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DOE OSTI2026

Freestanding SrNbO 3 membranes as flexible transparent conductors

Synthesizing flexible transparent conducting materials is important for applications in flexible optoelectronics. Metallic oxide membranes offer great promise due to their large elasticity and high transparency. Among them, SrNbO 3 , a correlated metal, stands out as a promise transparent conducting oxide. However, synthesizing freestanding SrNbO 3 membranes poses a challenge because it easily undergoes oxidation, resulting in degraded conductivity. To address this, we utilize epitaxial BaTiO 3 capping layers, which effectively prevents SrNbO 3 oxidation. We successfully fabricate millimeter-sized transparent conducting BaTiO 3 /SrNbO 3 /BaTiO 3 membranes using water-soluble sacrificial layers. The obtained SrNbO 3 (10 nm thick) membrane exhibits a room temperature sheet resistance (R S ) of 174 Ω/sq and a transmittance (T) of 92% at a wavelength of 550 nm. The figure of merit (T 10 /R S ) of this transparent conductor reaches 2.2 × 10 −3 Ω −1 in the visible regime, comparable to SrNbO 3 films on rigid substrates. These results open possibilities for applications as flexible transparent conductors.

Ko, Eun Kyo [SLAC National Accelerator Laboratory ↗

DOE OSTI2025

LCLS Big Data Handling – How I Learned to Stop Worrying and Love the Data Deluge

Advanced data and computing systems are vital to Linac Coherent Light Source (LCLS) operations, data interpretation and overall scientific productivity. The transition to MHz-era operation marks a fundamental change in scale that requires new infrastructure and architectures to link LCLS to the required scale of computing needed for scientific interpretation. The LCLS-II Data System meets big data challenges by implementing configurable data reduction that can adapt to multiple science areas, real-time analysis frameworks to provide visualization and fast feedback, and the ability to transfer data to local and remote computational facilities for near real time analysis at the appropriate scale. Feature extracted information generated in the data analysis pipeline - at the edge, local compute, or remote High-Performance Computing (HPC) resources - can be used to steer experiments and inform user decisions during beam time. Artificial Intelligence and Machine Learning (AI/ML) techniques present new opportunities to rapidly analyse large datasets and direct experiments, but create new challenges in scaling, adaptability, complexity, and trustworthiness. We describe how the LCLS-II Data System architecture addresses its data-driven challenges in the areas of data acquisition, data processing, data management, and workflow orchestration to decrease the overall time-to-science and provide a vision for future developments.

artificial intelligence↗

DOE OSTI2025

Fiber-coupled digital photo sensors for large Time Projection Chambers

Here, this paper presents a novel approach to addressing challenges in neutrino event reconstruction within large Time Projection Chambers (TPCs). By integrating fiber-coupled digital silicon photomultipliers, we propose a design that enhances light detection and improves both energy resolution and event reconstruction. Advancements in power and signal over fiber technologies are leveraged to deploy digital sensors within the TPC bulk volume, enabling precise timing and robust particle identification.

47 OTHER INSTRUMENTATION↗

DOE OSTI2026

Beam-beam backgrounds for the Cool Copper Collider

In this paper, we present a comprehensive characterization of beam-beam backgrounds for the Cool Copper Collider (C 3 ), a proposed linear e + e - collider designed for precision Higgs studies at center-of-mass energies of 250 and 550 GeV. Using a simulation pipeline based on the Key4hep framework, we evaluate incoherent pair production and hadron photoproduction backgrounds through the SiD detector for baseline, power-efficiency, and high-luminosity C 3 operating scenarios. The occupancy induced by the beam-beam background is evaluated for each scenario, validating the compatibility of the existing SiD detector design with operations at C 3 without substantial modifications. Furthermore, at the same time, the modular simulation framework and analysis methodology presented in this paper offer a versatile toolkit for background studies in future collider proposals, contributing to a common platform for different machine designs.

Analysis and statistical methods↗

DOE OSTI2025

Optical Interference for the Guidance of Cryogenic Focused Ion Beam Milling Beyond the Axial Diffraction Limit

Using a tri-coincident cryogenic FIB-SEM-LM system, we identify an interferometric optical response that can be used for targeting lamella production to fluorescently labelled structures with accuracy beyond the diffraction limit. We demonstrate the approach using synthetic samples of fluorescent beads embedded in micron-scale droplets of water. Here, we then apply the approach to capture virions inside host cells. Successful targeting is confirmed by cryogenic electron tomography revealing clusters of virions in intracellular vesicles.

