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DOE OSTI2013

An Internal Tin Tube Nb 3 Sn Conductor with Sn-B Core for Improved Non-Copper Critical Current Density

This STI product describes work performed under a Department of Energy Small Business Innovation Research Phase I award. The project was intended to further the development of the Internal Tin Tube (ITT) process for the fabrication of Nb 3 Sn conductor by utilizing a Sn-B powder core in the ITT filament instead of the conventional high-tin Cu-Sn core. The Sn-B core was to minimize the dissolution of the tubular niobium filament during heat treatment of the conductor and to simultaneously inhibit the growth of large-grained Nb 3 Sn at the interface of the core with the inner wall of the filament, effects that commonly occur in ITT conductors having high-tin cores. Both niobium wall dissolution and the formation of large-grained Nb 3 Sn are detrimental to the critical current density performance of ITT conductors. Wire fabrication problems were encountered due to the presence of large, hard Cu-Ti particles in the powder cores. However, it was found that thick (20-30 microns) layers of relatively fine grain Nb 3 Sn could be produced. A significant finding was the observation of fine precipitates on the Nb 3 Sn grain boundaries in reacted samples. Such precipitates could contribute to improved Nb 3 Sn conductor performance due to enhanced grain boundary flux pinning and restriction of grain growth.

36 MATERIALS SCIENCE↗

DOE OSTI2020

Additive Manufacturing of Energy Harvesting Material System for Active Wireless MEMS Sensors

Combustion systems make up a large sum of the world’s yearly energy production despite advances in renewable energy sources. Precise control of pressure and temperature in combustion chambers allows for lower carbon emissions, and overall higher efficiency. Wireless temperature and pressure sensors are critical for the operation of combustion chambers. Energy harvesters have emerged as a viable way to power wireless sensors when heat and mechanical energy are available. Lithium niobate (LNB), barium titanate (BTO), and lead zirconate titanate (PZT) pyroelectric ceramics were studied and fabricated through additive manufacturing (AM) for use as energy harvesting structures in combustion environments. The electric power generation potential of LNB and PZT ceramics was studied by varying the temperature from 50 to 60 °C and by introducing cyclic compression loads of 2000 N amplitude. It was found that thermal energy conversion had the highest output of 500 nW and that combined thermal and mechanical conversion did not increase the harvesting potential because of the competing contributions of both effects. Powder bed and slurry extrusion AM methods were used to fabricate BTO and PZT ceramic structures. Optimization of the powder-based binder jetting method produced BTO ceramics with a relative density of 36.77% a piezoelectric coefficient of 153 pC/N. The density of the ceramics increased up to 56% when increasing the saturation of binder in the powder to because of liquid phase sintering. Finally, PZT structures were manufactured through AM and fin features were added to the design to enhance the heat transfer along the material. The harvested power density of the flat samples was 3.643 μW/cm 3 and of the finned samples was 3.034 μW/cm3. This research paves the ways for the development of self-powered wireless sensors in critical areas of operation such as combustion.

01 COAL, LIGNITE, AND PEAT↗

DOE OSTI2021

Performance of Compact Pulsed Thermal Imaging System for In-Service Applications. Pulsed thermal tomography nondestructive examination of additively manufactured reactor materials and components

