thus appears that a theory is needed that is based on the mechanics of failure and is more generally applicable to the range of hole sizes and the varieties of laminates found in aircraft construction.

Whitney, J. M.↗

NASA NTRS1982

The relationship of compliance changes during fatigue loading to the fracture of composite materials

The study outlined here is based on measurements of the change in engineering stiffness values induced by the development of damage in composite laminates during quasi-static or cyclic (fatigue) loading. These changes are found to be related to the individual details of the damage events in the laminates, as well as to the residual strength and life of the laminates. It is believed that the stiffness changes can also be used to relate composite material behavior under cyclic loading to its behavior under quasi-static loading. Results are presented for both notched and unnotched laminates. Compliance changes are found to be caused by damage events that bring about both global and local redistributions of stress. It is also found that the redistributions of stress determine the residual strength of the laminate. The quantitative link between compliance changes and fracture strength is the mechanics of the internal stress redistributions.

Reifsnider, K. L.↗

NASA NTRS1985

Investigation of composite materials property requirements for sonic fatigue research

Experimental techniques for determining the extensional and bending stiffness characteristics for symmetric laminates are presented. Vibrational test techniques for determining the dynamic modulus and material damping are also discussed. Partial extensional stiffness results intially indicate that the laminate theory used for predicting stiffness is accurate. It is clearly shown that the laminate theory can only be as accurate as the physical characteristics describing the lamina, which may vary significantly. It is recommended that all of the stiffness characteristics in both extension and bending be experimentally determined to fully verify the laminate theory. Dynamic modulus should be experimentally evaluated to determine if static data adequately predicts dynamic behavior. Material damping should also be ascertained because laminate damping is an order of magnitude greater than found in common metals and can significantly effect the displacement response of composite panels.

Patrick, H. V. L.↗