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All sources NASA NTRS DOE OSTI

NASA NTRS1994

Ultraviolet photochemistry of cyanoacetylene: Application to Titan

Cyanoacetylene is believed to have had a central role in the formation of the pyrimidines essential for RNA synthesis leading to the origin of life on Earth. Cyanoacetylene has also been detected on Titan, Saturn's largest moon, and the only moon in the solar system that possesses a dense atmosphere. It is generally accepted that photochemistry plays a major role in the formation of the complex organic molecules and aerosols found in Titan's atmosphere. Because of its long wavelength absorption and low dissociation threshold it is expected that cyanoacetylene is an important part of these photochemical processes. Since cyanoacetylene would also have been subject to ultraviolet light in the atmosphere of early Earth, an investigation of cyanoacetylene photochemistry on Titan might lead to a better understanding of both the photochemical reactions occurring on primitive earth and the processes of chemical evolution as they occur in planetary atmospheres. The effects of irradiation wavelength, mixing with Titan's atmospheric gases, reducing the temperature and lowering cyanoacetylene partial pressures on product formation and polymer composition have been determined with the ultimate goal of understanding the chemical transformations taking place in Titan's atmosphere.

Clarke, D. W.↗

NASA NTRS1981

Structural tests on space shuttle thermal protection system constructed with nondensified and densified Li 900 and LI 2200 tile

Structural tests were conducted on thermal protection systems (TPS) LI 900 and LI 2200 tiles and .41 cm and .23 cm thick strain isolation pads. The bond surface of selected tiles was densified to obtain improved strength. Four basic types of experiments were conducted including tension tests, substrate mismatch (initial imperfection) tests, tension loads eccentrically applied, and pressure loads applied rapidly to the tile top surface. A small initial imperfection mismatch (2.29 m spherical radius on the substrate) did not influence significantly the ultimate failure strength. Densification of the tile bond region improved the strength of TPS constructed both of LI 900 tile and of LI 2200 tile. Pressure shock conditions studied did not significantly affect the TPS strength.

Williams, J. G.↗

NASA NTRS2016

Laser Induced Fluorescence Measurements in a Hall Thruster Plume as a Function of Background Pressure

A set of Laser Induced Fluorescence (LIF) measurements in the near-field region of the NASA- 173M Hall thruster plume is presented at four background pressure conditions varying from 9.4 x 10(exp -6) torr to 3.3 x 10(exp -5) torr. The xenon ion velocity distribution function was measured simultaneously along the axial and radial directions. An ultimate exhaust velocity of 19.6+/-0.25 km/s achieved at a distance of 20 mm was measured, and that value was not sensitive to pressure. On the other hand, the ion axial velocity at the thruster exit was strongly influenced by pressure, indicating that the accelerating electric field moved inward with increased pressure. The shift in electric field corresponded to an increase in measured thrust. Pressure had a minor effect on the radial component of ion velocity, mainly affecting ions exiting close to the channel inner wall. At that radial location the radial component of ion velocity was approximately 1000 m/s greater at the lowest pressure than at the highest pressure. A reduction of the inner magnet coil current by 0.6 A resulted in a lower axial ion velocity at the channel exit while the radial component of ion velocity at the channel inner wall location increased by 1300 m/s, and at the channel outer wall location the radial ion velocity remained unaffected. The ultimate exhaust velocity was not significantly affected by the inner magnet current.

Facility Effects↗

NASA NTRS1981

Coal desulfurization by low temperature chlorinolysis, phase 3

Laboratory scale, bench scale batch reactor, and minipilot plant tests were conducted on 22 bituminous, subbituminous, and lignite coals. Chemical pretreatment and post treatment of coals relative to the chlorination were tried as a means of enhancing desulfurization by the chlorinolysis process. Elevated temperature (500-700 C) hydrogen treatment of chlorinolysis-processed coal at atmospheric pressure was found to substantially increase coal desulfurization up to 90 percent. Sulfur forms, proximate and ultimate analyses of the processed coal are included. Minipilot plant operation indicates that the continuous flow reactor provides coal desulfurization results comparable to those obtained in the batch reactor. Seven runs were conducted at coal feed rates of 1.5 to 8.8 kg per hour using water and methylchloroform solvents, gaseous chlorine feed of 3 to 31.4 SCFH at 21 to 70 C, and atmospheric pressure for retention times of 20 to 120 minutes.

