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At least 1,441 records · Page 80
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Damped Dirac magnon in the metallic kagome antiferromagnet FeSn

The kagome lattice is a fertile platform to explore topological excitations with both Fermi-Dirac and Bose-Einstein statistics. While relativistic Dirac fermions and flat bands have been discovered in the electronic structure of kagome metals, the spin excitations have received less attention. Here, we report inelastic neutron scattering studies of the prototypical kagome magnetic metal FeSn. The spectra display well-defined spin waves extending to 120 meV. Above this energy, the spin waves become progressively broadened, reflecting interactions with the Stoner continuum. Using linear spin-wave theory, we determine an effective spin Hamiltonian that reproduces the measured dispersion. This analysis indicates that the Dirac magnon at the K point remarkably occurs on the brink of a region where well-defined spin waves become unobservable. Furthermore, our results emphasize the influential role of itinerant carriers on the topological spin excitations of metallic kagome magnets.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

Order and excitations in large-S kagomé-lattice antiferromagnets

In this work, we systematically investigate the ground-state and the spectral properties of antiferromagnets on a kagomé lattice with several common types of the planar anisotropy: XXZ, single-ion, and out-of-plane Dzyaloshinskii-Moriya. Our main focus is on the role of nonlinear, anharmonic terms, which are responsible for the quantum order-by-disorder effect and for the corresponding selection of the ground-state spin structure in many of these models. The XXZ and the single-ion anisotropy models exhibit a quantum phase transition between the q=0 and the $\sqrt{3}$ ×$\sqrt{3}$ states as a function of the anisotropy parameter, offering a rare example of the quantum order-by-disorder fluctuations favoring a ground state which is different from the one selected by thermal fluctuations. The nonlinear terms are also shown to be crucial for a very strong near-resonant decay phenomenon leading to the quasiparticle breakdown in the kagomé-lattice antiferromagnets whose spectra are featuring flat or weakly dispersive modes. The effect is shown to persist even in the limit of large spin values and should be common to other frustrated magnets with flat branches of excitations. Model calculations of the spectrum of the S=5/2 Fe-jarosite with Dzyaloshinskii-Moriya anisotropy provide a convincing and detailed characterization of the proposed scenario.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2024

Nanoparticle self-assemblies with modern complexity

Thanks to decades of tireless efforts, nanoparticle assemblies have reached at an extremely high level of controllability, sophistication, and complexity, with new insights provided by integration with graph theory, cutting-edge characterization, and machine learning (ML)-based computation and modeling, as well as with ever-diversifying applications in energy, catalysis, biomedicine, optics, electronics, magnetics, organic biosynthesis, and quantum technology. Nanoparticle assemblies can be crystalline, known as superlattices or supracrystals. Their assembly entails a transition from disorder—dispersed nanoparticles—to order, which can be achieved through classical nucleation pathways or nonclassical pathways via prenucleation precursors or particle aggregation. Further, the periodic lattices allow facile manipulations of electrons, phonons, photons, and even spins, leading to advanced device components and metamaterials. Meanwhile, aperiodic assemblies out of nanoparticles, such as gels, networks, and amorphous solids, also start to attract attentions. Despite the loss of periodicity, symmetry-lowering or symmetry-breaking three-dimensional (3D) structures emerge with unique properties, such as chiroptical activity, topological mechanical strength, and quantum entanglement. Real-space imaging such as electron microscopy and X-ray based tomography methods are utilized to characterize these complex structures, while mathematical tools such as graph theories are in need to describe such complex structures. This issue aims to provide a timely review of the efforts in this greatly broadened materials design space including experiment, simulation, theory, and applications. Nine top experts (and their teams) from four countries deliver six review papers, summarizing fundamental mechanistic understandings of nanoparticle assemblies, highlighted with the developments of state-of-the-art in situ characterization tools and ML-assisted reverse engineering, and newly emergent applications of nanoarchitectures.

