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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,477 records · Page 82
All sourcesNASA NTRSDOE OSTI
NASA NTRS1993

Process modelling for materials preparation experiments

The main goals of the research consist of the development of mathematical tools and measurement of transport properties necessary for high fidelity modeling of crystal growth from the melt and solution, in particular for the Bridgman-Stockbarger growth of mercury cadmium telluride (MCT) and the solution growth of triglycine sulphate (TGS). Of the tasks described in detail in the original proposal, two remain to be worked on: development of a spectral code for moving boundary problems, and diffusivity measurements on concentrated and supersaturated TGS solutions. During this eighth half-year period, good progress was made on these tasks.

Rosenberger, Franz↗
NASA NTRS1988

Airborne Arctic Stratospheric Expedition Preparation: Ozone

This video shows the rollout of the ER-2 and DC-8 at Ames, takeoffs and landings, and operations aboard the DC-8 and ER-2 in Puntas Arenas, Chile. Animation of the north polar regions showing the ozone hole is also included.

Source record↗
NASA NTRS1993

Preparation of particle-dispersion alloys (M-6)

A particle dispersion alloy is one type of metal-ceramic composite material, and is used as heat resistance material, wear resistance material, and electrical material. This material consists of a metal matrix and dispersed particles, and for its unique structure it has both tenacity as a metal and hardness as a ceramic. Its properties improve when the particles become finer and disperse more uniformly. Most of the particle dispersion alloys are produced by the powder metallurgical process. This process is favorable for uniform dispersion of particles, but it consists of complicated techniques such as mechanical alloying and hot extrusion, and has the following drawbacks: (1) it is difficult to fabricate large-sized products; (2) the amount of particles is limited to a few percent; and (3) the process is complicated and expensive. To overcome these drawbacks, recently special attention has been paid to conventional melting process. However, under terrestrial conditions, dispersions separate immediately due to the different specific gravities of the metal matrix and the particles and thermal convection effects. The microgravity environment is, therefore, considered to be an attractive place for fabricating the dispersion alloy. This space experiment is carried out to clarify the influence of microgravity on the properties of the particle dispersion alloy and to obtain a deeper understanding of the experiment under the microgravity environment.

Muramatsu, Yuji↗
NASA NTRS1993

Preparation of optical materials used in non-visible region (M-17)

The purpose of the experiment was the following: development of containerless glass melting technique; fabrication of high purity glass; and development of acoustic levitation technique. For the space experiment, glass 65CaO-25Ga2O3-10GeO2 was selected out of various types of glasses. The expected results are: ultra-high purity glass and manipulation by acoustics.

Hayakawa, J.↗
NASA NTRS1993

Physical and chemical properties of some new perfluoropolyalkylether lubricants prepared by direct fluorination

A series of perfluoropolyalkylether (PFPAE) fluids was synthesized by direct fluorination. Viscosity-temperature properties, oxidation stabilities, oxidation-corrosion properties, bulk modulus, lubricity, surface tension and density were measured. It was shown that as the carbon to oxygen ratio in the polymer repeating unit decreases, the viscometric properties improve, the fluids may become poorer boundary lubricants, the bulk modulus increases, the surface tension increases and the fluid density increases. The presence of difluoromethylene oxide units in the polymer does not significantly lower the oxidation and oxidation-corrosion stabilities as long as the difluoromethylene oxide units are separated by other units.

Jones, W. R., Jr.↗
NASA NTRS1994

Formation and chemical reactivity of carbon fibers prepared by defluorination of graphite fluoride

