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The Center for Momentum Transport and Flow Organization in Plasmas - Final Scientific Report

Overview of University of Colorado Efforts: The University of Colorado group has focused on two primary fronts during the grant period: development of a variety of multi-point diagnostic and/or imaging analysis techniques, and momentum-transport related experiments on a variety of devices (NSTX at PPPL, CSDX at UCSD, LAPD at UCLA, DIII-D at GA). Experimental work has taken advantage of several diagnostic instruments, including fast-framing cameras for imaging of electron density fluctuations (either directly or using injected gas puffs), ECEI for imaging of electron temperature fluctuations, and multi-tipped Langmuir and magnetic probes for corroborating measurements of Reynolds and Maxwell stresses. Mode Characterization in CSDX: We have performed a series of experiments at the CSDX linear device at UCSD, in collaboration with Center PI G. Tynan's group. The experiments included a detailed study of velocity estimation techniques, including direct comparisons between Langmuir probes and image-based velocimetry from fast-framing camera data. We used the camera data in a second set of studies to identify the spatial and spectral structure of coherent modes, which illuminates wave behavior to a level of detail previously unavailable, and enables direct comparison of dispersion curves to theoretical estimates. In another CSDX study, similar techniques were used to demonstrate a controlled transition from nonlinearly coupled discrete eigenmodes to fully developed broadband turbulence. The axial magnetic field was varied from 40-240 mT, which drove the transition. At low magnetic fields, the plasma is dominated by drift waves. As the magnetic field is increased, a strong potential gradient at the edge introduces an ExB shear-driven instability. At the transition, another mode with signatures of a rotation-induced Rayleigh–Taylor instability appears at the central plasma region. Concurrently, large axial velocities were found in the plasma core. For larger magnetic fields, all of the instabilities co-exist, leading to rich plasma dynamics and fully developed broadband turbulence. Edge-Turbulence and Flow Experiments in NSTX: A series of Gas Puff Imaging (GPI) observations on NSTX revealed a quasi-periodic oscillation in the plasma edge preceding the L-H transition in a limited set of neutral beam heated plasmas. These ~3 kHz flow oscillations exhibit both long wavelength and long correlation lengths, suggesting they are zonal-flow-like. The flow oscillations are strongly correlated with modulations of the level of edge turbulence, thus the system appears to undergo a predator--prey-type limit-cycle preceding the L-H transition. However, a clear trigger for the L-H transition was not observed. Reynolds stress profiles were obtained directly from image velocimetry for L-mode periods ELM-Precursor Studies in NSTX: A separate study based on NSTX-GPI data captured the two-dimensional evolution of edge-localized mode (ELM) precursors. Precursor events were observed preceding ELMs and ELM-induced H–L back-transitions in radio-frequency heated H-mode plasmas, and the growth of the precursor mode through the ELM filamentation was imaged in the plane perpendicular to the local B-field. Strong edge intensity modulations appeared to propagate in the electron diamagnetic direction while steadily drifting radially outwards. Intensity fluctuations were observed at frequencies around 20 kHz and wavenumbers of 0.05-0.2 cm -1 . Upon growing to a trigger point, precursor fluctuations were seen to form filamentary structures and move into the scrape-off layer (SOL) explosively with radial velocities peaking at 8 km/s. Once in the SOL, filaments reverse their propagation direction and travel in the ion diamagnetic direction. Edge intensity fluctuations were strongly correlated with magnetic signals from Mirnov coils, and toroidally distributed coils estimated toroidal mode numbers of n=5-10. Quantitatively similar precursors have been observed in ohmic H-mode plasmas as well, though significantly fewer events are seen in the ohmic cases and none were observed in the near-threshold NBI H-modes studied. Development of Velocimetry and Image Analysis Techniques: Along with the experiments listed above, the Colorado group has continued to explore various velocimetry techniques and their range of validity. We have developed a “linear optical flow” code, which calculates smooth velocity maps while accurately assessing local regions of high curl. This is critical for separating spatial scales of velocity behavior, and thus transport. This code has recently come on-line, and we are currently using it to revisit a number of older datasets. Additionally, we have worked on developing pattern-recognition techniques for imaging diagnostics, based on established digital image compression algorithms. This has the potential to open the analysis of turbulent plasma behavior beyond the well-trodden Fourier and wavelet approaches. Finally, we have extended several of these image-analysis routines to multiple other diagnostic sets, including GPI datasets in NSTX and ECEI imaging on DIII-D. In one study, correlation maps were used to measure the full 2-D mode structure of drift-wave level structures using ECEI for the first time. This enabled direct comparison to gyrokinetic simulations using the GEM code, from which is was determined that TEM modes were being measured in DIII-D.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Weak trimerization in the frustrated two-dimensional triangular Heisenberg antiferromagnet Lu y Y 1-y MnO 3