36 MATERIALS SCIENCE↗
DOE OSTI2010

Multi-collector Isotope Ratio Mass Spectrometer -- Operational Performance Report

This report describes the operational testing of a new magnetic sector mass spectrometer that utilizes seven full-sized discrete dynode electron multipliers operating simultaneously. The instrument includes a newly developed ion dispersion lens that enables the mass dispersed individual isotope beams to be separated sufficiently to allow a full-sized discrete dynode pulse counting multiplier to be used to measure each isotope beam. The performance of the instrument was measured using SRM 996 (244Pu spike) at loadings of 2.4 and 12 fg on resin beads and with SRM 4350B Columbia River Sediment samples. The measured limit of detection (3s) for 240Pu was 3.4 attograms for SRM 996. The limit of quantitation (LOQ), defined as 10 s, was 11.2 attograms. The measured concentration of 239Pu in the CRS standard was 152 ± 6 fg/g.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2014

Analysis of Phase Transformation Studies in Solute Addition Alloys

Components serving in a nuclear reactor plant must withstand a very harsh environment including extended time at elevated temperatures, neutron irradiation, stress, and/or corrosive media. The many modes of degradation are complex and very depending on material and service locations. However, understanding and managing materials degradation is paramount for the continued safe and reliable operation of nuclear power plants. For the reactor core and primary systems, several key areas have been identified. Thermomechanical considerations such as aging and fatigue must be examined. Irradiation-induced processes must also be considered for higher fluences under the life extension consideration of the current light water reactors (LWRs), which particularly includes the influence of radiation-induced segregation (RIS), swelling, and precipitation on component hardening and embrittlement. Corrosion takes many forms within the reactor core, although irradiation-assisted stress corrosion cracking (IASCC) and primary water stress corrosion cracking (PWSCC) are of high interest in extended life scenarios. Research in these areas can build upon other ongoing programs in the LWR industry as well as other reactor materials programs (such as fusion and fast reactors) to help resolve these issues for extended LWR life. Type 304 and 316 stainless steels are classic structural materials used in LWRs. A set of well designed type 304 and 316 variants by changing the amount of a single solute element were irradiated using the BOR-60 fast breeder reactor at ~320°C in Russia. This set of alloy samples has been used in this task to characterize detailed microstructural evolution and measure magnetic phase, swelling and hardness. This report summarizes the detailed microstructural results, characterized using conventional and scanning transmission electron microscopy (CTEM/STEM) and energy dispersive X-ray spectroscopy (EDS), and the newly developed model of strength factor for estimating radiation hardening. The results provide invaluable insights into understanding degradation mechanisms of key components and assists in the prediction of the life of similar materials and the base knowledge required to develop advanced radiation resistant alloys. The effect of solute elements on microstructural evolution under neutron irradiation is explored. The approximate correlation between microstructure changes and radiation hardening is established. The major results and implications are discussed below.

22 GENERAL STUDIES OF NUCLEAR REACTORS↗
DOE OSTI2017

Numerical Study on the Validity of the Taylor Hypothesis in Space Plasmas

In situ heliospheric measurements allow us to resolve fluctuations as a function of frequency. A crucial point is to describe the power spectral density as a function of the wavenumber, in order to understand the energy cascade through the scales in terms of plasma turbulence theories. The most favorable situation occurs when the average wind speed is much higher than the phase speed of the plasma modes, equivalent to the fact that the fluctuations’ dynamical times are much longer than their typical crossing period through the spacecraft (frozen-in Taylor approximation). Using driven compressible Hall-magneothydrodynamics simulations, in which an “imaginary” spacecraft flies across a time-evolving turbulence, here we explore the limitations of the frozen-in assumption. We find that the Taylor hypothesis is robust down to sub-proton scales, especially for flows with mean velocities typical of the fast solar wind. For slow mean flows (i.e., speeds of the order of the Alfvèn speed) power spectra are subject to an amplitude shift throughout the scales. At small scales, when dispersive decorrelation mechanisms become significant, the frozen-in assumption is generally violated, in particular for k -vectors almost parallel to the average magnetic field. A discussion in terms of the spacetime autocorrelation function is proposed. These results might be relevant for the interpretation of the observations, in particular for existing and future space missions devoted to very high-resolution measurements.