Sica, Anthony V. [SLAC National Accelerator Labora↗

DOE OSTI2025

Sensitivity of nEXO to 136 Xe charged-current interactions: Background-free searches for solar neutrinos and fermionic dark matter

We study the sensitivity of nEXO to solar neutrino charged-current interactions, 𝜈 𝑒 + 136 Xe → 136 Cs*+𝑒 − , as well as analogous interactions predicted by models of fermionic dark matter. Due to the recently observed low-lying isomeric states of 136 Cs, these interactions will create a time-delayed coincident signal observable in the scintillation channel. Here we develop a detailed Monte Carlo simulation of scintillation emission, propagation, and detection in the nEXO detector to model these signals under different assumptions about the timing resolution of the photosensor readout. We show this correlated signal can be used to achieve background discrimination on the order of 10 −9 , enabling nEXO to make background-free measurements of solar neutrinos above the reaction threshold of 0.668 MeV. We project that nEXO could measure the flux of neutrinos from the carbon-nitrogen-oxygen cycle with a statistical uncertainty of 25%, thus contributing a novel and competitive measurement toward addressing the solar metallicity problem. Additionally, nEXO could measure the mean energy of the 7 Be neutrinos with a precision of 𝜎 ≤ 1.5 keV and could determine the survival probability of 7 Be and pep solar 𝜈𝑒 with precision comparable to the state of the art. These quantities are sensitive to the Sun’s core temperature and to nonstandard neutrino interactions, respectively. Here, the strong background suppression would allow nEXO to search for charged-current interactions of fermionic dark matter in the mass range 𝑚 𝜒 = 0.668–7 MeV with a sensitivity up to three orders of magnitude better than current limits.

47 OTHER INSTRUMENTATION↗

DOE OSTI2025

Laser-Modulation-Driven X-Ray Pulse Shaping in Regenerative Amplifier Free-Electron Lasers

In this Letter, we present a robust method for generating custom-shaped, coherent hard x-ray pulses in regenerative amplifier free-electron lasers (RAFELs) using laser-induced energy modulation of the electron beam. A temporally shaped optical modulation imprints an optical-wavelength energy pattern on the beam, which interacts with the recirculated seed in the x-ray cavity to generate spectral sidebands. These sidebands lie outside the Bragg reflection bandwidth and are extracted as out-coupled radiation, while the seed is retained for continued amplification, enabling a novel mechanism for both output coupling and pulse shaping. Furthermore, this approach allows deterministic control over the spectral and temporal properties of the emitted x-rays, including multicolor generation, twin-pulse structures, pulse duration tuning, and complex temporal waveforms. Importantly, it does not require modification of the RAFEL cavity or optics and is fully compatible with high-repetition-rate operation, offering a practical pathway to deliver coherent, shaped, and on-demand x-ray pulses for advanced time-resolved and nonlinear x-ray science.

Free-electron lasers↗

DOE OSTI2025

Ultrafast x-ray diffraction of high-pressure phases in dynamically compressed TiO 2

Here, we investigate the high-pressure polymorphism of Ti⁢O 2 under laser-shock compression from 54(5) to 137(7) GPa using in situ femtosecond x-ray diffraction. Our results provide experimental evidence of the 𝑃⁢𝑐⁢𝑎⁢2 1 -type distorted fluorite structure formed from polycrystalline Ti⁢O 2 dynamically compressed to 54(5) GPa. Upon higher compression, we observe the direct formation of the ninefold coordinated F⁡e 2 ⁢P-type phase at 68(4) and 78(3) GPa in polycrystalline and [001]-oriented Ti⁢O 2 , respectively. This represents an unprecedented 100 GPa reduction in the shock synthesis pressure of the F⁡e 2⁢ P-type structure relative to quasihydrostatic loading conditions. On pressure release, the F⁡e 2⁢ P-type phase transforms to the α-Pb⁢O 2 structure and, at later times, reverts to rutile. Thus, the rutile →F⁡e 2⁢ P and α-Pb⁢O 2 →rutile transformations are both observed to occur on nanosecond timescales. Our results highlight the unique ability of high-strain-rate uniaxial compression to synthesize novel high-pressure phases and also indicate the importance of in situ atomic-level probes in developing pressure-temperature phase diagrams.

Crystal structures↗

DOE OSTI2026

Superconductivity Reinforces Charge-Density-Wave Phase Coherence across Cuprates

For decades, superconductivity in high-𝑇 c cuprates has been viewed as a competitor that suppresses charge-density-wave (CDW) order by reducing its amplitude and spatial extent. Here, in this study, we show that this picture is incomplete, as superconductivity is accompanied by a systematic enhancement of CDW phase coherence across multiple cuprate families. Using resonant soft x-ray scattering combined with a coherence-sensitive momentum-profile analysis, we uncover a BCS-like growth of phase coherence below 𝑇 c , which phenomenologically manifests as the absence of CDW peak broadening and near-perfect wave-vector locking. This enhancement remains visible even in a disorder-dominated regime created by long-term crystal aging and follows a common trend when compared with published data on Bi-, Hg-, Y-, and Nd-based cuprates. These results indicate that superconductivity reshapes CDW order in two distinct ways, suppressing its amplitude while strengthening its phase coherence, and reveal an additional phase-level interplay with lattice coupling in high-𝑇 c cuprates.