Kalvinskas, J. J.↗

NASA NTRS1987

Mechanical characteristics of filament-wound pressure vessel (burst pressure)

The finite element method is used to analyze the mechanical characteristics of a pressurized filament-wound (FW) pressure vessel, and to predict its burst pressure. The analysis takes into account the bending moment, the stretch-bend coupling effect, nonlinear stress-strain relations, and finite deflection. The analysis is based on two initial failure criteria for laminae, and two ultimate fracture criteria for laminated structures. The numerical results, obtained by applying the load incremental method to the isotensoid CFRP pressure vessel used in the launching of the Zikiken satellite, are in good agreement with the experimental burst pressure and fracture behaviors.

Iida, H.↗

NASA NTRS1997

Evaluation of a Composite Sandwich Fuselage Side Panel with Damage and Subjected to Internal Pressure

The results from an experimental and analytical study of a composite sandwich fuselage side panel for a transport aircraft are presented. The panel has two window cutouts and three frames, and has been evaluated with internal pressure loads that generate biaxial tension loading conditions. Design limit load and design ultimate load tests have been performed on the graphite-epoxy sandwich panel with the middle frame removed to demonstrate the suitability of this two-frame design for supporting the prescribed biaxial loading conditions with twice the initial frame spacing of 20 inches. The two-frame panel was damaged by cutting a notch that originates at the edge of a cutout and extends in the panel hoop direction through the window-belt area. This panel with a notch was tested in a combined-load condition to demonstrate the structural damage tolerance at the design limit load condition. The two panel configurations successfully satisfied all design load requirements in the experimental part of the study, and the three-frame and two-frame panel responses are fully explained by the analysis results. The results of this study suggest that there is potential for using sandwich structural concepts with greater than the usual 20-in.-wide frame spacing to further reduce aircraft fuselage structural weight.

Rouse, Marshall↗

NASA NTRS1998

Response of Composite Fuselage Sandwich Side Panels Subjected to Internal Pressure and Axial Tension

The results from an experimental and analytical study of two composite sandwich fuselage side panels for a transport aircraft are presented. Each panel has two window cutouts and three frames and utilizes a distinctly different structural concept. These panels have been evaluated with internal pressure loads that generate biaxial tension loading conditions. Design limit load and design ultimate load tests have been performed on both panels. One of the sandwich panels was tested with the middle frame removed to demonstrate the suitability of this two-frame design for supporting the prescribed biaxial loading conditions with twice the initial frame spacing of 20 inches. A damage tolerance study was conducted on the two-frame panel by cutting a notch in the panel that originates at the edge of a cutout and extends in the panel hoop direction through the window-belt area. This panel with a notch was tested in a combined-load condition to demonstrate the structural damage tolerance at the design limit load condition. Both the sandwich panel designs successfully satisfied all desired load requirements in the experimental part of the study, and experimental results from the two-frame panel with and without damage are fully explained by the analytical results. The results of this study suggest that there is potential for using sandwich structural concepts with greater than the usual 20-in. wide frame spacing to further reduce aircraft fuselage structural weight.

Rouse, Marshall↗

DOE OSTI2023

Transition to High-Hydrogen Fueled Advanced Gas Turbine Engines for Land-Based Power Generation and Industrial Applications

Invited lecture presented as part of the 2023 University of Central Florida - Mechanical and Aerospace Engineering Seminar Series. These slides discuss the role of multi-sourced hydrogen for electrical power generation. Particular focus is given to the combustion of hydrogen for the purpose of chemical to thermal energy. Pressure gain combustion is given as an example technology that could leverage hydrogen as a fuel source ultimately leading to higher rates of energy conversion (chemical to electrical) resulting in greater energy security and reduced cost of electricity.