To understand the 2D triangular Heisenberg antiferromagnetic system, we investigated the magnetic structures and the dynamics of Lu y Y 1-y MnO 3 in detail. The substitutions are adjusted to the Mn atomic position close to x Mn =$\frac{1}{3}$. The neutron powder diffraction data claims that the magnetic structure of Lu y Y 1-y MnO 3 is described as a mixture of Γ 3 (P6' 3 cm') and Γ 4 (P6' 3 c'm) at the x Mn position for y=0.15, 0.30, and 0.45. The ratio of Γ 3 and Γ 4 depends on temperature and composition and the fraction of Γ 3 increases upon cooling, while no clear trimerization was observed at the xMn position. We estimated exchange parameters from the analysis of the low-energy part of the spin waves. The results showed a weak trimerization effect on cooling because the nearest-neighbor exchange interaction is slightly enhanced. The temperature dependence of the spin-wave dispersion around the Γ point shows that the spin gap closes with increasing temperature because the exchange interactions in the nearest Mn-Mn neighbor become smaller. Gapless diffusive magnetic excitation from a Mn triangular lattice has been observed in a wide range in Q and E space of Lu y Y 1-y MnO 3 . We found that Lu 0.3 Y 0.7 MnO 3 could be an ideal case to investigate the trimerization, frustrated magnetism, and magnetoelastic coupling often observed in two-dimensional triangular lattice Heisenberg antiferromagnet systems.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Spin wave modes in a cylindrical nanowire in crossover dipolar-exchange regime

Nanoscale magnetic systems have been studied extensively in various geometries, such as wires of different cross-sections, arrays of wires, dots, rings, etc. Such systems have interesting physical properties and promising applications in advanced magnetic devices. Uniform magnetic nanowires are the basic structures which were broadly investigated. However, some of their dynamical properties, like: (anti)crossing between the spin wave modes and impact of the magnetic field on the spin wave spectrum, still need to be exploited. We continue this research by investigation of the spin wave dynamics in solid Ni nanowire of the circular cross-section. We use two approaches: semi-analytical calculations and numerical computations based on the finite element method. We solve coupled Landau-Lifshitz and Maxwell equations and consider both dipolar and exchange interactions. We identify the dispersion brunches and their (anti)crossing by plotting the spatial profiles of spin wave amplitudes and magnetostatic potential. We also check how we can tune the spectrum of the modes by application of the external magnetic field and how it affects the modes and their dominating type of interaction.

magnonics↗

PARTICLE-IN-CELL SIMULATIONS OF PARTICLE ENERGIZATION VIA SHOCK DRIFT ACCELERATION FROM LOW MACH NUMBER QUASI-PERPENDICULAR SHOCKS IN SOLAR FLARES

Low Mach number, high beta fast mode shocks can occur in the magnetic reconnection outflows of solar flares. These shocks, which occur above flare loop tops, may provide the electron energization responsible for some of the observed hard X-rays and contemporaneous radio emission. Here we present new two-dimensional particle-in-cell simulations of low Mach number/high beta quasi-perpendicular shocks. The simulations show that electrons above a certain energy threshold experience shock-drift-acceleration. The transition energy between the thermal and non-thermal spectrum and the spectral index from the simulations are consistent with some of the X-ray spectra from RHESSI in the energy regime of E {approx}< 40 {approx} 100 keV. Plasma instabilities associated with the shock structure such as the modified-two-stream and the electron whistler instabilities are identified using numerical solutions of the kinetic dispersion relations. We also show that the results from PIC simulations with reduced ion/electron mass ratio can be scaled to those with the realistic mass ratio.