Defluorination of graphite fluoride (CFX) by heating to temperatures of 250 to 450 C in chemically reactive environments was studied. This is a new and possibly inexpensive process to produce new carbon-based materials. For example, CF 0.68 fibers, made from P-100 carbon fibers, can be defluorinated in BrH2C-CH = CH-CH2Br (1,4-dibromo-2butene) heated to 370 C, and graphitized to produce fibers with an unusually high modulus and a graphite layer structure that is healed and cross-linked. Conversely, a sulfur-doped, visibly soft carbon fiber was produced by defluorinating CF 0.9 fibers, made from P-25, in sulfur (S) vapor at 370 C and then heating to 660 C in nitrogen (N2). Furthermore, defluorination of the CF 0.68 fibers in bromine (Br2) produced fragile, structurally damaged carbon fibers. Heating these fragile fibers to 1100 C in N2 caused further structural damage, whereas heating to 150 C in bromoform (CHBr3) and then to 1100 C in N2 healed the structural defects. The defluorination product of CFX, tentatively called activated graphite, has the composition and molecular structure of graphite, but is chemically more reactive. Activated graphite is a scavenger of manganese (Mn), and can be intercalated with magnesium (Mg). Also, it can easily collect large amounts of an alloy made from copper (Cu) and type 304 stainless steel to form a composite. Finally, there are indications that activated graphite can wet metals or ceramics, thereby forming stronger composites with them than the pristine carbon fibers can form.

Hung, Ching-Cheh↗
NASA NTRS1994

Process modelling for materials preparation experiments

The main goals of the research under this grant consist of the development of mathematical tools and measurement techniques for transport properties necessary for high fidelity modelling of crystal growth from the melt and solution. Of the tasks described in detail in the original proposal, two remain to be worked on: development of a spectral code for moving boundary problems, and development of an expedient diffusivity measurement technique for concentrated and supersaturated solutions. We have focused on developing a code to solve for interface shape, heat and species transport during directional solidification. The work involved the computation of heat, mass and momentum transfer during Bridgman-Stockbarger solidification of compound semiconductors. Domain decomposition techniques and preconditioning methods were used in conjunction with Chebyshev spectral methods to accelerate convergence while retaining the high-order spectral accuracy. During the report period we have further improved our experimental setup. These improvements include: temperature control of the measurement cell to 0.1 C between 10 and 60 C; enclosure of the optical measurement path outside the ZYGO interferometer in a metal housing that is temperature controlled to the same temperature setting as the measurement cell; simultaneous dispensing and partial removal of the lower concentration (lighter) solution above the higher concentration (heavier) solution through independently motor-driven syringes; three-fold increase in data resolution by orientation of the interferometer with respect to diffusion direction; and increase of the optical path length in the solution cell to 12 mm.

Rosenberger, Franz↗
NASA NTRS1994

A modular approach for automated sample preparation and chemical analysis

Changes in international relations, especially within the past several years, have dramatically affected the programmatic thrusts of the U.S. Department of Energy (DOE). The DOE now is addressing the environmental cleanup required as a result of 50 years of nuclear arms research and production. One major obstacle in the remediation of these areas is the chemical determination of potentially contaminated material using currently acceptable practices. Process bottlenecks and exposure to hazardous conditions pose problems for the DOE. One proposed solution is the application of modular automated chemistry using Standard Laboratory Modules (SLM) to perform Standard Analysis Methods (SAM). The Contaminant Analysis Automation (CAA) Program has developed standards and prototype equipment that will accelerate the development of modular chemistry technology and is transferring this technology to private industry.

Clark, Michael L.↗
NASA NTRS1994

Ferric chloride graphite intercalation compounds prepared from graphite fluoride

The reaction between graphite fluoride and ferric chloride was observed in the temperature range of 300 to 400 C. The graphite fluorides used for this reaction have an sp3 electronic structure and are electrical insulators. They can be made by fluorinating either carbon fibers or powder having various degrees of graphitization. Reaction is fast and spontaneous and can occur in the presence of air. The ferric chloride does not have to be predried. The products have an sp2 electronic structure and are electrical conductors. They contain first stage FeCl3 intercalated graphite. Some of the products contain FeCl2*2H2O, others contain FeF3 in concentrations that depend on the intercalation condition. The graphite intercalated compounds (GIC) deintercalated slowly in air at room temperature, but deintercalated quickly and completely at 370 C. Deintercalation is accompanied by the disappearing of iron halides and the formation of rust (hematite) distributed unevenly on the fiber surface. When heated to 400 C in pure N2 (99.99 vol %), this new GIC deintercalates without losing its molecular structure. However, when the compounds are heated to 800 C in quartz tube, they lost most of its halogen atoms and formed iron oxides (other than hematite), distributed evenly in or on the fiber. This iron-oxide-covered fiber may be useful in making carbon-fiber/ceramic-matrix composites with strong bonding at the fiber-ceramic interface.

