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NASA NTRSDate not supplied

Integral Channel Nozzles and Heat Exchangers using Additive Manufacturing Directed Energy Deposition NASA HR-1 Alloy

Heat exchangers for use in propulsion applications are very critical components because they must be efficient, compact and light and often operate with working fluids at extreme temperatures or pressures or both. Various components and systems use heat exchangers such as combustion chambers of gas turbines and internal combustion engines, fuel cells (air supply and thermal management), electric batteries (thermal management), evaporators and recuperators of waste-heat-to-power systems, and rocket engines. Even if the results are more generally applicable, the heat exchangers applications to which this study is more closely related are regeneratively cooled rocket nozzles and chambers, and repressurization systems for the launch vehicles. These components are often thin-walled and contain pressurized fluids, like propellants at cryogenic or elevated temperatures. Given that the environments that these propulsion components must endure are challenging, the manufacturing to meet these specifications often require long lead times due to specialty processes and unique tooling associated with the combined thin-wall integral channel and large-scale structures. Additive manufacturing (AM) offers programmatic advantages for reduction in processing time and cost in addition to various technical advantages, including the possibility to achieve enhanced hardware complexity targeted to superior performance, part consolidation, and the capability of processing of novel alloys. While AM is already being utilized for heat exchanger components in propulsion applications, almost all these AM components are made by means of Laser Powder Bed Fusion (L-PBF). L-PBF allows for fine features but is rather limited with respect to the overall size of the components that can be manufactured. Recent developments are maturing the Laser Powder Directed Energy Deposition (LP-DED) process which may be used, for example, to make integral channel thin-wall regeneratively-cooled rocket nozzles with diameters greater than 1 m. This paper highlights some integral channel heat exchanger demonstrator hardware applications of LP-DED, as well as the characterization of this process in combination with the use of the NASA HR-1 alloy. To properly utilize LP-DED for heat exchanger manufacturing, various aspects are being characterized such as geometry limitations, measurement of surface texture and geometric angled surfaces, surface enhancements for internal channels, and material evaluation. NASA HR-1 (FeNi-Cr) is a high strength hydrogen resistant superalloy developed for use in aerospace applications, such as heat exchangers. Some aspects and considerations about the design of heat exchangers are summarized together with data relevant to LP-DED manufacturing in combination with the NASA HR-1 alloy. Microchannels were successful deposited down to 2.54 mm and 1 mm wall thickness, wall angles of 30°, both with high reproducibility. It was also found that the areal surface roughness is highly dependent on the size of the powder feedstock used for deposition. The characterization of these LP-DED features is critical for fluid flow and heat transfer predictions as it can be exploited to enhance heat transfer at the cost of increased pressure drop.

additive manufacturing↗

NASA NTRS1980

Selective optical coatings for solar collectors

For best performance, energy-absorbing surface of solar collector should be characterized by high ratio of solar absorptance to thermal emitance. Report on optical characteristics of several chemical treatments and electrodeposited coatings for metal solar-absorbing surfaces should interest designers and users of solar-energy systems. Moisture resistance of some coatings is also reported.

Lowery, J. R.↗

NASA NTRS1988

Interfaces in polymer, ceramic, and metal matrix composites; Proceedings of the Second International Conference on Composite Interfaces (ICCI-II), Cleveland, OH, June 13-17, 1988

The present conference on interfacial factors in advanced composite materials discusses such topics in their development status and properties as silane coupling, the electrochemical and plasma-surface treatment of carbon fibers, fiber surface-analytical techniques, polymer molecular scale characterization by atom-probe field-ion microscopy, the study of carbon fiber-epoxy resin interface interactions by means of labeling techniques, and the surface tailoring of SiC by ion implantation. Also discussed are developments in laser light-scattered photoelasticity, microstructural evolutions under heat treatment and radiation damage, TEM for composites, the interfaces of carbon fiber-reinforced Al composites, the influence of the interface on macroscopic composite properties, and the status of the theoretical understanding of composite interfaces.

Ishida, Hatsuo↗

NASA NTRS2014

Importance of Geodetically Controlled Topography to Constrain Rates of Volcanism and Internal Magma Plumbing Systems

Investigation of lava flow deposits is a key component of Investigation II.A.1 in the VEXAG Goals, Objectives and Investigations. Because much of the Venus surface is covered in lava flows, characterization of lava flow emplacement conditions(eruption rate and eruption duration) is critical for understanding the mechanisms through which magma is stored and released onto the surface as well as for placing constraints on rates of volcanic resurfacing throughout the geologic record preserved at the surface.

