Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “materials evaluation”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 1,441 records · Page 80

Evaluation, development, and characterization of superconducting materials for space applications

The anisotropic electromagnetic features of a grain-aligned YBa2Cu3O(x) bulk sample derived from a process of long-time partial melt growth were investigated by the measurements of direct current magnetization (at 77 K) and alternating current susceptibility as a function of temperature, with the fields applied parallel and perpendicular to the c axis, respectively. The extended Bean model was further studied and applied to explain the experimental results. Upon comparison of the grain-aligned sample with pure single crystal materials, it is concluded that because of the existence of more effective pinning sites in the grain-aligned sample, not only its critical current density perpendicular to the c axis is improved, but the one parallel to the c axis is improved even more significantly. The anisotropy in the critical current densities in the grain-aligned sample at 77 K is at least one to two orders of magnitude smaller than in the pure single crystal. The measurement of anisotropy of alternating current susceptibility as a function of temperature, especially its imaginary part, shows that there are still some residues of interlayer weak links in the grain-aligned samples, but they are quite different from and far less serious than the weak links in the sintered sample.

Thorpe, Arthur N.↗

Venipuncture and intravenous infusion access during zero-gravity flight

The purpose of this experiment is to establish the difficulty associated with securing an intravenous (IV) catheter in place in microgravity flight and the techniques applicable in training the Crew Medical Officer (CMO) for Space Station Freedom, as well as aiding in the selection of appropriate hardware and supplies for the Health Maintenance Facility (HMF). The objectives are the following: (1) to determine the difficulties associated with venipuncture in a microgravity environment; (2) to evaluate the various methods of securing an IV catheter and attached tubing for infusion with regard to the unique environment; (3) to evaluate the various materials available for securing an intravenous catheter in place; and (4) to evaluate the fluid therapy administration system when functioning in a complete system. The inflight test procedures and other aspects of the KC-135 parabolic flight test to simulate microgravity are presented.

Krupa, Debra T.↗

Low earth orbit durability evaluation of Haynes 188 solar receiver material

The effects of elevated-temperature vacuum and elevated-temperature atomic oxygen exposure on the mass, surface chemistry, surface morphology, and optical properties of Haynes 188, a possible heat receiver material for space-based solar dynamic power systems, have been studied. Pristine and surface modified Haynes 188 were exposed to vacuum less than or equal to 10 exp -6 torr at 820 C for 5215.5 h, and to atomic oxygen in an air plasma asher at 34 and 827 C for fluences up to 5.6 x 10 exp 21 atoms/sq cm. Results obtained indicate that vacuum heat treatment caused surface morphology and chemistry changes with corresponding optical property changes. Atomic oxygen exposure caused optical property changes which diminished with time. Mass changes are considered to be negligible for both exposures.

De Groh, Kim K.↗

An overview of the evaluation of oxygen interaction with materials-third phase (EOIM-III) experiment - Space Shuttle Mission 46

An overview of EOIM-III, designed to produce benchmark atomic oxygen reactivity data is presented. Ambient density measurements are conducted using a quadrupole mass spectrometer calibrated for atomic oxygen measurements in a unique ground-based test facility. The combination of these data with the predictions of ambient density models permits an assessment of the accuracy of measured reaction rates on a variety of materials, many of which have never been tested in LEO previously.

Leger, Lubert J.↗

Nondestructive evaluation of a ceramic matrix composite material

Monolithic ceramic materials have proven their usefulness in many applications, yet, their potential for critical structural applications is limited because of their sensitivity to small imperfections. To overcome this extreme sensitivity to small imperfections, ceramic matrix composite materials have been developed that have the ability to withstand some distributed damage. A borosilicate glass reinforced with several layers of silicon-carbide fiber mat has been studied. Four-point flexure and tension tests were performed not only to determine some of the material properties, but also to initiate a controlled amount of damage within each specimen. Acousto-ultrasonic (AU) measurements were performed periodically during mechanical testing. This paper will compare the AU results to the mechanical test results and data from other nondestructive methods including acoustic emission monitoring and X-ray radiography. It was found that the AU measurements were sensitive to the damage that had developed within the material.