79 ASTRONOMY AND ASTROPHYSICS↗

Oxygen incorporation effects in annealed epitaxial La{sub (1-x)}Sr{sub x}MnO{sub 3} thin films

This paper presents our results regarding oxygen incorporation effects in epitaxial La{sub (1-x)}Sr{sub x}MnO{sub 3} thin films, deposited on SrTiO{sub 3} (001) single crystal substrates, by annealing in different gas mixtures of argon and oxygen. A particular emphasis is placed on the correlation of structural properties with the magnetic properties of the films, Curie temperature, and coercive field. In this sense, we demonstrate that the evolution of the diffuse part of the {omega}-scans performed on the films are due to oxygen excess in the film lattice, which creates cationic vacancies within the films. Also, we show that two regimes of oxygen incorporation in the films exist, one in which the films evolve toward a single phase and oxygen stoichiometry is recovered, and a second one dominated by oxygen over-doping effects. In order to support our study, XPS measurements were performed, from which we have evaluated the Mn{sup 3+}/Mn{sup 4+} ionic ratio.

36 MATERIALS SCIENCE↗

Hydrothermal synthesis of superparamagnetic Fe{sub 3}O{sub 4} nanoparticles with ionic liquids as stabilizer

Highlights: • Superparamagnetic Fe{sub 3}O{sub 4} nanoparticles with good dispersity have been synthesized via hydrothermal method. • Ionic liquid [C{sub 16}mim]Cl acts as stabilizer for the Fe{sub 3}O{sub 4} nanoparticles. • Fe{sub 3}O{sub 4} nanoparticles have a saturation magnetization of 67.69 emu/g at 300 K. - Abstract: Superparamagnetic Fe{sub 3}O{sub 4} nanoparticles have been successfully synthesized under hydrothermal condition with the assistant of ionic liquid 1-hexadecyl-3-methylimidazolium chloride ([C{sub 16}mim]Cl). The structure and morphology of the sample have been investigated by X-ray diffraction (XRD), X-ray photoelectron spectra (XPS), transmission electron microscopy (TEM), and high-resolution TEM (HRTEM), and the results indicate that the as-synthesized inverse spinel Fe{sub 3}O{sub 4} nanoparticles have an average diameter of about 10 nm and exhibit relatively good dispersity. More importantly, it is found that [C{sub 16}mim]Cl acts as stabilizer for the Fe{sub 3}O{sub 4} nanoparticles by adsorbing on the particles surfaces to prevent the agglomeration. In addition, the obtained superparamagnetic Fe{sub 3}O{sub 4} nanoparticles have a saturation magnetization of 67.69 emu/g at 300 K.

36 MATERIALS SCIENCE↗

The ion-ion hybrid Alfvén resonator in a fusion environment

An investigation is made of a shear Alfvén wave resonator for burning plasma conditions expected in the ITER device. For small perpendicular scale-lengths the shear mode, which propagates predominantly along the magnetic field direction, experiences a parallel reflection where the wave frequency matches the local ion-ion hybrid frequency. In a tokamak device operating with a deuterium–tritium fuel, this effect can form a natural resonator because of the variation in local field strength along a field line. The relevant kinetic dispersion relation is examined to determine the relative importance of Landau and cyclotron damping over the possible resonator parameter space. A WKB model based on the kinetic dispersion relation is used to determine the eigenfrequencies and the quality factors of modes trapped in the resonator. The lowest frequency found has a value slightly larger than the ion-ion hybrid frequency at the outboard side of a given flux surface. The possibility that the resonator modes can be driven unstable by energetic alpha particles is considered. It is found that within a bandwidth of roughly 600 kHz above the ion-ion hybrid frequency on the outboard side of the flux surface, the shear modes can experience significant spatial amplification. An assessment is made of the form of an approximate global eigenmode that possesses the features of a resonator. It is identified that magnetic field shear combined with large ion temperature can cause coupling to an ion-Bernstein wave, which can limit the instability.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Structure, dynamics, and deuterium fractionation of massive pre-stellar cores

High levels of deuterium fraction in N{sub 2}H{sup +} are observed in some pre-stellar cores. Single-zone chemical models find that the timescale required to reach observed values (D{sub frac}{sup N{sub 2}H{sup +}}≡N{sub 2}D{sup +}/N{sub 2}H{sup +}≳0.1) is longer than the free-fall time, possibly 10 times longer. Here, we explore the deuteration of turbulent, magnetized cores with 3D magnetohydrodynamics simulations. We use an approximate chemical model to follow the growth in abundances of N{sub 2}H{sup +} and N{sub 2}D{sup +}. We then examine the dynamics of the core using each tracer for comparison to observations. We find that the velocity dispersion of the core as traced by N{sub 2}D{sup +} appears slightly sub-virial compared to predictions of the Turbulent Core Model of McKee and Tan, except at late times just before the onset of protostar formation. By varying the initial mass surface density, the magnetic energy, the chemical age, and the ortho-to-para ratio of H{sub 2}, we also determine the physical and temporal properties required for high deuteration. We find that low initial ortho-to-para ratios (≲0.01) and/or multiple free-fall times (≳3) of prior chemical evolution are necessary to reach the observed values of deuterium fraction in pre-stellar cores.

