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All sourcesNASA NTRSDOE OSTI
DOE OSTI2017

Multipoint Observations of Energetic Particle Injections and Substorm Activity During a Conjunction Between Magnetospheric Multiscale (MMS) and Van Allen Probes

Here, this study examines multipoint observations during a conjunction between Magnetospheric Multiscale (MMS) and Van Allen Probes on 7 April 2016 in which a series of energetic particle injections occurred. With complementary data from Time History of Events and Macroscale Interactions during Substorms, Geotail, and Los Alamos National Laboratory spacecraft in geosynchronous orbit (16 spacecraft in total), we develop new insights on the nature of energetic particle injections associated with substorm activity. Despite this case involving only weak substorm activity (maximum AE <300 nT) during quiet geomagnetic conditions in steady, below-average solar wind, a complex series of at least six different electron injections was observed throughout the system. Intriguingly, only one corresponding ion injection was clearly observed. All ion and electron injections were observed at <600 keV only. MMS reveals detailed substructure within the largest electron injection. A relationship between injected electrons with energy <60 keV and enhanced whistler mode chorus wave activity is also established from Van Allen Probes and MMS. Drift mapping using a simplified magnetic field model provides estimates of the dispersionless injection boundary locations as a function of universal time, magnetic local time, and L shell. The analysis reveals that at least five electron injections, which were localized in magnetic local time, preceded a larger injection of both electrons and ions across nearly the entire nightside of the magnetosphere near geosynchronous orbit. The larger ion and electron injection did not penetrate to L < 6.6, but several of the smaller electron injections penetrated to L < 6.6. Due to the discrepancy between the number, penetration depth, and complexity of electron versus ion injections, this event presents challenges to the current conceptual models of energetic particle injections.

58 GEOSCIENCES↗
DOE OSTI2017

Energetic Particle Data From the Global Positioning System Constellation

Abstract Since 2000, Los Alamos National Laboratory (LANL) Combined X‐ray and Dosimeter (CXD) and Burst Detector Dosimeter for Block II‐R (BDD‐IIR) instruments have been fielded on Global Positioning System (GPS) satellites. Today, 21 of the 31 operational GPS satellites are equipped with a CXD detector and a further 2 carry a BDD‐IIR. Each of these instruments measures a wide range of energetic electrons and protons. These data have now been publicly released under the terms of the Executive Order for Coordinating Efforts to Prepare the Nation for Space Weather Events. The specific goal of releasing space weather data from the GPS satellites is to enable broad scientific community engagement in enhancing space weather model validation and improvements in space weather forecasting and situational awareness. The time period covered by this data release is approximately 16 years, which corresponds to more than 167 satellite years of data. The large number of GPS satellites, distributed over six orbital planes, will provide important context for ongoing and historical science missions, as well as enabling new types of research not previously possible.

54 ENVIRONMENTAL SCIENCES↗
DOE OSTI2014

Artificial viscosity: back to the basics

Summary In this paper, we take a different perspective on the derivation of artificial viscosity. Heretofore, the development of artificial viscosity has been based on the paper published in Journal of Applied Physics in 1950 authored by John von Neumann and Robert Richtmyer [1]. Earlier, in 1948, Richtmyer published a report at Los Alamos Scientific Laboratory documenting the original concept [2]. This report was the true origin of shock capturing methods and contains several key ideas that are conceptually different than the 1950 journal article. Unfortunately, this report (LA‐671) was classified until 1993. This has resulted in two issues: the misattribution of the invention of artificial viscosity as primarily being the work of von Neumann and the loss of the structurally different ideas in the original report. We seek to right the record of history here and use the ideas contained in Richtmyer's report to good effect in deriving a new shock viscosity. The focus of previous development has been the Hugoniot curve describing the locus of states connected by a single shock wave. Here we follow a path more focused upon the Rayleigh line, which is strongly guided by Richtmyer's line of development of the original artificial viscosity formulation. We provide an implementation of the method resulting from this perspective and computational results for simple shock problems. Copyright © 2014 John Wiley & Sons, Ltd.