advanced gas turbines↗

NASA NTRS2013

Multiphase Transport in Porous Media: Gas-Liquid Separation Using Capillary Pressure Gradients International Space Station (ISS) Flight Experiment Development

Advances in the understanding of multiphase flow characteristics under variable gravity conditions will ultimately lead to improved and as of yet unknown process designs for advanced space missions. Such novel processes will be of paramount importance to the success of future manned space exploration as we venture into our solar system and beyond. In addition, because of the ubiquitous nature and vital importance of biological and environmental processes involving airwater mixtures, knowledge gained about fundamental interactions and the governing properties of these mixtures will clearly benefit the quality of life here on our home planet. The techniques addressed in the current research involving multiphase transport in porous media and gas-liquid phase separation using capillary pressure gradients are also a logical candidate for a future International Space Station (ISS) flight experiment. Importantly, the novel and potentially very accurate Lattice-Boltzmann (LB) modeling of multiphase transport in porous media developed in this work offers significantly improved predictions of real world fluid physics phenomena, thereby promoting advanced process designs for both space and terrestrial applications.This 3-year research effort has culminated in the design and testing of a zero-g demonstration prototype. Both the hydrophilic (glass) and hydrophobic (Teflon) media Capillary Pressure Gradient (CPG) cartridges prepared during the second years work were evaluated. Results obtained from ground testing at 1-g were compared to those obtained at reduced gravities spanning Martian (13-g), Lunar (16-g) and zero-g. These comparisons clearly demonstrate the relative strength of the CPG phenomena and the efficacy of its application to meet NASAs unique gas-liquid separation (GLS) requirements in non-terrestrial environments.LB modeling software, developed concurrently with the zero-g test effort, was shown to accurately reproduce observed CPG driven gas-liquid separation phenomena. The design and fabrication of a micropost plate-lamina Hele-Shaw (HS) cell was performed which served as a computationally attainable geometric structure facilitating direct comparison between physical phenomena observed in our laboratory and the LB software predictions.

Wheeler, Richard R., Jr.↗

DOE OSTI2021

Injection data analysis using material balance time for CO 2 storage capacity estimation in deep closed saline aquifers

Estimating the ultimate storage capacity of deep saline aquifers is important to address the formation potential to store the envisioned large volumes of CO 2 . Injection data (i.e. injection rate, bottomhole pressure, and cumulative injected volume of CO 2 ) are routinely recorded during storage operations. These data contain valuable information on the subsurface (e.g. the reservoir pore volume and the formation storage capacity) that can be extracted. In this paper, we present a two-step graphical technique to infer the pore volume and the ultimate storage capacity of closed saline aquifers by analyzing the available injection data. First, the pore volume is inferred through adapting the concept of the material balance time. Material balance time is an approximate superposition time function developed to interpret production data from oil and gas wells operating at variable pressure/rate conditions during the boundary-dominated flow period. Using material balance techniques, the ultimate storage capacity is then estimated through linear extrapolation of the average pressure trend to the maximum allowable pressure the formation can withstand. The average pressure is not available in practice, but is can be obtained from the injection data. Two approaches are presented in this study to calculate the average pressure; namely the rigorous and the approximate approaches. Unlike the rigorous approach, the approximate approach does not require a prior knowledge of some reservoir properties (e.g. relative permeability, absolute permeability, formation porosity and thickness) to calculate the average pressure. To investigate its potential and reliability in analyzing CO 2 injection data, the proposed technique is applied to four synthetic cases representing different well operating conditions. Results indicate that the approximate approach consistently overestimates the actual (simulated) storage capacity as compared to the rigorous approach. The agreement - between the inferred and the simulated reservoir pore volume, and between the analytical and numerical estimates of storage capacity - validates the potential application of the technique to CO 2 storage in closed saline aquifers. The technique is further substantiated through application to a field data set utilized from a commercial-scale geological storage (CGS) project. Finally, field data interpretation shows that the proposed technique can be utilized to identify the degree of hydraulic continuity and reservoir compartmentalization within a target formation by interpreting the corresponding pressure and rate responses.