79 ASTRONOMY AND ASTROPHYSICS↗

Dispersive Electron Cooling for JLEIC

JLEIC is the electron ion collider under design at Jefferson Lab, which will provide a luminosity up to 1034 cm-2s-1. To reach the high luminosity, short ion and electron bunches with high charge density colliding in high frequency are proposed in JLEIC design. The high charge density of the ion beam leads to strong intrabeam scattering effect, which enlarges the ion beam emittance and ruins the luminosity if not mitigated. Magnetized electron cooling is implemented to overcome the intrabeam scattering effect and to reduce or maintain the ion beam emittance. In this paper, we discuss the redistribution of the cooling effects in the longitudinal and the transverse directions by introducing the dispersion of the ion beam in the cooling section. When the charge density of the cooling electron beam varies, the dispersion of the ion beam leads to an increase of the transverse cooling rate and a reduction of the longitudinal cooling rate, while the total decrement of the Courant-Snyder invariant of the ion beam increases. Both theoretical analysis and numerical calculation are presented.

Zhang, He↗

The Effect of Ba Doping on the Structural, Optical, Magnetic, and Dielectric Properties of BiFeO{sub 3} Nanoparticles

Nanoparticles (Nps) of Ba (0, 1 to 5 at.%)-doped BiFeO{sub 3} were synthesized by a sol-gel route at 100 °C using tartaric acid as a chelating agent. The obtained results were studied by using XRD, SEM with EDAX, TEM, UV-vis diffusion reflectance spectra, VSM, and impedance analyzer. EDAX spectra confirmed the presence of Bi, Ba, and Fe in the samples. X-ray diffraction studies showed that BiFeO{sub 3} and Bi{sub 1−x}Ba{sub x}FeO{sub 3} samples exhibited the expected rhombohedral perovskite structure up to a Ba concentration of 3%, whereas 4 and 5% of Ba concentration exhibited the tetragonal phase. TEM studies indicate the particle sizes in the range of 08–28 nm. Reflectance spectra measurements showed a decrease in band gap with increasing Ba concentration. Magnetic properties indicated that the undoped BiFeO{sub 3} and Ba-doped BiFeO{sub 3} samples were ferromagnetic at room temperature. The dielectric constant (ε{sup ′}) and loss (ε{sup ″}) show large dispersion behavior. The dielectric constant increases with an increase of dopant concentration, but a very high value of the dielectric constant was noticed for x = 0.05.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Competing magnetic and nonmagnetic states in monolayer VSe 2 with charge density wave

The field of two-dimensional ferromagnets has been reinvigorated by the discovery of VSe 2 monolayer grown on van der Waals substrates, which is reported to be ferromagnetic with a Curie point higher than 330 K. However, the ferromagnetic and nonmagnetic states of pristine monolayer VSe 2 are highly debated. Here, employing density functional theory, Wannier function calculations, and the band unfolding method, we explore the electronic structure of monolayer VSe 2 with a $\sqrt{3} × \sqrt{7}$ charge density wave (CDW). Certain qualitative aspects of the calculated unfolded band dispersion and unfolded Fermi surface of monolayer VSe 2 with the $\sqrt{3} × \sqrt{7}$ CDW in the nonmagnetic state agree well with previous angle-resolved photoemission spectroscopy results, albeit with uncertainty about whether these experiments probed single or multiple domains. Specifically, we find that an isolated CDW domain naturally induces a strong breaking of the threefold symmetry of the electronic structure. In addition we find that, relative to the undistorted structure, the CDW structure shows a strong competition between nonmagnetic and various magnetic states, with an energy difference less than 5 meV/f.u. For the CDW structure in the antiferromagnetic state, the band dispersions and Fermi surface are similar to those in the nonmagnetic state, while the unfolded bands of the ferromagnetic CDW state display a sizable exchange splitting. These results indicate the possibility of various antiferromagnetic fluctuations in VSe 2 to coexist and compete with ferromagnetic order and the experimentally reported CDW order. In this work, our calculations build insights for exploring the interplay between magnetism and CDW behaviors more generally in transition metal dichalcogenides.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Facile scalable synthesis of Co{sub 3}O{sub 4}/carbon nanotube hybrids as superior anode materials for lithium-ion batteries