79 ASTRONOMY AND ASTROPHYSICS↗
NASA NTRS1976

Field-aligned fluxes in the geomagnetic equator

During 12 electron injection events observed by Explorer 45 during the December, 1971, and February, 1972, in magnetic storms it was found that the lowest observable pitch angle particles (down to 7 degrees in one case) arrived first. Pitch angle dispersion and shell-splitting effects are shown to be inadequate explanations for most of these pitch angle distributions. It is suggested that parallel electric fields may be supplying 1- to 5-keV electrons to the magnetosphere from the ionosphere. Various models of parallel electric fields are discussed.

Semar, C. L.↗
NASA NTRS1986

Fragmented molecular complexes: The role of the magnetic field in feeding internal supersonic motions

A hierarchical structure for molecular complexes in their cold phase i.e., preceeding the formation of massive stars, was derived from extensive large scale CO(13)(J=1=0) observations: the mass is found to be distributed into virialized clouds which fill only a very low fraction approx. 01 of the volume of the complex and are supported against gravity by internal supersonic motions. An efficient mechanism was found to transfer kinetic energy from the orbital motions of the clouds to their internal random motions. The large perturbations of the magnetic field induced at the cloud boundaries by their interactions with their neighbors generate systems of hydromagnetic waves trapped inside the clouds. The magnetic field lines being closely coupled to the gas at the densities which prevail in the bulk of the clouds volume, internal velocity dispersion is thus generated. Some conclusions derived from this data are given.

Falgarone, E.↗
NASA NTRS1992

The dynamic cusp

Results of a study of satellite and ground-based data acquired near the dayside cusp during a period when the IMF was inferred to have a strong northward component are presented. The presence of Pc 1 bursts, Pc 4-5 pulsations, and a tailward traveling twin vortex pattern of ionospheric convection suggests that the magnetosphere may have been temporarily compressed. Magnetic field data acquired at a synchronous altitude from GOES 5 and on the ground from Huanacayo support this suggestion. Plasma with ion dispersion characteristics associated with a cusp during southward IMF was detected by Viking over a 3.5-deg range of latitude. The presence of standing Alfven waves and ring current ions suggests that this 'cusplike' plasma was observed on closed geomagnetic field lines. It is suggested that the magnetosphere, during a northward IMF, is temporarily compressed by a solar wind pressure enhancement that produces the Pc 1 bursts, Pc 4-5 pulsations, and ionospheric vortices.

Potemra, T. A.↗
NASA NTRS1992

Comparison of weakly and strongly nonlinear wave evolution in a dispersive plasma

An investigation of the evolution of strongly nonlinear, low frequency (ion gyrofrequency), parallel propagating wave packets in a dispersive, collisionless, and low beta(= 8piP/B-squared = 0.3) plasma is undertaken using a hybrid numerical code. These strongly nonlinear wave packets have a transverse magnetic field strength, or wave amplitude, which is of order or greater the field strength along the direction of propagation, and their evolution can differ qualitatively from that of weakly nonlinear packets. The development of spreading fast wave (right helicity) and rarefraction regions competes strongly with steepening, and leads to a long time waveform which differs greatly from that for weak nonlinearity. Results are used to suggest that strongly nonlinear wave evolution occurs frequently in the earth's foreshock.

Vasquez, Bernard J.↗
NASA NTRS1995

Non-gyrotropic proton and alpha-particle velocity distributions in the solar wind: TAUS observations and stability analysis

Ion velocity distribution functions have been measured with high time resolution by the TAUS plasma instrument on the PHOBOS mission to Mars in 1989. The unambiguous separation of protons and alpha-particles by TAUS enabled us to study the nonthermal features of their distributions separately and to analyze the stability of the distributions against excitation of waves in the cyclotron-frequency domain. Typical nonthermal features include temperature anisotropies, with T(sub perpendicular) larger than T(sub parallel), and ion beam populations drifting along the local magnetic field direction. Also, distinctly non-gyrotropic alpha-particle velocity distributions were sometimes found. Non-gyrotropy strongly changes the wave dispersion and gives rise to new growing modes, related to the coupling of the standard wave modes existing in gyrotropic plasma. It is found that for the measured non-gyrotropic ion distributions the right-hand polarized wave can also be excited by a temperature anistropy instead of the usual beam drift.

Astudillo, H. F.↗
NASA NTRS1997

Alfvenic Solitons in Ultrarelativistic Electron-Position Plasmas

In electron-positron plasmas some of the plasma modes are decoupled due to the equal charge-to-mass ratio of both species. We derive the dispersion law for a low-frequency, generalized X-mode, which exists at all angles of propagation with respect to the static magnetic field.