02 PETROLEUM↗

NASA NTRS1998

Tropospheric- Stratospheric Measurement Studies Summary

The two high altitude aircraft, ER-2 NASA #706 and 709 and the DC-8 NASA #717 are in active use in several programs of upper atmospheric research to study polar ozone changes, stratospheric-tropospheric exchange processes and atmospheric effects of aviation aircraft. The ER-2 has participated in seven major missions which mainly concentrated on vortex dynamics and the large losses of Ozone in the Polar regions (Ozone hole) observed in the spring. One mission verified the complex dynamical chemical and physical processes that occur during sunrise and sunset. Stratospheric Tracers of Atmospheric Transport (STRAT) obtained background measurements using the full ER-2 suite of instruments. Photochemistry of Ozone Loss in the Arctic Region in Summer (POLARIS) in 1997 assisted in understanding the mid-latitude and Arctic Ozone losses during the Northern Summer. The DC-8 with the Meteorological Measurement System (MMS) has participated in the Subsonic Aircraft: Cloud and Contrail Effects Special Study (SUCCESS), in 1996 and the Subsonic assessment Ozone and Nitrogen oxide experiment (SONEX) in 1997 missions. The MMS with its sophisticated software accurately measures ground speed and attitude, in-situ static and dynamic pressure total temperature, which are used to calculate the three dimensional wind fields, static pressure, temperature and turbulence values to meteorological accuracy. The meteorological data is not only of interest for its own sake in atmospheric dynamical processes such as mountain waves and flux measurements; but is also required by other ER-2 experiments that simultaneously measure water vapor, O3, aerosols, NO, HCl, CH4, N2O, ClO, BrO, CO2, NOy, HOx and temperature gradients. MMS products are extensively used to assist in the interpretation of their results in understanding the importance of convective effects relative to in-situ chemical changes, as may be noted by examining the list of references attached. The MMS consists of three subsystems: (a) aircraft instrumentation, inertial navigation system (INS), static and dynamic pressure taps, (b) additional dedicated instrumentation measuring angle of attack, yaw, total temperature, and a GPS which on the DC-8 measures position, velocity and attitude (c) an on board data, storage and computing acquisition system. This instrumentation and the associated software requires both an on-going laboratory ground calibration procedure for the total air temperature, static and total pressure inputs, verification of the INS dynamic response and also extensive air measurements and intercomparisons which ultimately verify and calibrate the complete system and its software. More than the usual accuracy is required because of the near cancellation occurring in the difference between the ground speed and true airspeed vectors used to give the wind vector. In the past year we have redesigned, recalibrated and used the MMS system on the NASA DC-8 that was previously used in the SUCCESS mission for the SONEX mission. Two papers were co-authored based on SUCCESS flights. Several reports and handouts were written for SONEX. Calibrations of the DC-8 pressure transducer temperature measuring thermistors was completed and an extensive analysis spanning several years of data files of the DC-8 Rosemount pressure transducer calibrations was done.

Browen, Stuart W.↗

DOE OSTI2021

Employing Weibull Analysis and Weakest Link Theory to Resolve Crystalline Silicon PV Cell Strength Between Bare Cells and Reduced- and Full-Sized Modules

Weibull analysis and weakest link theory are employed to resolve the probability of crystalline silicon PV cell fracture when measured as bare cells and when stressed in reduced- and full-sized modules. Experimental results indicated that the characteristic cell strength is reduced by ~20% once packaged into the laminate of a one-cell module and loaded in four-point flexure (4PF). This experimental observation was shown consistent with a weakest link theory prediction that the strength limiting flaws reside on the surface of the cell's edge. Here, the analysis is ultimately extended to present the equivalent loading of four-cell modules by uniform pressure and 4PF and a uniformly loaded full-sized module and demonstrates that smaller, representative, modules must be loaded to a much higher level than their parent full-sized modules to achieve an equivalent probability for cell fracture.