Hung, Ching-Cheh↗
NASA NTRS1994

NASA/DOD Aerospace Knowledge Diffusion Research Project. Paper 44: Becoming an aerospace engineer: Some thoughts on the career goals and educational preparation of AIAA student members

Similarities and differences between undergraduate and graduate engineering students in the context of two general aspects of educational experience are described. Considered first is the extent to which students differ regarding the factors that led to the choice of a career in aerospace engineering, their current levels of satisfaction with that choice, and career-related goals and objectives. Second, the importance of certain information-use skills for professional success, and the frequency of use and importance of specific information sources and products to meet students' educational needs, are explored.

Pinelli, Thomas E.↗
NASA NTRS1995

Ultra-high pressure water jetting for coating removal and surface preparation

This paper shall examine the basics of water technology with particular attention paid to systems currently in use and some select new applications. By providing an overview of commercially available water jet systems in the context of recent case histories, potential users may evaluate the process for future applications. With the on going introduction of regulations prohibiting the use of chemical paint strippers, manual scrapping and dry abrasive media blasting, the need for an environmentally compliant coating removal process has been mandated. Water jet cleaning has been a traditional part of many industrial processed for year, although it has only been in the last few years that reliable pumping equipment capable of ultra-high pressure operation have become available. With the advent of water jet pumping equipment capable of sustaining pressures in excess of 36,000 psi. there has been shift away from lower pressure, high water volume systems. One of the major factors in driving industry to seek higher pressures is the ability to offer higher productivity rates while lowering the quantity of water used and subsequently reprocessed. Among benefits of the trend toward higher pressure/lower volume systems is the corresponding reduction in water jet reaction forces making hand held water jetting practical and safe. Other unique applications made possible by these new generation pumping systems include the use of alternative fluids including liquid ammonia for specialized and hazardous material removal applications. A review of the equipment used and the required modifications will be presented along with the conclusions reached reached during this test program.

Johnson, Spencer T.↗
NASA NTRS1995

Analytical pyrolysis experiments of Titan aerosol analogues in preparation for the Cassini Huygens mission

Comparative pyrolysis mass spectrometric data of Titan aerosol analogs, called 'tholins', are presented. The Titan tholins were produced in the laboratory at Cornell by irradiation of simulated Titan atmospheres with high energy electrons in plasma discharge. Mass-spectrometry measurements were performed at FOM of the solid phase of various tholins by Curie-point pyrolysis Gas-Chromatography/Mass-Spectrometry (GCMS) and by temperature resolved in-source Pyrolysis Mass-Spectrometry to reveal the composition and evolution temperature of the dissociation products. The results presented here are used to further define the ACP (Aerosol Collector Pyrolyser)-GCMS experiment and provide a basis for modelling of aerosol composition on Titan and for the iterpretation of Titan atmosphere data from the Huygens probe in the future.

Ehrenfreund, P.↗
NASA NTRS1995

Improved Preparation Of Solid-Electrolyte Films

Modified process ensures compatability among components. Improved chemical-blending procedure produces composite material for thin, large-area solid-electrolyte films for lithium batteries. Films have uniform compositions and dimensionally stable. Transport number of their lithium cations is high, close to unity. Batteries made with these films expected to have energy and power densities up to about 100 W h/kg and 100 W/kg, respectively. Previous version of composite material described in "Composite Solid Electrolyte for Lithium Cells" (NPO-18694).

Nagasubramanian, Ganesan↗
NASA NTRS1995

Preparation, structure and superconductivity of high T(c) compounds: Research of high temperature superconductors in Hungary

In this paper the main directions, methods and results of the investigation of high-T(c) superconductors in Hungary are briefly summarized. The fundamental idea of this research is to study the effect of starting conditions on the microstructure of samples and the influence of the latter one on their superconducting parameters. The investigation concerning technical development is also mentioned.