Mattsson, Ann E.↗
DOE OSTI2019

Total Recoverable Aluminum: Not Totally Relevant for Water Quality Standards

Abstract A large water quality data set, representing more than 100 surface-water locations sampled from 2007 to 2017 in the Los Alamos area of New Mexico, USA's Pajarito Plateau, was assembled to evaluate Al concentrations in unfiltered and filtered samples. Aluminum concentrations often exceeded United States Environmental Protection Agency (USEPA) and New Mexico ambient water quality criteria (AWQC), regardless of filter size and sample location. However, AWQC are based on laboratory toxicity studies using soluble Al salts and do not reflect natural conditions in Pajarito Plateau surface waters. The plateau is predominately covered by glassy and recrystallized volcanic ashes (e.g., Bandelier Tuff) containing colloidal to sand-sized aluminosilicates. Samples from natural background drainages and areas downstream of developed regions exhibited similar Al concentrations, suggesting that AWQC exceedances are caused by naturally elevated Al concentrations. Solubility calculations indicated that most samples were oversaturated with respect to amorphous Al(OH)3(s). Therefore, AWQC exceedances are likely artifacts of the “total recoverable” sample preparation, which includes acidification and partial digestion, thereby liberating nonbioavailable Al from aluminosilicates. Accordingly, Al concentrations were strongly associated with suspended sediment concentrations (SSCs), implying that aluminosilicates in suspended sediment contributed to AWQC exceedances and Al oversaturation. Solid-phase particle characterization, using X-ray diffraction (XRD) and scanning electron microscopy with electron dispersive spectroscopy (SEM/EDS) did not identify potentially bioavailable amorphous Al(OH)3(s) in any sample tested. Thus, current sample collection and analysis protocols should not be used to evaluate attainment of Al AWQC on the Pajarito Plateau or locations where aluminosilicates are substantial contributors to total recoverable Al. A sample preparation method (e.g., pH 4 extraction) capable of differentiating nonbioavailable and bioavailable forms of Al is recommended. Otherwise, current New Mexico and USEPA sample preparation approaches will continue to generate artifactual AWQC exceedances in surface waters that contain aluminosilicates. Integr Environ Assess Manag 2019;00:1–14. © 2019 SETAC

Ryan, Adam C.↗
DOE OSTI2016

Biostimulation and microbial community profiling reveal insights on RDX transformation in groundwater

Abstract Hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine (RDX) is a high explosive released to the environment as a result of weapons manufacturing and testing worldwide. At Los Alamos National Laboratory, the Technical Area (TA) 16 260 Outfall discharged high‐explosives‐bearing water from a high‐explosives‐machining facility to Cañon de Valle during 1951 through 1996. These discharges served as a primary source of high‐explosives and inorganic‐element contamination in the area. Data indicate that springs, surface water, alluvial groundwater, and perched‐intermediate groundwater contain explosive compounds, including RDX (hexahydro‐1,3,5‐trinitro‐1,3,5‐triazine); HMX (octahydro‐1,3,5,7‐tetranitro‐1,3,5,7‐tetrazocine); and TNT (2,4,6‐trinitrotoluene). RDX has been detected in the regional aquifer in several wells, and a corrective measures evaluation is planned to identify remedial alternatives to protect the regional aquifer. Perched‐intermediate groundwater at Technical Area 16 is present at depths from 650 ft to 1200 ft bgs. In this study, we examined the microbial diversity in a monitoring well completed in perched‐intermediate groundwater contaminated by RDX, and examined the response of the microbial population to biostimulation under varying geochemical conditions. Results show that the groundwater microbiome was dominated by Actinobacteria and Proteobacteria . A total of 1,605 operational taxonomic units (OTUs) in 96 bacterial genera were identified. Rhodococcus was the most abundant genus (30.6%) and a total of 46 OTUs were annotated as Rhodococcus . One OTU comprising 25.2% of total sequences was closely related to a RDX ‐degrading strain R. erythropolis HS4. A less abundant OTU from the Pseudomonas family closely related to RDX‐degrading strain P. putida II‐B was also present. Biostimulation significantly enriched Proteobacteria but decreased/eliminated the population of Actinobacteria . Consistent with RDX degradation, the OTU closely related to the RDX‐degrading P. putida strain II‐B was specifically enriched in the RDX‐degrading samples. Analysis of the accumulation of RDX‐degradation products reveals that during active RDX degradation, there is a transient increase in the concentration of the degradation products MNX, DNX, TNX, and NDAB. The accumulation of these degradation products suggests that RDX is degraded via sequential reduction of the nitro functional groups followed by abiotic ring‐cleavage. The results suggest that strict anaerobic conditions are needed to stimulate RDX degradation under the TA‐16 site‐specific conditions.