GEODETICALLY↗

NASA NTRS2021

Assessing Relay Communications for Mars Sample Return Surface Mission Concepts

The Mars Sample Return (MSR) Campaign would be a 3-mission campaign concept supported by NASA and ESA to return samples from the Mars surface. MSR would, for the first time ever, present a need to communicate with multiple surface assets that are co-located on Mars in a coordinated effort to accomplish the unified objective of fetching, transporting, and returning samples from Mars. Currently, Mars surface assets relay data to and from Earth using a number of orbiters in what’s known as the Mars Relay Network (MRN). This network is characterized by a small number of surface assets distributed across the Martian globe and a larger number of orbiters to provide relay services. As of June 2020, there are two surface assets for which five orbiters are providing relay. During the MSR Campaign, there would be two rovers and a lander that all would require relay communication from a small number of Mars orbiters to meet the aggressive MSR timeline. The inversion of the current MRN paradigm, a system of many surface assets requiring relay and few orbiters to provide relay, necessitates the unique challenge of optimally allocating relay passes to maximize the operational capability of all assets. The allocation must consider a large number of trade variables including Mars asset operational requirements and Earth ground system constraints, including staffing schedules, operations planning across time zones, and more. To address these telecommunication challenges, the Mars Asset Relay Mission Link Allocation Design Environment (MARMLADE) tool was developed. It is a MATLAB-based tool to assign orbiter passes or Direct-From-Earth (DFE) links to each of the three surface assets and quantify the operational efficiency of each surface asset.MARMLADE uses a data set of simulated Mars relay orbiter geometry and telecommunication capabilities provided by JPL’s Telecom Orbit Analysis and Simulation Tool (TOAST) software to compute which asset should get each pass based on a series of heuristics and predictions of all assets’ states. Within MARMLADE, the user can provide inputs including the option for time-based pass splitting, fixed FWD data rate capabilities, DFE communication capabilities, and link parameters allowing for the assessment of complex operations and hardware trades using surface mission operational efficiency as a primary figure of merit. As the MSR mission concepts continue to mature, MARMLADE is being used to assess ability of all MSR elements to meet the surface mission timeline requirements and to provide relay link allocations to each of the MSR surface assets.This paper will describe the motivation and design of the MARMLADE tool and how it is being used to perform campaign and mission level trades, generate requirements, and support development of the MSR surface mission scenarios.

Lee, Charles↗

DOE OSTI2025

Variability of Eastern North Atlantic Summertime Marine Boundary Layer Clouds and Aerosols Across Different Synoptic Regimes Identified With Multiple Conditions

Abstract This study estimates the meteorological covariations of aerosol and marine boundary layer (MBL) cloud properties in the eastern North Atlantic (ENA) region, characterized by diverse synoptic conditions. Using a deep‐learning‐based clustering model with mid‐level and surface daily meteorological data, we identify seven distinct synoptic regimes during the summer from 2016 to 2021. Our analysis, incorporating reanalysis data and satellite retrievals, shows that surface aerosols and MBL clouds exhibit clear regime‐dependent characteristics, whereas lower tropospheric aerosols do not. This discrepancy likely arises from synoptic regimes determined by daily large‐scale conditions, which may overlook air mass histories that predominantly dictate lower tropospheric aerosol conditions. Focusing on three regimes dominated by northerly winds, we analyze the Atmospheric Radiation Measurement Program (ARM) ENA observations on Graciosa Island in the Azores. In the subtropical anticyclone regime, fewer cumulus clouds and more single‐layer stratocumulus clouds with light drizzle are observed, along with the highest cloud droplet number concentration (Nd), surface cloud condensation nuclei (CCN) and surface aerosol levels. The post‐trough regime features more broken or multi‐layer stratocumulus clouds with slightly higher surface rain rate, and lower Nd and surface CCN levels. The weak trough regime is characterized by the deepest MBL clouds, primarily cumulus and broken stratocumulus clouds, with the strongest surface rain rate and the lowest Nd, surface CCN and surface aerosol levels, indicating strong wet scavenging. These findings highlight the importance of considering the covariation of cloud and aerosol properties driven by large‐scale regimes when assessing aerosol indirect effects using observations.