14 SOLAR ENERGY↗

NASA NTRS1995

Large-eddy simulations with wall models

The near-wall viscous and buffer regions of wall-bounded flows generally require a large expenditure of computational resources to be resolved adequately, even in large-eddy simulation (LES). Often as much as 50% of the grid points in a computational domain are devoted to these regions. The dense grids that this implies also generally require small time steps for numerical stability and/or accuracy. It is commonly assumed that the inner wall layers are near equilibrium, so that the standard logarithmic law can be applied as the boundary condition for the wall stress well away from the wall, for example, in the logarithmic region, obviating the need to expend large amounts of grid points and computational time in this region. This approach is commonly employed in LES of planetary boundary layers, and it has also been used for some simple engineering flows. In order to calculate accurately a wall-bounded flow with coarse wall resolution, one requires the wall stress as a boundary condition. The goal of this work is to determine the extent to which equilibrium and boundary layer assumptions are valid in the near-wall regions, to develop models for the inner layer based on such assumptions, and to test these modeling ideas in some relatively simple flows with different pressure gradients, such as channel flow and flow over a backward-facing step. Ultimately, models that perform adequately in these situations will be applied to more complex flow configurations, such as an airfoil.

Cabot, W.↗

NASA NTRS2013

Rocket Sled Propelled Testing of a Supersonic Inflatable Aerodynamic Decelerator

Decelerators (IADs) have traditionally been tested in wind tunnels. As the limitations of these test facilities are reached, other avenues must be pursued. The IAD being tested is a Supersonic IAD (SIAD), which attaches just aft of the heatshield around the perimeter of an entry body. This 'attached torus' SIAD is meant to improve the accuracy of landing for robotic class missions to Mars and allow for potentially increased payloads. The SIAD Design Verification (SDV) test aims to qualify the SIAD by applying a targeted aerodynamic load to the vehicle. While many test architectures were researched, a rocket sled track was ultimately chosen to be the most cost effective way to achieve the desired dynamic pressures. The Supersonic Naval Ordnance Research Track (SNORT) at the Naval Air Warfare Center Weapons Division (NAWCWD) China Lake is a four mile test track, traditionally used for warhead and ejection seat testing. Prior to SDV, inflatable drag bodies have been tested on this particular track. Teams at Jet Propulsion Laboratory (JPL) and NAWCWD collaborate together to design and fabricate one of the largest sleds ever built. The SDV sled is comprised of three individual sleds: a Pusher Sled which holds the solid booster rockets, an Item Sled which supports the test vehicle, and a Camera Sled that is pushed in front for in-situ footage and measurements. The JPL-designed Test Vehicle has a full-scale heatshield shape and contains all instrumentation and inflation systems necessary to inflate and test a SIAD. The first campaign that is run at SNORT tested all hardware and instrumentation before the SIAD was ready to be tested. For each of the three tests in this campaign, the number of rockets and top speed was increased and the data analyzed to ensure the hardware is safe at the necessary accelerations and aerodynamic loads.

Supersonic Inflatable Aerodynamic Decelerators (SI↗

DOE OSTI2021

Hydrogen Component Leak Rate Quantification for System Risk and Reliability Assessment through QRA and PHM Frameworks: Preprint

The National Renewable Energy Laboratory's (NREL) Hydrogen Safety Research and Development (HSR&D) program in collaboration with the University of Maryland's Systems Risk and Reliability Analysis Laboratory (SyRRA) are working to improve reliability and reduce risk in hydrogen systems. This approach strives to use quantitative data on component leaks and failures, together with Prognosis and Health Management (PHM), and Quantitative Risk Assessment (QRA) to identify at-risk components, reduce component failures and downtime, and predict when components require maintenance. Hydrogen component failures increase facility maintenance cost, facility downtime, and reduce public acceptance of hydrogen technologies, ultimately increasing facility size and cost because of potentially overly conservative requirements. Leaks are a predominant failure mode for hydrogen components. However, uncertainties in the amount of hydrogen emitted from leaking components and the frequency of those failure events limit the understanding of the risks that they present under real-world operational conditions. NREL has deployed a test fixture, the Leak Rate Quantification Apparatus (LRQA), to quantify the mass flow rate of leaking gases from medium and high-pressure components that have failed while in service. Quantitative hydrogen leak rate data from this system could ultimately be used to better inform risk assessment and Regulation Codes and Standards (RCS). Parallel activity explores the use of PHM and QRA techniques to assess and reduce risk, thereby improving safety and reliability of hydrogen systems. The results of QRAs could further provide a systematic and science-based foundation for the design and implementation of RCS, as in the latest versions of the NFPA 2 code for gaseous hydrogen stations. Alternatively, data-driven techniques of PHM could provide new damage diagnosis and health-state prognosis tools. This research will help end users, station owners and operators, and regulatory bodies move towards risk-informed preventative maintenance versus emergency corrective maintenance, reducing cost and improving reliability. Predictive modelling of failures could improve safety and affect RCS requirements such as setback distances at liquid refuelling sites. The combination of leak rate quantification research, PHM, and QRA can lead to better informed models enabling data-based decision to be made for hydrogen system safety improvements.