Lee, H. [SLAC National Accelerator Laboratory (SLA↗

DOE OSTI2026

Searches for Light Dark Matter and Evidence of Coherent Elastic Neutrino-Nucleus Scattering of Solar Neutrinos with the LUX-ZEPLIN (LZ) Experiment

We present searches for light dark matter (DM) with masses 3–9 GeV/𝑐 2 in the presence of coherent elastic neutrino-nucleus scattering (CE⁢𝜈⁢NS) from 8 B solar neutrinos with the LUX-ZEPLIN experiment. This analysis uses a 5.7 tonne-yr exposure with data collected between March 2023 and April 2025. In an energy range spanning 1–6 keV, we report no significant excess of events attributable to dark matter nuclear recoils, but we observe a significant signal from 8 B CE ⁢𝜈 ⁢NS interactions that is consistent with expectation. We set world-leading limits on spin-independent and spin-dependent-neutron DM-nucleon interactions for masses down to 5 GeV/𝑐 2 . In the no-dark-matter scenario, we observe a signal consistent with 8 B CE⁢ 𝜈 ⁢NS events, corresponding to a 4.5⁢𝜎 statistical significance. This is the most significant evidence of 8 B CE 𝜈 ⁢NS interactions and is enabled by robust background modeling and mitigation techniques. This demonstrates LZ’s ability to detect rare signals at keV-scale energies.

Dark matter detectors↗

DOE OSTI2026

Study of few-electron backgrounds in the LUX-ZEPLIN detector

The LUX-ZEPLIN (LZ) experiment aims to detect rare interactions between dark matter particles and xenon. Although the detector is designed to be the most sensitive to GeV/𝑐 2 –TeV/𝑐 2 weakly interacting massive particles (WIMPs), it is also capable of measuring low-energy ionization signals down to a single electron that may be produced by scatters of sub-GeV/𝑐 2 dark matter. The major challenge in exploiting this sensitivity is to understand and suppress the ionization background in the few-electron regime. We report a characterization of the delayed electron backgrounds following energy depositions in the LZ detector under different detector conditions. In addition, we quantify the probability for photons to be emitted in coincidence with electron emission from the high voltage grids. We then demonstrate that spontaneous grid electron emission can be identified and rejected with a high efficiency using a coincident photon tag, which provides a tool to improve the sensitivity of future dark matter searches.

Akerib, D. S. [SLAC National Accelerator Laborator↗

DOE OSTI2025

Maximizing quantum enhancement in axion dark matter experiments

We provide a comprehensive comparison of linear amplifiers and microwave photon counters in axion dark matter experiments. The study is done assuming a range of realistic operating conditions and detector parameters, over the frequency range between 1 and 30 GHz. As expected, photon counters are found to be advantageous under low background, at high frequencies (𝜈 >5 GHz), if they can be implemented with robust wide-frequency tuning or a very low dark count rate. Additional noteworthy observations emerging from this study include: (1) an expanded applicability of off-resonance photon background reduction, including the single-quadrature state squeezing, for scan rate enhancements; (2) a much broader appeal for operating the haloscope resonators in the overcoupling regime, up to 𝛽 ∼10; (3) the need for a detailed investigation into the cryogenic and electromagnetic conditions inside haloscope cavities to lower the photon temperature for future experiments; (4) the necessity to develop a distributed network of coupling ports in high-volume axion haloscopes to utilize these potential gains in the scan rate.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2025

Focusing of relativistic electron beams with permanent magnetic solenoid

Achieving strong focusing of MeV electron beams is a critical requirement for advanced beam applications such as compact laboratory x-ray sources, high gradient accelerators, and ultrafast electron scattering instrumentation. To address these needs, a compact radially magnetized permanent magnetic solenoid (PMS) has been designed, fabricated, and tested. The solenoid provides a compact and inexpensive solution for delivering high axial magnetic fields (1 T) to focus MeV electron beams. Field characterization of the solenoid demonstrates good agreement with analytical models, validating the PMS design. The electron beam test employs a high-brightness photoinjector to study the focusing properties of the PMS. The results indicate a focal length of less than 10 cm and a significant reduction in beam size with small spherical aberrations. Two application cases are evaluated: angular magnification in ultrafast electron diffraction setups and strong focusing for Compton scattering or other microfocus uses.