Graphical abstract: Co{sub 3}O{sub 4}/MWCNT hybrids were synthesized via strong ultra-sonication assisted shaking processes. The resultant samples as anode electrode display enhanced cycling performance and rate capability compared with pure Co{sub 3}O{sub 4} particle. - Highlights: • Co{sub 3}O{sub 4}/MWCNT hybrids were synthesized via ultra-sonication assisted shaking process. • The resulting Co{sub 3}O{sub 4} nanoparticles are highly dispersed onto MWCNT network backbone. • Co{sub 3}O{sub 4}/MWCNT hybrid displays highly enhanced lithium storage properties. • The present synthetic approach is facile, controllable, and scalable. - Abstract: In this report, Co{sub 3}O{sub 4}/multiple-wall carbon nanotube (MWCNT) hybrid materials were synthesized via strong ultrasonication-assisted shaking and magnetic stirring processes. The prepared samples were well characterized by utilizing powder X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and Raman spectroscopy techniques. Results indicated that the resulting Co{sub 3}O{sub 4} nanoparticles were highly dispersed in the MWCNT network backbone and further form Co{sub 3}O{sub 4}/MWCNT hybrid materials. The obtained Co{sub 3}O{sub 4}/MWCNT hybrids can be employed as anode electrode in Lithium-ion batteries and deliver as high as discharge capacity of 1250 mA h g{sup −1} at a current density of 0.2 C, additionally, 81% of the discharge capacity for sample 2 with 20 wt.% MWCNT loading could be retained after 70 cycles, which could be associated with the specific hybrid structure of the electrode as well as the addition of MWCNT. Most importantly, the present synthetic approach is facile, controllable, and scalable, which allowing it more easily adapted to prepare other hybrid materials with specific architectures.

36 MATERIALS SCIENCE↗

Coupled modes in magnetized dense plasma with relativistic-degenerate electrons

Low frequency electrostatic and electromagnetic waves are investigated in ultra-dense quantum magnetoplasma with relativistic-degenerate electron and non-degenerate ion fluids. The dispersion relation is derived for mobile as well as immobile ions by employing hydrodynamic equations for such plasma under the influence of electromagnetic forces and pressure gradient of relativistic-degenerate Fermi gas of electrons. The result shows the coexistence of shear Alfven and ion modes with relativistically modified dispersive properties. The relevance of results to the dense degenerate plasmas of astrophysical origin (for instance, white dwarf stars) is pointed out with brief discussion on ultra-relativistic and non-relativistic limits.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗

Violation of Field Line Conservation and Associated Spatial Scales in Particle-in-Cell Simulations and MMS Data

For the first time, space flight technology exists to detect, in situ, violation of magnetic field line conservation. The violation of magnetic line conservation on scales smaller than the system size is a necessary and sufficient condition for finite magnetic field reconnection. We demonstrate that violation of line conservation produces a detectable, structured signature both in particle-in-cell simulations of reconnection and in data from the Magnetospheric Multi-Scale mission. In particle-in-cell simulations of asymmetric reconnection, the quantity—which we call M—that identifies this violation achieves significant values in electron skin depth-scale layers that extend away from the separator, with higher values emerging on the low-density, high-magnetic-field side of the current sheet. At the separator, M owes largely to perpendicular gradients in the parallel electric field, while it attains its highest values away from the separator in dispersed, layered structures associated with gradients in the perpendicular nonideal electric field and electron transport. Sub-ion scale bipolar forms of the quantity also appear further from the separator. In two MMS burst data intervals detecting the electron diffusion region, we find that M exceeds measurement uncertainties both at the separator and near the separatrices. One interval has highly sheared reconnecting fields and the other a stronger guide field. For one event, we determine the location and scale of M and the inner electron diffusion region relative to electron outflows and the magnetic separatrices. The measure can therefore serve as a potent diagnostic for magnetic reconnection in space measurements.