Electron-positron plasmas Pulsars Nonlinear Modes↗
NASA NTRS2021

The First Widespread Solar Energetic Particle Event Observed By Solar Orbiter on 2020 November 29

Context. On 2020 November 29, the first widespread solar energetic particle (SEP) event of solar cycle 25 was observed at four widely separated locations in the inner (. 1AU) heliosphere. Relativistic electrons as well as protons with energies > 50MeV were observed by Solar Orbiter (SolO), Parker Solar Probe (PSP), the Solar Terrestrial Relations Observatory (STEREO)-A and multiple near-Earth spacecraft. The SEP event was associated with an M4.4 class X-ray flare and accompanied by a coronal mass ejection (CME) and an extreme ultraviolet (EUV) wave as well as a type II radio burst and multiple type III radio bursts. Aims. We present multi-spacecraft particle observations and place them in context with source observations from remote sensing instruments and discuss how such observations may further our understanding of particle acceleration and transport in this widespread event. Methods. Velocity dispersion analysis (VDA) and time shift analysis (TSA) were used to infer the particle release times at the Sun. Solar wind plasma and magnetic field measurements were examined to identify structures that influence the properties of the energetic particles such as their intensity. Pitch angle distributions and first-order anisotropies were analyzed in order to characterize the particle propagation in the interplanetary medium. Results. We find that during the 2020 November 29 SEP event, particles spread over more than 230° in longitude close to 1AU. The particle onset delays observed at the different spacecraft are larger as the flare–footpoint angle increases and are consistent with those from previous STEREO observations. Comparing the timing when the EUV wave intersects the estimated magnetic footpoints of each spacecraft with particle release times from TSA and VDA, we conclude that a simple scenario where the particle release is only determined by the EUV wave propagation is unlikely for this event. Observations of anisotropic particle distributions at SolO, Wind, and STEREO-A do not rule out that particles are injected over a wide longitudinal range close to the Sun. However, the low values of the first-order anisotropy observed by near-Earth spacecraft suggest that diffusive propagation processes are likely involved.

A Kollhoff↗
DOE OSTI2014

Growth and characterization of Pt-protected Gd{sub 5}Si{sub 4} thin films

Successful growth and characterization of thin films of giant magnetocaloric Gd{sub 5}(Si{sub x}Ge{sub 1−x}){sub 4} were reported in the literature with limited success. The inherent difficulty in producing this complex material makes it difficult to characterize all the phases present in the thin films of this material. Therefore, thin film of binary compound of Gd{sub 5}Si{sub 4} was deposited by pulsed laser deposition. It was then covered with platinum on the top of the film to protect against any oxidation when the film was exposed to ambient conditions. The average film thickness was measured to be approximately 350 nm using a scanning electron microscopy, and the composition of the film was analyzed using energy dispersive spectroscopy. X-ray diffraction analysis indicates the presence of Gd{sub 5}Si{sub 4} orthorhombic structure along with Gd{sub 5}Si{sub 3} secondary phase. The transition temperature of the film was determined from magnetic moment vs. temperature measurement. The transition temperature was between 320 and 345 K which is close to the transition temperature of the bulk material. Magnetic moment vs. magnetic field measurement confirmed that the film was ferromagnetic below 342 K.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2015

Microstructural, dielectric and magnetic properties of multiferroic composite system barium strontium titanate – nickel cobalt ferrite

Multiferroic composites (1-x) Ba{sub 0.95}Sr{sub 0.05}TiO{sub 3} + (x) Ni{sub 0.8}Co{sub 0.2}Fe{sub 2}O{sub 4} (where x = 0.1, 0.2, 0.3, 0.4) has been prepared by solid state reaction method. X-ray diffraction analysis of the composite samples confirmed the presence of both barium strontium titanate (BST) and nickel cobalt ferrite (NCF) phases. FESEM images indicated the well dispersion of NCF grains among BST grains. Dielectric constant and loss of the composite samples decreases with increase in frequency following Maxwell-Wagner relaxation mechanism. Composite sample with highest ferrite content possesses highest values of remanent and saturation magnetization.