Electron diffraction↗

DOE OSTI2025

First high peak and average power single-pass THz free-electron laser in operation

We report on the operation of the first high peak and average power single-pass terahertz free-electron laser (THz FEL) based on a high-brightness photoinjector for developing a THz source for pump-probe experiments at advanced x-ray FELs (XFELs). Electron beams with 17 MeV/c momentum and charge up to 2.4 nC were used to generate narrow-band 3 THz radiation with pulse energies of more than 0.1 mJ. The novelty of the realized method is that the undulator radiation by electron beams is much longer than the radiation wavelength, with FEL starting from coherent beam contribution rather than shot noise. This proved to be not a simple scaling of the XFEL mechanism due to the significant role of the bunching factor in the considered case.

47 OTHER INSTRUMENTATION↗

DOE OSTI2026

High-pressure melt dynamics in shock-compressed titanium

In this work we study the high-pressure melting behavior of titanium using laser-driven shock compression with in situ femtosecond x-ray diffraction and molecular-dynamics simulations based on a machine-learned interatomic potential. The MD simulations predict the solid-liquid coexistence on the Hugoniot in the ∼111−124GPa range. Experimentally, we observe the first evidence of liquid at 86 GPa. We also observe pronounced microstructural changes with pressure, with strong grain refinement associated with the emergence of liquid, within the solid-liquid coexistence (∼110−126GPa). Above 126 GPa, we observe the persistence of residual levels of highly textured crystalline Ti to ∼180GPa, well above the expected melt completion pressure. We discuss the accuracy that current laser-shock experimental platforms have at determining the melt onset and completion pressures.

36 MATERIALS SCIENCE↗

DOE OSTI2025

Mixed gain detector configurations for time-resolved X-ray solution scattering

X-ray detection at X-ray free-electron lasers is challenging in part due to the XFEL's extremely short and intense X-ray pulses. Experimental measurements are further complicated by the large fluctuations inherent to the self-amplified spontaneous emission process producing the X-rays. At the Linac Coherent Light Source the ePix10ka2M detector offers multiple gain modes, and auto-ranging between these, to increase the dynamic range while retaining low noise. For diffuse scattering techniques, such as time-resolved X-ray solution scattering, where the shape of the scattering pattern largely does not change between exposures, a fixed mix of different gain modes offers many of the same advantages as auto-ranging. We find that configuring individual ASICs in separate gain modes does not impact the intensity linearity of the gain response and has a limited effect on the effective dynamic range in regions with different gain mode settings while avoiding the complexities of auto-ranging. Small (<5%) non-linear gain contributions arise when pixels on the same ASIC are configured in different gain modes. We present a configuration scheme that is designed to select the optimal mixed gain configuration to minimize effects of saturation in the high-/medium-gain region, while maximizing the number of pixels with higher gain to improve the signal-to-noise ratio.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2025

Conformational ensembles reveal the origins of serine protease catalysis

Enzymes exist in ensembles of states that encode the energetics underlying their catalysis. Conformational ensembles built from 1231 structures of 17 serine proteases revealed atomic-level changes across their reaction states. By comparing the enzymatic and solution reaction, we identified molecular features that provide catalysis and quantified their energetic contributions to catalysis. Serine proteases precisely position their reactants in destabilized conformers, creating a downhill energetic gradient that selectively favors the motions required for reaction while limiting off-pathway conformational states. The same catalytic features have repeatedly evolved in proteases and additional enzymes across multiple distinct structural folds. In conclusion, our ensemble-function analyses revealed previously unknown catalytic features, provided quantitative models based on simple physical and chemical principles, and identified motifs recurrent in nature that may inspire enzyme design.

Du, Siyuan [Stanford Univ., CA (United States)] (O↗

DOE OSTI2025

Selective chemical looping combustion of acetylene in ethylene-rich streams

Here, the requirement for C 2 H 2 concentrations below 2 parts per million (ppm) in gas streams for C 2 H 4 polymerization necessitates its semihydrogenation to C 2 H 4 . Here, we demonstrate selective chemical looping combustion of C 2 H 2 in C 2 H 4 -rich streams by Bi 2 O 3 as an alternative catalytic pathway to reduce C 2 H 2 concentration below 2 ppm. Bi 2 O 3 combusts C 2 H 2 with a first-order rate constant that is 3000 times greater than the rate constant for C 2 H 4 combustion. In successive redox cycles, the lattice O of Bi 2 O 3 can be fully replenished without discernible changes in local Bi coordination or C 2 H 2 combustion selectivity. Heterolytic activation of C–H bonds across Bi–O sites and the higher acidity of C 2 H 2 results in lower barriers for C 2 H 2 activation than C 2 H 4 , enabling selective catalytic hydrocarbon combustion leveraging differences in molecular deprotonation energies.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