codes and standards↗

DOE OSTI2021

Optical and mass-spectral characterization of mixed-gas flowing atmospheric-pressure afterglow sources

Plasma-based ambient desorption/ionization (ADI) sources for mass spectrometry (MS) often use helium as the primary discharge gas due to the large reaction cross section of excited helium species with atmospheric gases, which ultimately leads to efficient reagent-ion formation. However, some studies have shown that mixed-gas plasmas provide unique advantages. For instance, our group showed that a helium-oxygen flowing atmospheric-pressure afterglow (He:O 2 -FAPA) source yielded enhanced ion signals for small polar analytes, but compounds with aromatic rings underwent chemical modification to produce pyrylium species. Here, it is shown that the addition of H 2 to the helium FAPA gas significantly decreased the reagent-ion signals, but analyte-ion signal was not affected to the same degree. In addition, mass spectra obtained with He:H 2 -FAPA were chemically cleaner with fewer ions stemming from analyte species and produced less oxidation of analytes. Addition of nitrogen increased the abundance of negative reagent ions (e.g., NO 2 - and NO 3 - ) which led to enhanced ion signal for RDX. To better understand these unique advantages of a mixed-gas FAPA, the impact of molecular-gas (O 2 , N 2 , or H 2 ) addition on the optical-emission spectra from the discharge was also measured. Spatially resolved emission was obtained from the anode- and negative-glow regions. In general, addition of small fractions (~0.1%) of molecular gases decreased helium and OH emission intensities. Atomic oxygen and hydrogen emission increased with the addition of O 2 and H 2 , respectively. Furthermore, emission characteristics of N 2 , N 2 + , and NO with respect to molecular gas composition on He-FAPA were measured. Finally, fundamental plasma parameters, such as OH rotational temperature (T rot ), were also calculated for these mixed-gas systems.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2021

Cooperative Research and Development Agreement among Ames Laboratory; NexTech Materials, Ltd. dba Nexceris; and National Energy Technology Laboratory [Abstract]

The CRADA focuses on pressurized testing of Nexceris solid oxide fuel cell (SOFC) stacks in a hybrid configuration with a recuperated gas turbine with the ultimate goal of demonstrating efficiencies in excess of 70% (LHV NG). NETL’s cyber-physical approach will be used to develop and test control strategies before installing the Nexceris SOFC stacks to maximize the chances of success. A successful test will represent a demonstration of the Nexceris stack to endure pressures associated with hybrid operation and the first public demonstration of automated hybrid SOFC/GT technology.

30 DIRECT ENERGY CONVERSION↗

NASA NTRS1981

Recent Darrieus vertical axis wind turbine aerodynamical experiments at Sandia National Laboratories

Experiments contributing to the understanding of the aerodynamics of airfoils operating in the vertical axis wind turbine (VAWT) environment are described. These experiments are ultimately intended to reduce VAWT cost of energy and increase system reliability. They include chordwise pressure surveys, circumferential blade acceleration surveys, effects of blade camber, pitch and offset, blade blowing, and use of sections designed specifically for VAWT application.

Klimas, P. C.↗