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At least 145 records · Page 8

Proceedings of the 25th International Instrumentation Symposium, May 7-10, 1979, Anaheim, California

The papers deal essentially with the instrumentation needs of the transportation industry, machinery diagnostics, and energy research. The sessions covered include: acoustic emission, reentry vehicle ground and flight testing, performance of nose tip materials, instrumentation for solar heating and cooling systems, vibration measurement, data acquisition and analysis, system for aerospace pressure measurements, wind tunnel instrumentation and control, energy source instrumentation, nondestructive testing, pressure and flow measurements, automated test facilities, strain measurements, electrooptical instrumentation, thermal measurements, microcomputer applications in instrumentation and automation, flight testing, blast pressure measurement, two-phase liquid/gas mass flow measurement, and machinery monitoring and instrumentation.

Conferences↗

Eddy current probe measures size of cracks in nonmetallic materials

Nondestructive method uses powdered iron and eddy current probe to measure the depth/width ratio of cracks in electrically nonconductive materials. The eddy current probe measures the mass of metal in the crack after it has been filled with the powdered iron.

Musser, C. W.↗

Nondestructive Characterization of Antireflective Coatings on PV Modules

Antireflective coatings (ARCs) are used on the vast majority of solar photovoltaic (PV) modules to increase power production. However, ARC longevity can vary from less than 1 to over 15 years depending on coating quality and deployment conditions. A technique that can quantify ARC degradation nondestructively on commercial modules would be useful both for in-field diagnostics and accelerated aging tests. In this article, we demonstrate that accurate measurements of ARC spectral reflectance can be performed using a modified commercially available integrating-sphere probe. The measurement is fast, accurate, nondestructive, and can be performed outdoors in full-sun conditions. We develop an interferometric model that estimates coating porosity, thickness, and fractional area coverage from the measured reflectance spectrum for a uniform single-layer coating. We demonstrate the measurement outdoors on an active PV installation, identify the presence of an ARC, and estimate the properties of the coating.

14 SOLAR ENERGY↗

NA-22 Write for Consortium Efforts

We are asked to look into the improvements for the measurement of Pu of a variety of material types (MT): MT41 (Pu-242, 20 – 60% enriched), MT42 (Pu-242 > 60% enrichment), and MT-82 (Np-237). Many of these are legacy items that were packaged years ago (Fig 1&2), and when the items are re-packaged for long-term storage, they must be re-measured using either NDA (nondestructive analysis methods or radiochemical methods. It is of interest to improve the NDA and radiochemistry to reduce the un-certainty in the measurements, as in the case of larger items (250 g to 2 kg items) the uncertainty in measurements makes it difficult to certify the mass of the material down to the 0.5 g accountability requirement per DOE orders by only doing NDA measurement. It would be of interest to look into methods to improve the detection of these materials, which would not only benefit the weapon manufacturing community, but also has the ability to significantly improve the non-proliferation community.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Delayed Neutron Temporal Signatures for Uranium Enrichment Measurement NA-241 SGTech (Final Report)

Nondestructive determination of uranium enrichment is a core capability for nuclear material accounting and control (NMAC) and safeguards verification measurements; however, traditional gamma spectroscopy-based techniques for enrichment measurement rely on significant assumptions of material composition and geometry, precluding their use in scenarios where a heterogeneous spatial distribution of enrichments is encountered. As an alternative, we are developing a technique to use delayed neutron temporal signatures for the measurement of uranium enrichment. Each uranium isotope has unique delayed neutron group yields, resulting in a unique delayed neutron decay time profile which can be analyzed to determine enrichment without the need for calibration sources. As part of this effort, we performed a series of measurement campaigns in which we used an active well coincidence counter (AWCC) retrofitted with commercial D-D and D-T generators to evaluate the operational characteristics of this method in response to a set of uranium enrichment and mass standards, as well as representative diversion scenarios in which either “concealed” enriched uranium is shielded by depleted uranium or declared enriched uranium is “hollowed out” and replaced with a central region of depleted uranium. A standard operating procedure and best practices were compiled to facilitate the use of delayed neutron-based enrichment measurements for international safeguards inspections.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Integrated Nondestructive Evaluation and Finite Element Analysis Predicts Crack Location and Shape