Additive manufacturing (AM) is an emerging method for cost-efficient fabrication of complex topology nuclear reactor parts from high-strength corrosion resistance alloys, such as stainless steel and Inconel. AM of metallic structures for nuclear energy applications is currently based on laser powder bed fusion (LPBF) process, which has the capability of melting metallic powder and net shaping the structures with relatively high precision. Some of the challenges with using LPBF method for nuclear manufacturing include the possibility of introducing pores into metallic structures. Integrity of AM structures needs to be evaluated nondestructively because material flaws could lead to premature failures due to creep in high temperature nuclear reactor environment. Currently, there exist limited capabilities to evaluate actual AM structures nondestructively. Pulsed Thermography (PT) imaging provides a capability for non-destructive evaluation (NDE) of sub-surface defects in arbitrary size structures. The PT method is based on recording material surface temperature transients with infrared (IR) camera following thermal pulse delivered on material surface with flash light. The PT method has advantages for NDE of actual AM structures because the method involves one-sided non-contact measurements and fast processing of large sample areas captured in one image. The data cube of PT measurements consists of surface temperature taken at sequential time intervals T(x,y,t). Material defects can be detected either by analyzing the thermograms T(x,y,t) data cube, or by using thermal tomography (TT) algorithm to obtain 3D spatial reconstruction of thermal effusivity e(x,y,z). To reduce the cost and enable in-service NDE in spatially constrained environment, it is highly desirable to develop PT with compact and inexpensive IR camera. Following initial qualification of an AM component for deployment in a nuclear reactor, a compact PT system can also be used for in-service nondestructive evaluation (NDE) applications. However, data cube obtained with PT based on compact IR camera suffers from strong thermal noises and loss of features due to relatively low sampling rate. In this report we describe two unsupervised machine learning (ML) algorithms for enhancement of PT images obtained with compact IR camera. In one approach, we introduce Sparse Coding Discrete Cosine Transform (SC/DCT) algorithm to remove additive white Gaussian noise (AWGN) from spatial thermal effusivity reconstructions. In another approach we introduce a Spatial Temporal Denoised Thermal Source Separation (STDTSS) ML algorithm to process thermograms. The STDTSS algorithm consists of spatial and temporal denoising using Gaussian and Savitzky–Golay filtering, followed by the matrix decomposition using Principal Component Analysis (PCA), and Independent Component Analysis (ICA) to automatically detect flaws. In the work described in this report, we constructed a compact PT system using a relatively small and low-cost FLIR A65 camera, consisting on uncooled microbolometer detector. Performance of SC/DCT algorithm was demonstrated on enhancing TT images of Inconel 718 AM plate. Performance of the STDTSS methods was investigated using thermography data obtained from imaging stainless steel 316L specimens produced with LPBF method with imprinted calibrated porosity defects.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗

DOE OSTI2021

Fabrication and Characterization of Non-Equilibrium Plasma-Treated PVDF Nanofiber Membrane-Based Sensors

The effect of a self-pulsing non-equilibrium plasma discharge on piezoelectric PVDF nanofiber membrane was investigated. The plasma discharge was generated in air with a DC power source, with a discharge current of 0.012 mA, a nominal interelectrode separation of 1 mm, and discharge voltage of ~970 V. In a continuous fabrication process, the electrospinning method was used to generate thin nanofiber membrane with a flow rate of 0.7–1 mL h -1 and 25–27 kV voltage to obtain the nanofiber with high sensitivity and a higher degree of alignment and uniformity over a larger area. Plasma treatment was applied on both single layer and multi-layer (three layers) nanomembranes. In addition, simultaneously, the nanofiber membranes were heat-treated at a glass transition temperature (80–120 °C) and then underwent plasma treatment. Fourier-transform infrared (FTIR) spectroscopy showed that the area under the curve at 840 and 1272 cm -1 (β phase) increased due to the application of plasma and differential scanning calorimeter (DSC) indicated an increase in the degree of crystallinity. Finally, PVDF sensors were fabricated from the nanofibers and their piezoelectric properties were characterized. The results suggested that compared to the pristine samples the piezoelectric properties in the plasma and plasma-heat-treated sensors were enhanced by 70% and 85% respectively.

42 ENGINEERING↗

DOE OSTI2017

The spatially resolved [C ii] cooling line deficit in galaxies

We present [C ii] 158 μm measurements from over 15,000 resolved regions within 54 nearby galaxies of the Kingfish program to investigate the so-called [C ii] “line-cooling deficit” long known to occur in galaxies with different luminosities. The [C ii]/TIR ratio ranges from above 1% to below 0.1% in the sample, with a mean value of 0.48 ± 0.21%. We find that the surface density of 24 μm emission dominates this trend, with [C ii]/TIR dropping as νI{sub ν}(24 μm) increases. Deviations from this overall decline are correlated with changes in the gas-phase metal abundance, with higher metallicity associated with deeper deficits at a fixed surface brightness. We supplement the local sample with resolved [C ii] measurements from nearby luminous infrared galaxies and high-redshift sources from z = 1.8–6.4, and find that star formation rate density drives a continuous trend of deepening [C ii] deficit across six orders of magnitude in Σ{sub sfr}. The tightness of this correlation suggests that an approximate Σ{sub sfr} can be estimated directly from global measurements of [C ii]/TIR, and a relation is provided to do so. Several low-luminosity active galactic nucleus (AGN) hosts in the sample show additional and significant central suppression of [C ii]/TIR, but these deficit enhancements occur not in those AGNs with the highest X-ray luminosities, but instead those with the highest central starlight intensities. Taken together, these results demonstrate that the [C ii] line-cooling line deficit in galaxies likely arises from local physical phenomena in interstellar gas.