Grosskopf, Paul P.↗

Engineering development program of a closed aluminum-oxygen semi-cell system for an unmanned underwater vehicle: An update

Most emerging unmanned undersea vehicle (UUV) missions require significantly longer range and endurance than is achievable with existing battery technology. The Aluminum-Oxygen (Al-O2) semi-cell is a candidate technology capable of providing a significant improvement in endurance compared to the silver-zinc battery technology currently used in UUVs and compares favorably to other proposed UUV power systems not only in performance, but also in safety and logistics. An Al-O2 semi-cell system is under development by Loral Defense Systems-Akron (Loral) for the ARPA/Navy 44 in. diameter UUV test vehicle. The power plant consists of a cell stack, gas management, oxygen storage, electrolyte management, coolant and controller subsystems, designed to replace the existing silver-zinc battery and meet existing weight, volume, electrical and thermal requirements, therefore minimizing modifications to the UUV. A detailed system design is complete. A component and material endurance test to evaluate compatibility and reliability of various material arid components is complete. Sub scale (Short stack) system testing is completed. A full-scale demonstration unit is now under construction in the second half of 1995. The full scale demonstration test will simulate environmental conditions of the operational system. This paper summarizes the results of the extensive short stack and endurance test programs, describes the plan for full-scale testing, and concludes with a brief discussions of future directions for this technology. This program is sponsored by ARPA Maritime Systems Technology Office under NASA contract NAS3-26715.

Gregg, Dane W.↗

Engineering Development Program of a Closed Aluminum-Oxygen Semi-cell System for an Unmanned Underwater Vehicle: An Update

Most emerging unmanned undersea vehicle (UUV) missions require significantly longer range and endurance than is achievable with existing battery technology. The Aluminum-Oxygen (Al-O2) semi-cell is a candidate technology capable of providing a significant improvement in endurance compared to the silver-zinc battery technology currently in use in UUVs and compares favorably to other proposed UUV power systems not only in performance, but also in safety and logistics. An Al-O2 semi-cell system is under development, consisting of a cell stack, gas management, oxygen storage, electrolyte management coolant and controller subsystems. It is designed to replace the existing silver-zinc battery and meet existing weight, volume, electrical and thermal requirements, therefore minimizing modification to the UUV. A detailed system design is complete. A component and material endurance test to evaluate compatibility and reliability of various materials and components is complete. Sub=scale (short stack) system testing is complete. A full-scale demonstration unit is now under construction for testing in the second half of 1995. The full scale demonstration test will simulate environmental conditions of the operational system. This paper summarizes the results of the extensive short stack and endurance test programs, describes the plan for full-scale testing, and concludes with a brief discussion of future directions for this technology.

Gregg, Dane W.↗

Preparation, Fabrication, and Evaluation of Advanced Polymeric and Composite Materials

The thesis titles are given below: physical and mechanical behavior of amorphous poly(arylene ether-co-imidasole)s and poly(arylene ether-co-imidasole) modification epoxies; the requirements of patentability as applied to the chemical arts; fabrication of thermoplastic polymer composite ribbon; blend of reactive diluents with phenylethynyl-terminated arylene ether oligomers; the synthesis, characterization, and application of ether-containing polyimides; the synthesis of reflective and electrically conductive polyimide films via an in-situ self-metalization procedure using silver (I) complexes; the thermal cure of phenylethynyl terminated polyimides and selected model compounds; and the synthesis, characterization, and molecular modeling of cyclic arylene ether oligomers.