79 ASTRONOMY AND ASTROPHYSICS↗

Violation of Field Line Conservation and Associated Spatial Scales in Particle-In-Cell Simulations and MMS Data

For the first time, space flight technology exists to detect, in situ, violation of magnetic field line conservation. The violation of magnetic line conservation on scales smaller than the system size is a necessary and sufficient condition for finite magnetic field reconnection. We demonstrate that violation of line conservation produces a detectable, structured signature both in particle-in-cell simulations of reconnection and in data from the Magnetospheric Multi-Scale mission. In particle-in-cell simulations of asymmetric reconnection, the quantity-which we call M-that identifies this violation achieves significant values in electron skin depth-scale layers that extend away from the separator, with higher values emerging on the low-density, high-magnetic-field side of the current sheet. At the separator, M owes largely to perpendicular gradients in the parallel electric field, while it attains its highest values away from the separator in dispersed, layered structures associated with gradients in the perpendicular nonideal electric field and electron transport. Sub-ion scale bipolar forms of the quantity also appear further from the separator. In two MMS burst data intervals detecting the electron diffusion region, we find that M exceeds measurement uncertainties both at the separator and near the separatrices. One interval has highly sheared reconnecting fields and the other a stronger guide field. For one event, we determine the location and scale of M and the inner electron diffusion region relative to electron outflows and the magnetic separatrices. The measure can therefore serve as a potent diagnostic for magnetic reconnection in space measurements.

Wendel, Deirdre E.↗

Magnetic Studies of Mutiferroic Bi{sub 1-x}La{sub x}FeO{sub 3} Ceramics Synthesized By Solution Combustion Technique

Bi{sub 1-x}La{sub x}FeO{sub 3} (x = 0.0, 0.05, 0.10, 0.15) ceramic samples were prepared by solution combustion technique. X-ray diffraction patterns confirmed the formation of perovskite structured Bi{sub 1-x}La{sub x}FeO{sub 3} phase. Saturation magnetization (M{sub s}) increases with increasing La concentration from x = 0.0 to x = 0.15. Weak ferromagnetism is observed at room temperature in all the doped and undoped BFO samples. Mossbauer spectroscopy confirmed the presence of single-phase material for the doped compositions. Improvement in magnetic behavior appears to arise from a combination of the propensity of the samples to form pure phase material, partial destruction of spin cycloids and increased canting of spins.

36 MATERIALS SCIENCE↗

Discrete breakup arcs and kinetic Alfven waves

Attention is confined to the extremely narrow auroral structures whose characteristic dimensions perpendicular to the magnetic fields are of the order of several hundred meters or even less. The starting point of the model used here is the assumption that discrete breakup arcs are caused by a change in the magnetosphere convection pattern that is localized in space. Particular attention is given to the shear Alfven mode. It is proposed that discrete breakup arcs are a direct manifestation of kinetic interaction between charged particles and an 'mhd' perturbation. It is stressed that the model applies only to narrow structures (thickness of the order of the plasma skin depth) and to short-lived phenomena (time scales shorter than a dispersion time). It is shown that a change of convection pattern in a spatially limited region leads to the emission of a shear-Alfven wave packet which propagates along the magnetic field line with a characteristic velocity.

Goertz, C. K.↗

Single-Grain Bulk YBa{sub 2}Cu{sub 3}O{sub y} Superconductor Grown in Shorter Duration by IG Process

The top-seeded infiltration growth (IG) process is considered to be an attractive, well-established route compared to melt growth (MG) process due to its successful ability to resolve observed problems in MG process such as pores, shrinkage, and an ununiformed Y{sub 2}BaCuO{sub 5} (Y-211) secondary phase particle dispersion in Y-123 matrix. This is among the first accounts of superconductivity where a large grain YBa{sub 2}Cu{sub 3}O{sub y} (Y-123) was produced by IG process. Further, by utilizing homemade Y-123 and Y-211, we had prepared YBa{sub 2}Cu{sub 3}O{sub y} samples via Y-123 + liquid (1:1) as a liquid source and had further characterized by utilizing the scanning electron microscopy (SEM), superconducting transition temperature (T{sub c}), and critical current density (J{sub c}) at 77 K. Here, we provide temperature dependence of magnetization measurements that indicated a sharp superconducting transition with T{sub c} (onset) around 92 K. In addition, the critical current density was calculated on the basis of Bean’s model and resulted as 30,000 A/cm{sup 2} at 77 K (self-field), H//c-axis. Trapped field experiments had lucidly indicated that single-grain nature with maximum-trapped field of 0.3 T at 77 K and 1 mm above sample surface even samples are produced shorter duration, i.e., 50 h.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