79 ASTRONOMY AND ASTROPHYSICS↗

NASA NTRS1982

Aluminum and chromium ion particle studies for enhancement of surface properties

An experimental project was undertaken which produced ion plated coatings on steel substrates. About twenty tensile samples of 4340 steel were ion plated in the Denton system with aluminum using resistance heating evaporation boats. In the V.T.A. 7375 system, ten samples were chromium ion plated; four on 4340 steel disks and the other six onto 440-C stainless steel rods for roller bearing wear improvement testing. Each of the samples was plated on a separate run to correlate the film parameters with the run parameters. Some of the chromium literature was reviewed, and improvements to the vacuum system were made.

Source record↗

NASA NTRS1982

BRDF measurements of sunshield and baffle materials for the IRAS telescope

Measurements of the far-infrared bidirectional reflectance distribution functions (BRDF) of four samples of Martin Black coating and one sample of gold coated aluminum from the telescope to be flown on the Infrared Astronomy Satellite (IRAS) are presented. At incidence angles near 35 deg Martin Black is a diffuse reflector at wavelengths as long as 36 microns. The gold coated aluminum sample from the IRAS sunshield has a visible grain which causes a strong diffraction enhancement of the BRDF at large nonspecular angles. This enhancement from the sunshield will increase the stray light level inside the telescope.

Smith, S. M.↗

NASA NTRS1988

In situ observations of ClO in the wintertime Northern Hemisphere: ER-2 aircraft results from 21 N to 61 N latitude

Measurements of lower stratospheric ClO taken during a NASA ER-2 flight between Moffett Field, CA (37 N, 122 W) and Great Slave Lake, Canada (61 N, 116 W) on 13 February 1988 are reported. Northbound, the aircraft was flown at about 20 km altitude from 39 N to 56 N, at 18 km from there to 58 N, in a descent to 15 km at 60 N, and in a rise and turn at the northernmost point. The southbound leg was flown in a gradual climb from 20 km to 21.5 km. On this day, the central position of the Arctic polar vortex, as determined by an NMC analysis of heights and temperatures at the 50 mb and 70 mb levels, was approximately 79 N, 100 W. Because the vortex was located on the North American side of the pole, the aircraft was able to reach a point slightly inside the maximum horizontal wind region where wind speeds were 80 to 90 knots. The general pattern for the observed ClO is that it increased with both latitude and altitude, and attained a maximum of about 55 pptv at 61 N latitude and 20.5 km altitude. This value is about 20 times smaller than the maxima observed over Antarctica, but is comparable to those seen just outside the chemical containment vessel located inside the Antarctic Polar vortex. On the other hand, in a comparison with northern midlatitude data taken on this and three other February flights, ClO mixing ratios observed north of 55 N latitude are 2 to 5 times larger at all flight altitudes (15 to 20 km). Possible reasons are discussed for this enhancement over midlatitude and the evidence is considered for whether or not the instruments sampled Arctic polar vortex air. A second feature of the data is the strong positive correlation between ClO and O3 during the entire flight.

Brune, W. H.↗

NASA NTRS1989

Candidate sample acquisition systems for the Rosetta

The Comet Nucleus Sample Return (CNSR) mission, one of the four cornerstones of the ESA scientific program, is one of the most complex space ventures within the next century, both from technological and deep space exploration point of view. In the Rosetta scenario the sample acquisition phase represents the most critical point for the global mission's success. The proposed paper illustrates the main results obtained in the context of the CNSR-SAS ongoing activity. The main areas covered are related to: (1) sample properties characterization (comet soil model, physical/chemical properties, reference material for testing); (2) concepts identification for coring, shovelling, harpooning and anchoring; (3) preferred concept (trade off among concepts, identification of the preferred configuration); and (4) proposed development activity for gaining the necessary confidence before finalizing the CNSR mission. Particular emphasis will be given to the robotic and flexibility aspects of the identified sample acquisition systems (SAS) configuration, intended as a means for the overall system performance enhancement.