59 BASIC BIOLOGICAL SCIENCES↗
DOE OSTI2018

Synthesis and Evaluation of 3-Picrylamino-1,2,4-Triazole (PATO) Formulations

3–Picrylamino–1,2,4–triazole (PATO) is a thermally stable explosive invented at Los Alamos National Laboratory (LANL) almost half a century ago. Despite a rapid and high yielding synthesis, performance data for this promising explosive are scant. We prepared material using Coburn's synthesis, and discovered that the particle size distribution and morphology leads to difficulty in pressing formulations to high density. Three formulations were made using glycidyl azide polymer (GAP), FK–800, and Estane 5703/nitroplasticizer (NP) as binders. The maximum pressed density of these formulations was 89 % of theoretical maximum density (TMD). We determined detonation velocity and, for the FK–800 formulation, detonation pressure. Furthermore, the performance of PATO is similar to TATB at equivalent pressed density.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2021

An initial exploration of Bayesian model calibration for estimating the composition of rocks and soils on Mars

The Mars Curiosity rover carries an instrument, ChemCam, designed to measure the composition of surface rocks and soil using laser-induced breakdown spectroscopy (LIBS). The measured spectra from this instrument must be analyzed to identify the component elements in the target sample, as well as their relative proportions. This process, which we call disaggregation, is complicated by so-called matrix effects, which describe nonlinear changes in the relative heights of emission lines as an unknown function of composition due to atomic interactions within the LIBS plasma. In this work, we explore the use of the plasma physics code ATOMIC, developed at Los Alamos National Laboratory, for the disaggregation task. ATOMIC has recently been used to model LIBS spectra and can robustly reproduce matrix effects from first principles. The ability of ATOMIC to predict LIBS spectra presents an exciting opportunity to perform disaggregation in a manner not yet tried in the LIBS community, namely via Bayesian model calibration. However, using it directly to solve our inverse problem is computationally intractable due to the large parameter space and the computation time required to produce a single output. Therefore, we also explore the use of emulators as a fast solution for this analysis. We discuss a proof of concept Gaussian process emulator for disaggregating two-element compounds of sodium and copper. The training and test datasets were simulated with ATOMIC using a Latin hypercube design. After testing the performance of the emulator, we successfully recover the composition of 25 test spectra with Bayesian model calibration.

97 MATHEMATICS AND COMPUTING↗
DOE OSTI2020

Temperature response and brine availability to heated boreholes in bedded salt

Abstract There is a growing need for disposal of high‐level nuclear waste. To reduce uncertainty associated with brine availability to repository excavations in salt formations, a collaboration between Sandia, Los Alamos, and Lawrence Berkeley National Laboratories is performing a series of borehole‐scale coupled process tests. Here, we report on the first round of the Brine Availability Test in Salt (BATS) project, a “shakedown” experiment called Phase 1s. Experimental testing included placing a resistive heater, a 260‐W radiative heater, and a 750‐W radiative heater within previously drilled horizontal boreholes at the Waste Isolation Pilot Plant (WIPP) while monitoring temperature and water inflow. The experiments successfully achieved the targeted temperature of 120 °C when using the 750‐W radiative heater. Simulations using FEHM (Finite Element Heat and Mass transfer code) and TOUGH‐FLAC (Transport Of Unsaturated Groundwater and Heat–Fast Lagrangian Analysis of Continua) were able to accurately predict the coupled thermo–hydro–mechanical–chemical response of salt, matching the observed temperature and brine production. Due to the extremely low permeability of salt, these systems take many years to reach steady state when perturbed by mining activities. Long‐term numerical simulations are used to develop the initial pressure and saturation conditions. The inclusion of a damaged rock zone with higher permeability around the borehole also affects the saturation and pressure distributions and plays an important role in dissipating the potential for thermal pressurization. Knowledge gained from this round of experimentation and simulation will be used to conduct the next BATS project experiment in new boreholes at WIPP.

58 GEOSCIENCES↗
DOE OSTI2023

Analysis of Coronado State Historic Site artifacts using X‐rays

Abstract Two historic‐period metal artifacts were provided by the New Mexico Historic Sites to Los Alamos National Laboratory for non‐destructive analysis. The artifacts were a crossbow quarrel (or bolthead) and a reliquary pendant recovered from Kuaua Pueblo (also known as the Coronado Historic Site) in Bernalillo, NM. The quarrel is a heavily patinated metal that had been flattened due to compressive forces. The pendant consisted of a metal casing that had previously surrounded two center gemstones on the front and rear face of the pendant. The gemstone in the rear setting had fractured and was displaced from the setting, leaving only a small, loose fragment within the pendant for study. The front gem appeared to be very dark, near‐black in color, and the fragment of the rear gem was a bright red color. The artifacts were analyzed to ascertain their composition and glean insight into their provenance using the following X‐ray techniques: X‐ray computed tomography, confocal micro X‐ray fluorescence, and X‐ray diffraction. Infrared spectroscopy and electron microscopy were used on selected areas. Ultraviolet Raman spectra were collected on the two gems and the pendant. The metal material of the artifacts was found to be primarily composed of copper. The gems in the pendant were composed of manganese (front gem) and calcium (side gem).