54 ENVIRONMENTAL SCIENCES↗

NASA NTRS1980

Carbonaceous chondrites. II - Carbonaceous chondrite phyllosilicates and light element geochemistry as indicators of parent body processes and surface conditions

Petrographic analyses of CM matrices characterized four phyllosilicates in Murray and Murchison meteorites and Fe- and Mg-serpentines in Nogoya. All phyllosilicates and bulk matrices show enrichment of K relative to Na when compared with bulk meteorites; the loss of Na and some Cl, and the addition of H2O, CO2, and water-soluble organics during alteration indicates a partially open system. Synthesis of soluble organic materials may have occurred in CM matrices before aqueous alteration of the precursive phases. Nogoya was 95% altered and has a bulk C content of 5.2%, higher than any meteorite; also, it has the lowest measured C-13/C-12 ratio of any carbonaceous chondrite except for Karoonda.

Bunch, T. E.↗

NASA NTRS2024

Morphometric Characterization of Lunar Landing Sites

As ambitious surface exploration of the Moon commences in the 2020s, it is important to develop reliable and objective metrics for understanding the quality of future landing sites. A key prerequisite for any exploration and utilization of the lunar surface is a safe landing. One of the most important methods to provide understanding of potential metrics for landing site safety in the lunar context is the systematic comparison of candidate and historic landing sites. The goal of this project is to determine the morphometric parameters of the lunar surface at 16 successful lunar landing sites where adequate data exists to execute a quantitative comparison using various parameters. Quantitative analysis of Lunar Reconnaissance Orbiter (LRO) data should inform mission planning activities by providing morphologic metrics for landing sites including slope, Terrain Ruggedness Index (TRI), and rock abundance. These comparisons will assist mission planners and exploration scientists by providing “calibration points” for using Lunar Reconnaissance Orbiter (LRO) data to successfully plan and execute lunar powered descents in the future. The metrics included in this analysis describe the form of the terrain and can be calculated for any potential future landing site. Another objective of this project is to determine how the derived morphologic parameters for the same landing site change between common pixel scales. In ideal lighting conditions, 2m/px Narrow Angle Camera Digital Terrain Models (NAC DTMs) can be assembled using stereoscopic imagery from two or more concentric orbits of the LRO. However, due to low light conditions near the lunar poles, the highest quality data for many potential lunar landing sites comes from the Lunar Orbiter Laser Altimeter (LOLA). Therefore, we seek to assess how the derived slope and TRI values change as a function of changes in the DTM postings from 2m/px to 5m/px.

J M McCallion↗

DOE OSTI2021

Multiple Reaction Pathways for the Oxygen Evolution Reaction May Contribute to IrO 2 (110)’s High Activity

Density functional theory calculations in conjunction with statistical mechanical arguments are performed on the rutile IrO 2 (110) facet in order to characterize multiple reaction pathways on the surface at the highest active limit (the stoichiometric surface with all metal sites available) and at the lowest active limit (the oxygen-terminated surface). Alternative pathways to the oxygen evolution reaction (OER) are found, with multiple pathways determined at each step of the four proton-coupled electron transfer reaction. Of particular interest is the detailed characterization of a co-adsorption pathway utilizing neighboring, adsorbed O, OH species in order to evolve oxygen; activation energies of this pathway are <0.5 eV and therefore easily surmountable at the high operating potentials of OER. We also determined that surface Ir atoms can potentially participate in deprotonating an OOH* intermediate; the activation energy to this is 0.67 eV on the oxygen-terminated surface. These theoretical findings explain in part the high activity present in iridium oxide catalysts and also provide insight into the mechanistic pathways available on metal oxide catalysts, which may require the concerted interaction of nearest neighbor co-adsorbates to produce chemicals of interest.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

NASA NTRS1985

Classification of Circular Features on Venus

Among the unanswered questions concerning Venus are the age of its surface and the mechanisms of lithospheric heat transfer (conduction, plate recycling, and hot spot volcanism). If there is a large population of impact craters, then the surface is ancient and Venus is characterized by conduction like the Moon, and Mercury, rather than plate recycling and hot spot volcanism. Alternatively, if there is a large population of volcanic craters, then the surface is younger and other mechanisms of heat transfer likely dominate. Previous studies have emphasized various aspects of the observational, theoretical, experimental, and comparative planetological studies of cratering on Venus, and several have reached divergent opinions concerning the age of the Venus surface. A major source of uncertainty in previous studies is the possible inclusion of circular features of nonimpact (volcanic or tectonic) origin in the so called impact crater population. A classification scheme of circular features on Venus is developed in order to further distinguish their origin and distribution.