Magnani, P. G.↗

NASA NTRS1992

The Burning of Metals and Alloys in Microgravity

The NASA-Lewis 2.2-sec drop tower has been used to characterize the oxygen-atmosphere burning of several representative spacecraft environment metallic materials in microgravity; these included rods of 2219 Al alloy, 316 stainless steel, Fe, and Ti, as well as sheets and meshes of 316 stainless steel. The absence of buoyant forces does not preclude extinguishment of the combustion process, and the regression rate of the melting interface of the cylindrical rods is significantly greater than in normal gravity. The flammability of such sample shapes as thin sheets, which are known to extinguish in normal gravity, is enhanced. Volatile combustion products are generated, in contrast to the normal gravity regime.

Steinberg, Theodore A.↗

NASA NTRS1992

Ions with low charges in the solar wind as measured by SWICS on board Ulysses

We present new data on rare ions in the solar wind. Using the Ulysses-SWICS instrument with its very low background we have searched for low-charge ions during a 6-d period of low-speed solar wind and established sensitive upper limits for many species. In the solar wind, we found He(1+)/He(2+) of less than 5 x 10 exp -4. This result and the charge state distributions of heavier elements indicate that all components of the investigated ion population went through a regular coronal expansion and experienced the typical electron temperatures of 1 to 2 million Kelvin. We argue that the virtual absence of low-charge ions demonstrates a very low level of nonsolar contamination in the source region of the solar wind sample we studied. Since this sample showed the FlP effect typical for low-speed solar wind, i.e., an enhancement in the abundances of elements with low first ionization potential, we conclude that this enhancement was caused by an ion-atom separation mechanism operating near the solar surface and not by foreign material in the corona.

Geiss, J.↗

NASA NTRS1993

Pairing statistics for infrared-luminous galaxies

A knowledge of the pairing fraction of IR-selected galaxies is important in understanding the role of interactions in star formation and nuclear activity. It is clear that interactions are extremely common among the most IR-luminous systems, but results have been inconsistent for less luminous systems; this may result from using peculiar morphology as an indicator of an interaction. Since features associated with milder interactions (e.g., tidal tails) tend to be faint, their detection necessarily depends on the depth of the survey used to identify interacting pairs. We present a sample of IR- and optically-selected galaxies for which we have computed pairing fractions using strictly geometrical, quantitative criteria. For the analysis we used a likelihood ratio technique developed by Keel and van Soest (1992). We find that the pairing fraction for IR-selected galaxies is roughly 30 percent, comparable to that found by Keel and van Soest for optically-selected starbursts. We also detect a strong correlation (r above 0.99) between the 60 micron luminosity of a galaxy sample and its pairing fraction. We conclude that although tidal interactions do not guarantee enhanced activity (AGN or starburst), they can amplify internal properties that would feed such activity.

Gallimore, J. F.↗

NASA NTRS2016

Coordinates of Anthropogenic Features on the Moon

High-resolution images from the Lunar Reconnaissance Orbiter Camera (LROC) Narrow Angle Camera (NAC) reveal the landing locations of recent and historic spacecraft and associated impact sites across the lunar surface. Using multiple images of each site acquired between 2009 and 2015, an improved Lunar Reconnaissance Orbiter (LRO) ephemeris, and a temperature-dependent camera orientation model, we derived accurate coordinates ( less than 12 meters) for each soft-landed spacecraft, rover, deployed scientific payload, and spacecraft impact crater that we have identified. Accurate coordinates enhance the scientific interpretations of data returned by the surface instruments and of returned samples of the Apollo and Luna sites. In addition, knowledge of the sizes and positions of craters formed as the result of impacting spacecraft provides key benchmarks into the relationship between energy and crater size, as well as calibration points for reanalyzing seismic measurements acquired during the Apollo program. We identified the impact craters for the three spacecraft that impacted the surface during the LRO mission by comparing before and after NAC images.

Moon↗

NASA NTRS2016

Technology Development and Design of a Hybrid Mars Ascent Vehicle Concept

Hybrid propulsion has been investigated as an enhancing technology for a Mars Ascent Vehicle (MAV) concept as part of potential Mars Sample Return (MSR) because of its high specific impulse, restartability, and the ability to operate and survive at extremely low temperatures. A new wax-based hybrid fuel formulation has been developed that could withstand the harsh and variable Mars environment protected solely by a minimal layer of passive insulation. This formulation could provide substantial energy savings for a notional lander and is critical for rover mobility. Preliminary thermal cycle testing has determined that the formulation can survive the expected temperature extremes and lifetime thermal testing is currently underway. A complete preliminary design using this new fuel formulation combined with a low temperature oxidizer such as Mixed Oxides of Nitrogen (MON30) is presented. Several key features associated with a complete hybrid MAV concept are investigated to determine their mission suitability (e.g. Thrust Vector Control and restartable ignition options). Potential challenges along a path towards developing such a system are outlined and future work is suggested as a means of technology maturation. The hybrid design presented here was the lowest Gross Lift Off Mass (GLOM) result of a 2015 Jet Propulsion Laboratory (JPL) led MAV concept study.