Kirschner, I.↗
NASA NTRS1995

Preparation of polymeric diacetylene thin films for nonlinear optical applications

A method for producing polymeric diacetylene thin films having desirable nonlinear optical characteristics has been achieved by producing amorphous diacetylene polymeric films by simultaneous polymerization of diacetylene monomers in solution and deposition of polymerized diacetylenes on to the surface of a transparent substrate through which ultraviolet light has been transmitted. These amorphous polydiacetylene films produced by photo-deposition from solution possess very high optical quality and exhibit large third order nonlinear optical susceptibilities, such properties being suitable for nonlinear optical devices such as waveguides and integrated optics.

Frazier, Donald O.↗
NASA NTRS1995

NASA/DOD Aerospace Knowledge Diffusion Research Project. Paper 55: Career goals and educational preparation of aerospace engineering and science students: An international perspective

Results are presented of a survey of aerospace engineering and science students conducted in India, Japan, Russia, the United Kingdom, and the United States. The similarities and differences among aerospace engineering and science students from the five countries are examined in the context of two general aspects of educational experience. First, the extent to which students differ regarding the factors that led to the choice of a career in aerospace, their current levels of satisfaction with that choice, and career-related goals and objectives is considered. Second, the importance of certain communications/information-use skills for professional use is examined, as well as the frequency of use and importance of specific information sources and products to meet students' educational needs. Overall, the students who participated in this research remain relatively happy with the choice of a career in aerospace engineering, despite pessimism in some quarters about the future of the industry. Regardless of national identity, aerospace engineering and science students appear to share a similar vision of the profession in terms of their career goals and aspirations. The data also indicate that aerospace engineering and science students are well aware of the importance of communications/information-use skills to professional success and that competency in these skills will help them to be productive members of their profession. Collectively, all of the students appear to use and value similar information sources and products, although some differences appear by country.

Pinelli, Thomas E.↗
NASA NTRS1995

Overview of the preparation and use of an OV-10 aircraft for wake vortex hazards flight experiments

An overview is presented of the development, use, and current flight-test status of a highly instrumented North American Rockwell OV-10A Bronco as a wake-vortex-hazards research aircraft. A description of the operational requirements and measurements criteria, the resulting instrumentation systems and aircraft modifications, system-calibration and research flights completed to date, and current flight status are included. These experiments are being conducted by the National Aeronautics and Space Administration as part of an effort to provide the technology to safely improve the capacity of the nation's air transportation system and specifically to provide key data in understanding and predicting wake vortex decay, transport characteristics, and the dynamics of encountering wake turbulence. The OV-10A performs several roles including meteorological measurements platform, wake-decay quantifier, and trajectory-quantifier for wake encounters. Extensive research instrumentation systems include multiple airdata sensors, video cameras with cockpit displays, aircraft state and control-position measurements, inertial aircraft-position measurements, meteorological measurements, and an on-board personal computer for real-time processing and cockpit display of research data. To date, several of the preliminary system check flights and two meteorological-measurements deployments have been completed. Several wake encounter and wake-decay-measurements flights are planned for the fall of 1995.

Stuever, Robert A.↗
NASA NTRS1996

Preparation of Flight Operations and IWS Integration of the CELIAS Experiment on the SOHO Spacecraft

During this annual progress report time period, the following activities took place: (1) Generation of several versions of the CELIAS (STOF/SEM/CTOF/MTOF/DPU) commissioning timeline for the first 180 days after launch. These were written and submitted by A. Galvin after consultation (phone, fax, e-mail, meetings) with the CELIAS Instrument Manager and Lead-Co-I's. (2) Identification of several problems with the CELIAS portion of the Project Data Base (PDB). (3) Meetings with the Flight Operations Team regarding PDB, critical commands, etc. (4) Attend Science Operations Working Group (SOWG) Meetings (November 1994, February 1995, May 1995) and Flight Operations Review Meeting (July 1995). (5) Participate in Flight Operation Simulations SIM 1 (November 14-18, 1994), SIM 2 (May 1-4, 1995) and SIM3 (August 7-11, 1995). (6) Participate in the Ground System Compatibility Test Rehearsal (April 24- 28, 1995), GSCT #2 (May 30-June 14, 1995), GSCT #3 (September 12-22, 1995), and GSCT #4b (October 30-November 5, 1995). A small portion of the documentation for the above cited activities is appended.

Ipavich, Fred↗