Stofan, E. R.↗

NASA NTRS1993

Study of atmospheric and bidirectional effects on surface reflectance and vegetation index time series: Application to NOAA AVHRR and preparation for future space missions

The objectives of the investigation, namely 'to characterize the atmospheric and directional effects on surface reflectance and vegetation index using the First International Satellite Cloud Climatology Project (ISLCSP) Field Experiment (FIFE) data set, develop new algorithms to obtain better Advanced Very High Resolution Radiometer (AVHRR) indices, and define possible improvements for future satellite missions', were addressed in three separate, yet complementary studies. First, it was shown, from theoretical calculations, that visible and near infrared reflectances combined linearly at optimum (one or two) viewing angles relate linearly to the fraction of photosynthetically available radiation absorbed by plants, f(sub par), can be used independently of the type of foliage and substrate, eliminate the effects of sub-pixel spatial heterogeneity, and improve the accuracy of the f(sub par) estimates when compared to the Normalized Difference Vegetation Index, NDVI. Second, it was demonstrated that NDVI, even though it is not a linear combination of radiances or reflectances, can be spatially integrated without significant loss of information from scales of 300 to 1000 m. Third, AVHRR visible and near-infrared reflectances over the FIFE site, separating temporal and bidirectional components and determining the model parameters through an original iterative scheme was successfully modeled. It appears that NDVI generated from the top-of-atmosphere reflectances normalized by the bidirectional effects (as determined in the scheme) is a better vegetation index than maximum NDVI. Details about the three studies are presented.

Frouin, Robert↗

NASA NTRS2010

Projected Applications of a "Climate in a Box" Computing System at the NASA Short-Term Prediction Research and Transition (SPoRT) Center

The NASA Short-term Prediction Research and Transition (SPoRT) Center focuses on the transition of unique observations and research capabilities to the operational weather community, with a goal of improving short-term forecasts on a regional scale. Advances in research computing have lead to "Climate in a Box" systems, with hardware configurations capable of producing high resolution, near real-time weather forecasts, but with footprints, power, and cooling requirements that are comparable to desktop systems. The SPoRT Center has developed several capabilities for incorporating unique NASA research capabilities and observations with real-time weather forecasts. Planned utilization includes the development of a fully-cycled data assimilation system used to drive 36-48 hour forecasts produced by the NASA Unified version of the Weather Research and Forecasting (WRF) model (NU-WRF). The horsepower provided by the "Climate in a Box" system is expected to facilitate the assimilation of vertical profiles of temperature and moisture provided by the Atmospheric Infrared Sounder (AIRS) aboard the NASA Aqua satellite. In addition, the Moderate Resolution Imaging Spectroradiometer (MODIS) instruments aboard NASA s Aqua and Terra satellites provide high-resolution sea surface temperatures and vegetation characteristics. The development of MODIS normalized difference vegetation index (NVDI) composites for use within the NASA Land Information System (LIS) will assist in the characterization of vegetation, and subsequently the surface albedo and processes related to soil moisture. Through application of satellite simulators, NASA satellite instruments can be used to examine forecast model errors in cloud cover and other characteristics. Through the aforementioned application of the "Climate in a Box" system and NU-WRF capabilities, an end goal is the establishment of a real-time forecast system that fully integrates modeling and analysis capabilities developed within the NASA SPoRT Center, with benefits provided to the operational forecasting community.

Jedlovec, Gary J.↗

NASA NTRS2009

Power Spectral Density Specification and Analysis of Large Optical Surfaces

The 2-dimensional Power Spectral Density (PSD) can be used to characterize the mid- and the high-spatial frequency components of the surface height errors of an optical surface. We found it necessary to have a complete, easy-to-use approach for specifying and evaluating the PSD characteristics of large optical surfaces, an approach that allows one to specify the surface quality of a large optical surface based on simulated results using a PSD function and to evaluate the measured surface profile data of the same optic in comparison with those predicted by the simulations during the specification-derivation process. This paper provides a complete mathematical description of PSD error, and proposes a new approach in which a 2-dimentional (2D) PSD is converted into a 1-dimentional (1D) one by azimuthally averaging the 2D-PSD. The 1D-PSD calculated this way has the same unit and the same profile as the original PSD function, thus allows one to compare the two with each other directly.

wavefront↗

DOE OSTI2021

Spontaneous dynamical disordering of borophenes in MgB2 and related metal borides

Abstract Layered boron compounds have attracted significant interest in applications from energy storage to electronic materials to device applications, owing in part to a diversity of surface properties tied to specific arrangements of boron atoms. Here we report the energy landscape for surface atomic configurations of MgB 2 by combining first-principles calculations, global optimization, material synthesis and characterization. We demonstrate that contrary to previous assumptions, multiple disordered reconstructions are thermodynamically preferred and kinetically accessible within exposed B surfaces in MgB 2 and other layered metal diborides at low boron chemical potentials. Such a dynamic environment and intrinsic disordering of the B surface atoms present new opportunities to realize a diverse set of 2D boron structures. We validated the predicted surface disorder by characterizing exfoliated boron-terminated MgB 2 nanosheets. We further discuss application-relevant implications, with a particular view towards understanding the impact of boron surface heterogeneity on hydrogen storage performance.