Orwoll, Robert A.↗

ZBLAN Viscosity Instrumentation

The past year's contribution from Dr. Kaukler's experimental effort consists of these 5 parts: a) Construction and proof-of-concept testing of a novel shearing plate viscometer designed to produce small shear rates and operate at elevated temperatures; b) Preparing nonlinear polymeric materials to serve as standards of nonlinear Theological behavior; c) Measurements and evaluation of above materials for nonlinear rheometric behavior at room temperature using commercial spinning cone and plate viscometers available in the lab; d) Preparing specimens from various forms of pitch for quantitative comparative testing in a Dynamic Mechanical Analyzer, Thermal Mechanical Analyzer; and Archeological Analyzer; e) Arranging to have sets of pitch specimens tested using the various instruments listed above, from different manufacturers, to form a baseline of the viscosity variation with temperature using the different test modes offered by these instruments by compiling the data collected from the various test results. Our focus in this project is the shear thinning behavior of ZBLAN glass over a wide range of temperature. Experimentally, there are no standard techniques to perform such measurements on glasses, particularly at elevated temperatures. Literature reviews to date have shown that shear thinning in certain glasses appears to occur, but no data is available for ZBLAN glass. The best techniques to find shear thinning behavior require the application of very low rates of shear. In addition, because the onset of the thinning behavior occurs at an unknown elevated temperature, the instruments used in this study must provide controlled low rates of shear and do so for temperatures approaching 600 C. In this regard, a novel shearing parallel plate viscometer was designed and a prototype built and tested.

Kaukler, William↗

Promoted Combustion Behavior of 316 Stainless Steel and 6061 Aluminum Alloys in Elevated Pressure Nitrox Environments

Promoted combustion testing (outlined in the ASTM G124 “Standard Test Method for Determining the Combustion Behavior of Metallic Materials in Oxygen Enriched Atmospheres”) refers to a useful testing method to evaluate how metallic materials will behave when combusted in environments with high oxygen concentrations, elevated pressure, or both. These tests yield data which is useful for engineers and scientists from a variety of industries who need and rely on oxygen systems. Oxygen Compatibility Assessments (OCA’s) are vital for ensuring that materials will be safe for use, and these assessments rely on data from OCA’s or interpolation if a desired pressure/concentration is outside of previously tested bounds. It was identified that these bounds leave out significant areas of data for materials which are tested at high pressures (above 1500 psi) and variable oxygen concentrations (with nitrogen as the diluent gas). For this reason, the authors posited that conducting promoted combustion testing on materials above 1500 psi and in various concentrations of oxygen would be incredibly useful in future analyses for oxygen compatibility with similar environments (such as breathing air) as well as for further understanding of how materials behave at very high pressures (such as 10000 psi). Two materials were selected which are commonly used in industry today - 316 stainless steel and 6061 aluminum – and they were tested and analyzed for the purposes of this study.

oxygen compatibility↗

Development of a Generic Small-Satellite Payload for On-Orbit Characterization and Evaluation of Novel Radiation-Shielding Materials

There is a need for lightweight and novel radiation shielding for small satellites operating in LEO and beyond. Current state of the art shielding materials include aluminum and polyethylene, or no shielding due to weight and dimensional considerations. New materials are being developed which may offer advantages over current options. These materials include novel lightweight composites impregnated with metallic nanoparticles, chitin-derived bioplastics, and aerogel-family materials. A compact experiment platform that allows the simultaneous testing of a number of potential shielding materials will be useful in comparing and validating them. The effort now underway seeks to develop a miniaturized, modularized payload which will allow testing of materials using 1U CubeSat form factor modules with four scintillator radiation detectors arrayed behind four sample material windows exposed to space. The first proposed mission will utilize a 2U payload volume to host two test quartets enabling eight materials to be tested. Such a test platform can potentially be used as a hosted payload on a variety of spacecraft to test other materials in the future.

Avery D Brock↗

Development of a Universal Small-Satellite Payload for On-Orbit Characterization and Evaluation of Novel Radiation-Shielding Materials

There is a need for novel lightweight radiation shielding materials for small satellites operating in LEO and beyond. Current commonly used shielding materials include aluminum and polyethylene, though often no additional shielding than that provided by structure is used due to mass and dimensional constraints. New materials are being developed which may offer advantages over these current solutions. These materials include novel lightweight composites impregnated with metallic nanoparticles, chitin-derived bioplastics, and aerogel-family materials. A compact CubeSat experiment payload that allows the simultaneous testing of numerus potential shielding materials would be useful to enable material comparison and efficacy validation. An effort currently underway seeks to develop such a miniaturized modularized payload, which will enable the testing of materials in 1U CubeSat form factor modules, with each module hosting four scintillator radiation detectors arrayed behind four sample material windows exposed to space. The first proposed mission will utilize a 2U payload volume to host two test quartets enabling eight materials to be tested. Such a test platform can potentially be used as a hosted payload on a variety of spacecraft to test additional materials in the future