36 MATERIALS SCIENCE↗
DOE OSTI2020

Magnesium Technology 2020

Magnesium and its alloys are being investigated widely for applications that require extraordinarily high strength-to-weight ratio, vibration damping, electromagnetic shielding, reduction in carbon footprint, sustainability improvements, and low toxicity. In the past decade or so, this drive has led to increased adoption of magnesium and its alloys in everyday products and it is no longer regarded as an esoteric material. The overarching goal of its widespread adoption and replacement of conventional materials such as steel and aluminum alloys has been restricted because of the cost of the material, limited sources of primary material, alloying constraints, high chemical reactivity, and challenges associated with its plasticity. Researchers, scientists, engineers, and economists from industry, government agencies and laboratories, and academic institutions alike are actively developing roadmaps for next-generation products and addressing these challenges as quickly as possible through unique and innovative methods. The TMS Magnesium Committee has been actively involved in providing a platform to these entities for disseminating the latest information, developments, and cutting-edge research and development, and showcasing the latest research and development trends related to magnesium and its alloys through the Magnesium Technology Symposium, which takes place every year at the TMS Annual Meeting. This proceedings volume retains the essence of this longstanding tradition. The twenty-first volume in the series, Magnesium Technology 2020, is the proceedings of the Magnesium Technology Symposium held during the 149th TMS Annual Meeting & Exhibition in San Diego, CA, February 23–27, 2020. The volume captures commentaries and papers from 15 different countries. The papers have been categorized systematically based on topics pertaining to magnesium production, casting and solidification, thermomechanical processing, deformation mechanisms, modeling, corrosion, and applications. The symposium began with keynote sessions that featured several distinguished invited speakers from government organizations and academia, who provided their perspectives on the state of the art, goals, and opportunities in magnesium alloy research and development. Dr. Carlos Tomé from Los Alamos National Laboratory, U.S. Department of Energy, discussed 3D characterization of mechanical twins across grain boundaries. This was followed by a talk on hierarchically structured ultrafine-grained magnesium alloys by Dr. Rajiv Mishra from the University of North Texas, USA, who presented an example of using friction stir additive manufacturing for implementing such microstructures at a component level. Dr. Mark Horstemeyer from Liberty University, USA, presented an overview of fatigue modeling to capture the corrosion-fatigue behavior of magnesium alloys. The final talk in this session was presented by Dr. Bin Jiang from Chongqing University, China, who presented a novel extrusion approach for achieving high-strength magnesium alloy plates.

Jordon, J. Brian↗
DOE OSTI2026

Prospects for exploring non-standard neutrino properties with argon-based CEvNS experiments

Coherent elastic neutrino-nucleus scattering (CEvNS) provides a powerful frame-work for testing the Standard Model (SM) and searching for new physics at low energies. In this work, we examine the prospects for argon-based CEvNS experiments at stopped-pion sources to perform precision measurements of weak interactions and probe non-standard neutrino properties. Our study focused on the CENNS-10 and CENNS-750 detectors at the Spallation Neutron Source at Oak Ridge National Laboratory, the Coherent Captain Mills (CCM) detector at Los Alamos National Laboratory, and the proposed PIP2-BD detector at Fermilab’s Facility for Dark Matter Discovery (F2D2). Using realistic neutrino fluxes and detector configurations corresponding to these facilities, we evaluate event rates and sensitivities to a range of observables. Within the SM, argon-based CEvNS detectors enable precision tests of electroweak parameters, including the weak mixing angle, at momentum transfers well below the electroweak scale. We also investigate the sensitivity of these experiments to neutrino electromagnetic properties, such as the magnetic moment and effective charge radius, as well as to possible non-standard neutrino interactions with quarks. Together, these studies highlight the potential of argon-based CEvNS experiments as a clean and versatile platform for precision exploration of non-standard neutrino properties.

Carey, Sam [Wayne State U.] (ORCID:000900029607531↗
DOE OSTI2017

3D Cosmic Ray Muon Tomography from an Underground Tunnel

Here, we present an underground cosmic ray muon tomographic experiment imaging 3D density of overburden, part of a joint study with differential gravity. Muon data were acquired at four locations within a tunnel beneath Los Alamos, New Mexico, and used in a 3D tomographic inversion to recover the spatial variation in the overlying rock–air interface, and compared with a priori knowledge of the topography. Densities obtained exhibit good agreement with preliminary results of the gravity modeling, which will be presented elsewhere, and are compatible with values reported in the literature. The modeled rock–air interface matches that obtained from LIDAR within 4 m, our resolution, over much of the model volume. This experiment demonstrates the power of cosmic ray muons to image shallow geological targets using underground detectors, whose development as borehole devices will be an important new direction of passive geophysical imaging.