36 MATERIALS SCIENCE↗

NASA NTRS1979

Definition of mutually optimum NDI and proof test criteria for 2219 aluminum pressure vessels. Volume 3: Applications to rail defect evaluation

The technique for inspection of railroad rails containing transverse fissure defects was discussed. Both pulse-echo and pitch-catch inspection techniques were used. The pulse-echo technique results suggest that a multiple-scan approach using varying angles of inclination, three-surface scanning, and dual-direction traversing may offer promise of characterization of transverse defects. Because each scan is likely to produce a reflection indicating only a portion of the defect, summing of the individual reflections must be used to obtain a reasonably complete characterization of the defect. The ability of the collimated pitch-catch technique to detect relatively small amounts of flaw growth was shown. The method has a problem in characterizing the portions of the defect near the top surface or web intersection. The work performed was a preliminary evaluation of the prospects for automated mapping of rail flaws.

Schwartzberg, F. R.↗

NASA NTRS1992

Measurment Of Residual Stress In Ferromagnetic Materials

Magnetoacoustic (MAC) and magnetoacoustic emission (MAE) techniques combined to provide complete characterization of residual stresses in ferromagnetic structural materials. Combination of MAC and MAE techniques makes it possible to characterize residual tension and compression without being limited by surface conditions and unavailability of calibration standards. Significant in field of characterization of materials as well as detection of fatigue failure.

Namkung, Min↗

DOE OSTI2020

Surface Modification of a MXene by an Aminosilane Coupling Agent

MXenes, two–dimensional (2D) transition metal carbides and/or nitrides, possess surface termination groups such as hydroxyl, oxygen, and fluorine, which are available for surface functionalization. Their surface chemistry is critical in many applications. This article reports amine functionalization of Ti 3 C 2 T x MXene surface with [3–(2–aminoethylamino)–propyl]trimethoxysilane (AEAPTMS). Characterization techniques such as X–ray photoelectron spectroscopy verify the success of the surface functionalization and confirm that the silane coupling agent bonds to Ti 3 C 2 T x surface both physically and chemically. The functionalization changes the MXene surface charge from –35 to +25 mV at neutral pH, which allows for in situ preparation of self–assembled films. Further, surface charge measurements of the functionalized MXene at different pH values show that the functionalized MXene has an isoelectric point at a pH around 10.7, and the highest reported positive surface charge of +62 mV at a pH of 2.58. Furthermore, the existence of a mixture of different orientations of AEAPTMS and the simultaneous presence of protonated and free amine groups on the surface of Ti 3 C 2 T x are demonstrated. As a result, the availability of free amine groups on the surface potentially permits the fabrication of crosslinked electrically conductive MXene/epoxy composites, dye adsorbents, high–performance membranes, and drug carriers. Surface modifications of this type are applicable to many other MXenes.

36 MATERIALS SCIENCE↗

NASA NTRS1991

The use of aircraft-based Thermal Infrared Multispectral Scanner (TIMS) data to measure surface energy budgets on a landscape scale

A series of Thermal Infrared Multispectral Scanner Data (TIMS) was collected over the H. J. Andrews experimental forest in western Oregon and at the Coweeta Hydrologic Laboratory in North Carolina. Flight lines were overlapped with an 8 to 28 minute time difference between flight lines. Concurrent radiosonde measurements of atmospheric profiles of air and dew point temperatures provided inputs to LOWTRAN6 for atmospheric radiance corrections of the TIMS data. Surface temperature differences over time between flight lines allowed the development of thermal response numbers (TRN) which characterized the thermal response of the different surface types. The polygons containing mostly soil and bare rock had the lowest TRN whereas the forested polygons were the highest. Results indicate that forest canopy temperatures measured by the TIMS are comparable to needle thermocouples temperatures. ET models developed from the TIMS data obtained similar ET rates as those using energy balance techniques.

Luvall, Jeffrey C.↗