36 MATERIALS SCIENCE↗
DOE OSTI2014

Faraday dispersion functions of galaxies

The Faraday dispersion function (FDF), which can be derived from an observed polarization spectrum by Faraday rotation measure synthesis, is a profile of polarized emissions as a function of Faraday depth. We study intrinsic FDFs along sight lines through face-on Milky Way like galaxies by means of a sophisticated galactic model incorporating three-dimensional MHD turbulence, and investigate how much information the FDF intrinsically contains. Since the FDF reflects distributions of thermal and cosmic-ray electrons as well as magnetic fields, it has been expected that the FDF could be a new probe to examine internal structures of galaxies. We, however, find that an intrinsic FDF along a sight line through a galaxy is very complicated, depending significantly on actual configurations of turbulence. We perform 800 realizations of turbulence and find no universal shape of the FDF even if we fix the global parameters of the model. We calculate the probability distribution functions of the standard deviation, skewness, and kurtosis of FDFs and compare them for models with different global parameters. Our models predict that the presence of vertical magnetic fields and the large-scale height of cosmic-ray electrons tend to make the standard deviation relatively large. In contrast, the differences in skewness and kurtosis are relatively less significant.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2019

Phosphate glass matrix composites incorporating trisilanol phenyl polyhedral oligomeric silsesquioxane prepared by viscous flow sintering method with enhanced benefits

The effect of mixing and sintering processes to prepare tin fluorophosphate glass (Pglass) matrix composites incorporating trisilanol phenyl polyhedral oligomeric silsesquioxane (TSP-POSS) was investigated by comparing manual and suspension mixing, one-step and stepwise sintering processes to explore the structure dynamics and physical properties in the composites as a function of the different process conditions used. Energy Dispersive X-ray analysis confirmed optimal homogeneous dispersion of the TSP-POSS molecules in the composites prepared by the suspension method. The observed increase of glass transition temperature and the reduction of non-bridging bonds in the composites are believed to be the reason for the effective dispersion of TSP-POSS molecules in the composites. The chemical reaction between the TSP-POSS and Pglass was strongly influenced by the mixing/dispersion and sintering processes investigated. 13 C cross polarized magic angle spinning (CP MAS) solid state nuclear magnetic resonance (NMR) spectroscopy confirmed the chemical stability of the TSP-POSS during the sintering process at elevated temperatures. In addition, a chemical reaction between the TSP-POSS and Pglass was evidenced by 29 Si CP MAS NMR analysis. Here, this study will provide a better fundamental understanding of the effective dispersion mechanism of the TSP-POSS molecules in the Pglass matrix that will facilitate tailoring the physicochemical properties of the composites with addition of various small concentrations of TSP-POSS for a number of applications where the pure Pglass is not applicable due to the intrinsic properties of the Pglass.

36 MATERIALS SCIENCE↗
DOE OSTI2017

Reduced Magnetism in Core–Shell Magnetite@MOF Composites

Rare-earth elements (REEs) have significant commercial and military uses.1-3 However, REE extraction through conventional mining processes is expensive and feasible at only a few locations worldwide. Alternative methods are needed to produce REEs from more geographically disperse resources and in a cost effective, environmental friendly manner.4,5 Among various sources, geothermal brine, used for generating geothermal energy can possess attractive concentrations (ppb to ppm level) of REEs along with other dissolved metal ions.6 A system that can selectively trap the REEs using an existing geothermal power plant infrastructure would be an attractive additional revenue stream for the plant operator that could accelerate the development and deployment of geothermal plants in the United States and rest of the world.7,8 Here, we demonstrate a magnetic core-shell approach that can effectively extract REEs in their ionic form from aqueous solution with up to 99.99% removal efficiency. The shell, composed of thermally and chemically stable functionalized metal-organic framework (MOF), is grown over a synthesized Fe3O4 magnetic core. Magnetic susceptibility of the particles was found to decline significantly after in situ growth of a MOF shell, which resulted from oxidation of Fe2+ species of the magnetite (Fe3O4) to Fe3+ species (maghemite). The core-shell particles can be completely removed from the mixture under an applied magnetic field, offering a practical, economic, and efficient REE-removal process.

77 NANOSCIENCE AND NANOTECHNOLOGY↗