MSR↗

NASA NTRS2016

Technology Development and Design of a Hybrid Mars Ascent Vehicle Concept

Karp, Ashley C.↗

NASA NTRSDate not supplied

Guidance Enhancements and Performance Assessments for the Mars Ascent Vehicle Spin-Stabilized Upper Stage Configuration

he objective of the Mars Sample Return (MSR) campaign is to return samples from the surface of Mars to Earth for research. As one element of the MSR campaign, the Mars Ascent Vehicle (MAV) is responsible for transporting the samples from the surface of Mars to a Low-Martian Orbit (LMO) for retrieval. Complete autonomy is required throughout ascent, and orbital insertion is constrained by tight dispersion boundaries. An unguided, spin-stabilized second stage for MAV has been selected over a guided upper-stage to drive mass savings and reduce overall MSR campaign mass risk, at the cost of reduced GNC capability. To address this design change, the MAV GNC team has derived a robust prediction algorithm, building on previous energy management schemes, that solves for a single inertial pointing direction solution for the spin-stabilized 2nd stage burn. Algorithm stability is explored that compared to previous versions of the algorithm. Also, a set of analytical partials was developed to study MAV’s dispersed orbital insertion performance with respect to MAV system uncertainties. These partials were verified through simulation analysis and prove useful for analytical insight into the dynamics of MAV during the 2nd stage maneuver.

Jason M Everett↗

NASA NTRSDate not supplied

Guidance Enhancements and Performance Assessments for the Mars Ascent Vehicle Spin-Stabilized Upper Stage Configuration

The objective of the Mars Sample Return (MSR) campaign is to return samples from the surface of Mars to Earth for research. As one element of the MSR campaign, the Mars Ascent Vehicle (MAV) is responsible for transporting the samples from the surface of Mars to a Low-Martian Orbit (LMO) for retrieval. Complete autonomy is required throughout ascent, and orbital insertion is constrained by tight dispersion boundaries. An unguided, spin-stabilized second stage for MAV has been selected over a guided upper-stage to drive mass savings and reduce overall MSR campaign mass risk, at the cost of reduced GNC capability. To address this design change, the MAV GNC team has derived a robust prediction algorithm, building on previous energy management schemes, that solves for a single inertial pointing direction solution for the spin-stabilized 2nd stage burn. Algorithm stability is explored that compared to previous versions of the algorithm. Also, a set of analytical partials was developed to study MAV’s dispersed orbital insertion performance with respect to MAV system uncertainties. These partials were verified through simulation analysis and prove useful for analytical insight into the dynamics of MAV during the 2nd stage maneuver.

GNC↗

NASA NTRS2023

3D Printed TiO 2 Negative Electrodes for Sodium-Ion and Lithium-ion Batteries using Vat Photopolymerization

Additive manufacturing, also called 3D printing, represents a unique approach to develop three dimensional shape-conformable batteries with enhanced electrodes, specific surface area, improved ion diffusion, and power. For the first time, the formulation of a composite photocurable resin loaded with battery electrochemically active components was designed to feed a vat photopolymerization (VPP) 3D printer. In direct alignment with NASA’s Artemis mission goals to develop sustainable lunar energy storage infrastructure necessary to support long-term human operations, TiO 2 was here selected as an active material for the negative electrode for sodium-ion and lithium-ion batteries due to its abundance on the lunar surface. The TiO 2 loading in the composite photocurable resin and in the resulting VPP-printed negative electrode was increased as high as possible to enhance the electrochemical performance, while simultaneously ensuring the printability and acceptable mechanical strength for sample handling. The effect of thermal post-processing on the electrical, electrochemical and mechanical performance is reported. Finally, a configurational study is implemented to identify the impact of two different electrode designs (cubic and gyroid lattice unit cells) on the electrochemical performance. This work addresses the difficulties related to the introduction of solid particles within a VPP photocurable resin and the need for a compromise between the electrochemical performances and printability to obtain fully functional VPP-printed electrodes.

sodium-ion battery↗