Luke Idziak↗

Evaluation of an Eulerian multi-material mixture formulation based on a single inverse deformation gradient tensor field

We report high energy-density solids undergoing elastic-plastic deformations coupled to compressible fluids are a common occurrence in engineering applications. Examples include problems involving high-velocity impact and penetration, cavitation, and several manufacturing processes, such as cold forming. Numerical simulations of such phenomena require the ability to handle the interaction of shock waves with multi-material interfaces that can undergo large deformations and severe distortions. As opposed to Lagrangian (Benson 1992) and arbitrary Lagrangian-Eulerian (ALE) methods (Donea et al. 2004), fully Eulerian methods use grids that do not change in time. Consequently, Eulerian methods do not suffer from difficulties on account of mesh entanglement, and do not require periodic, expensive, remap operations.

36 MATERIALS SCIENCE↗

Evaluation of radiation hardness of semiconductor materials against alpha particles for an API detector

An Associated Particle Imaging (API) system consists of a high vacuum chamber where deuterium ions are accelerated on a tritium-loaded target, resulting in alpha particles and neutrons emitted back-to-back, the latter escaping the chamber and used, for example, for tomography of a high-Z sample. An accurate determination of the alpha position is crucial to determine the trajectory of the neutron. Existing API systems have several limitations which a semiconductor-based API detector placed inside the vacuum chamber should not present. The semiconductor material can be either silicon or diamond. In particular, large and fast signals are generated by the alpha interactions in these materials. A pixelated API detector will measure the time and hit position of the alphas produced in the reaction. However, during the lifetime of the generator, the semiconductor detector will be exposed to an intense flux of alpha particles that will degrade its performance over time. To assess the radiation hardness of silicon and diamond against the alpha particles, we exposed single diodes made of either of the two materials to a 5 MeV alpha flux generated by an 241Am radioactive source. During irradiation, the diodes were biased and mounted on current-sensitive preamplifier boards. We have therefore been able to measure insitu the evolution of the waveforms as the damage was accumulating in their substrates.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Plan for Post-Irradiation Examination of Zion Reactor Pressure Vessel Beltline Materials

The reactor pressure vessel (RPV) is a potentially life-limiting component in light-water reactors (LWR) because replacement of the RPV is not considered a viable option. Researchers studying the effects of radiation on RPV materials have long been interested in evaluating service-irradiated materials to assess currently available models for predicting radiation embrittlement of RPV steels. The decommissioning of the Zion Unit 1 NPP in Zion, Illinois presents a unique opportunity for characterization of an actual reactor pressure vessel (RPV) material after inservice degradation. The main interests in this case are the belt-line weld and base metals. Through-RPV wall thickness attenuation and chemical composition distributions are the obvious objectives of this characterization program. However, it also provides an opportunity to examine the inservice degradation and its comparison with currently available models for prediction of radiation embrittlement of RPV steels. All of these efforts will provide a better understanding of materials degradation and other issues associated with extending the lifetime of existing NPPs beyond 60 years of service. The primary foci are the Linde 80 flux, wire heat 72105 (WF-70) circumferential belt-line weld and the A533B-1 base metal from the intermediate shell harvested from a region of peak fluence (0.7 x 10{sup 19} n/cm{sup 2}, E > 1.0 MeV) on the internal surface of the Zion Unit 1 vessel. Following determination of the through-thickness chemical composition, Charpy impact, fracture toughness, tensile, and hardness testing will be being performed to characterize the through-thickness mechanical properties of the base metal and belt-line-weld materials. In addition to mechanical properties, microstructural characterizations will be performed using various techniques, including Atom Probe Tomography, Small Angle Neutron Scattering, and Positron Annihilation Spectroscopy.

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