3-D inversion↗
DOE OSTI2015

Quality assurance of temporal variability of natural decay chain and neutron induced background for low-level NORM analysis

In this study, twenty-one high purity germanium (HPGe) background spectra were collected over 2 years at Los Alamos National Laboratory. A quality assurance methodology was developed to monitor spectral background levels from thermal and fast neutron flux levels and naturally occurring radioactive material decay series radionuclides. 238 U decay products above 222 Rn demonstrated minimal temporal variability beyond that expected from counting statistics. 238 U and 232 Th progeny below Rn gas displayed at most twice the expected variability. Further, an analysis of the 139 keV 74 Ge(n, γ) and 691 keV 72 Ge(n, n') spectral features demonstrated temporal stability for both thermal and fast neutron fluxes.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
DOE OSTI2015

Determination of initial fuel state and number of reactor shutdowns in archived low-burnup uranium targets

This article presents a method for destructive analysis of irradiated uranium (U) targets, with a focus on collection and measurement of long-lived (t 1/2 > ~10 years) and stable fission product isotopes of ruthenium and cesium. Long-lived and stable isotopes of these elements can provide information on reactor conditions (e.g. flux, irradiation time, cooling time) in old samples (> 5–10 years) whose short-lived fission products have decayed away. The separation and analytical procedures were tested on archived U reactor targets at Los Alamos National Laboratory as part of an effort to evaluate reactor models at low-burnup.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2016

Preparation of iridium targets by electrodeposition for neutron capture cross section measurements

Here, the preparation of 191 Ir and 193 Ir electrodeposits for neutron capture cross-section measurements at the detector for advanced neutron capture experiments located at the at Los Alamos Neutron Science Center is described. The electrodeposition of iridium in the desired thickness of 0.4–1 mg/cm 2 is challenging. Better yields and thicknesses were obtained using electrodeposition from isopropyl alcohol solutions than from ammonium sulfate solutions. 191 Ir and 193 Ir targets were initially prepared using the standard single-sided electrodeposition cell. Iridium electrodepositions using a double-sided electrodeposition cell were developed and were optimized, resulting in thick, uniform iridium deposits. LA UR 15-22475.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2018

Comparison of the Davies and Gray titrimetric method with potassium dichromate and ceric titrants

The modified New Brunswick Laboratory (NBL) Davies and Gray titrimetry method uses potassium dichromate standard 136-f from the National Institute of Standards and Technology for calibration. However, the presence of chromium in the resulting waste stream makes the disposal of waste from this procedure costly. We report that the Actinide Analytical Chemistry (C-AAC) group at Los Alamos National Laboratory investigated and transitioned to a cerium based titrant as an alternative. We present the first long-term analytical study using this ceric-based titration method and compare it with NBL results based on the more-widely used dichromate titrimetric method.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
DOE OSTI2020

An interlaboratory collaboration to determine consensus 231 Pa/ 235 U model ages of a uranium certified reference material for nuclear forensics

Application of the 231 Pa/ 235 U radiochronometer for nuclear forensic investigations is challenged by a lack of certified reference materials with 231 Pa/ 235 U model purification dates. The Japan Atomic Energy Agency, Los Alamos National Laboratory, and Lawrence Livermore National Laboratory completed an interlaboratory study measuring 231 Pa/ 235 U model ages of New Brunswick Laboratory CRM U100. Results from independent laboratories were combined to calculate a consensus 231 Pa/ 235 U model purification date for CRM U100 of March 26, 1959 ± 237 days. This 231 Pa/ 235 U consensus date for CRM U100 may be used by the nuclear forensic community for quality control of 231 Pa/ 235 U radiochronometry measurements of unknown materials.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
DOE OSTI2020

International cooperation in age-dating uranium standards for nuclear forensics using the 231 Pa/ 235 U radiochronometer

During 2017–2018 Los Alamos National Laboratory, Lawrence Livermore National Laboratory and the China Institute of Atomic Energy collaborated in an interlaboratory 231 Pa/ 235 U radiochronometry exercise. The laboratories used different analytical methods to obtain a consensus model purification date for CRM U010 of December 28, 1958 ± 198 days and for CRM U850 of May 20, 1958 ± 363 days. These results agree with previously reported model dates using the 230 Th/ 234 U radiochronometer as well as the production histories of these materials. The concordance of interlaboratory data here confirms the ability of laboratories to make reproducible radiochronometry measurements using distinct analytical approaches.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