This study describes the finite-element analyses and the NDE modality undertaken on two flywheel rotors that were spun to burst speed. Computed tomography and dimensional measurements were used to nondestructively evaluate the rotors before and/or after they were spun to the first crack detection. Computed tomography data findings of two- and three-dimensional crack formation were used to conduct finite-element (FEA) and fracture mechanics analyses. A procedure to extend these analyses to estimate the life of these components is also outlined. NDE-FEA results for one of the rotors are presented in the figures. The stress results, which represent the radial stresses in the rim, clearly indicate that the maximum stress region is within the section defined by the computed tomography scan. Furthermore, the NDE data correlate well with the FEA results. In addition, the measurements reported show that the NDE and FEA data are in parallel.

Abdul-Azia, Ali↗

Ultrasonic measurement of fracture toughness

Inexpensive nondestructive method ranks materials by crack toughness. Method can reduce expenses involved in conventional mechanical destructive testing and can be inspection tool in determining local variations of materials in fracture-prone components.

Vary, A.↗

Ultrasonic measurement of porosity in casts and welds

The development of a quantitative nondestructive method which involves ultrasonic attenuation measurements in frequency domain to determine volume fraction of porosity in aluminum cast is discussed. The aluminum alloy A357 casting samples were produced at the Ohio State University Foundry with controlled porosity contents ranging from 0% to 6%. A computer controlled system was used to direct ultrasonic beam to a test sample to different places to conduct ultrasonic attenuation measurements. The plot of attenuation coefficients as a function of frequency was then evaluated based on existing theories to determine volume fraction of porosity and pore size.

Adler, L.↗

In-situ measurements of alloy oxidation/corrosion/erosion using a video camera and proximity sensor with microcomputer control

Two noncontacting and nondestructive, remotely controlled methods of measuring the progress of oxidation/corrosion/erosion of metal alloys, exposed to flame test conditions, are described. The external diameter of a sample under test in a flame was measured by a video camera width measurement system. An eddy current proximity probe system, for measurements outside of the flame, was also developed and tested. The two techniques were applied to the measurement of the oxidation of 304 stainless steel at 910 C using a Mach 0.3 flame. The eddy current probe system yielded a recession rate of 0.41 mils diameter loss per hour and the video system gave 0.27.

Deadmore, D. L.↗

Nondestructive evaluation of printed wiring boards by microhm resistance measurements

Application of the microhm measuring circuit to measurement of plated-through hole resistances, when combined with appropriate probes, provides data that can be related to the quality of copper plating on printed wiring boards. Acceptance limits can be established and continuous inspection performed, with plating defects causing abnormal readings.

Stiefeld, B.↗

Effect of Ion Sputtering on Interface Chemistry and Electrical Properties of an Gaas (100) Schottky Contacts

Auger and electron photoelectron spectroscopy were used to measure the extent of As depletion during 1 keV to 5 keV argon sputtering of GaAs surfaces. This depletion was correlated with a general decrease in the barrier height of the rectifying Au contact deposited in situ. However, nondestructive angle resolved XPS measurements showed As was depleted at the outer surface more by 1 keV than 3 keV argon. These effects are explained based on a combined work effective work function model and creation of a donor like surface damage layer. The donor layer was correlated with As depletion by sputtering. Deep level trap formation and annealing of sputtering effects were studied.

Wang, Y. X.↗

Interrelation of material microstructure, ultrasonic factors, and fracture toughness of two phase titanium alloy

The pivotal role of an alpha-beta phase microstructure in governing fracture toughness in a titanium alloy, Ti-662, is demonstrated. The interrelation of microstructure and fracture toughness is demonstrated using ultrasonic measurement techniques originally developed for nondestructive evaluation and material property characterization. It is shown that the findings determined from ultrasonic measurements agree with conclusions based on metallurgical, metallographic, and fractographic observations concerning the importance of alpha-beta morphology in controlling fracture toughness in two phase titanium alloys.

Vary, A.↗

Tomographic Measurement Of Laser-Bored Holes

Nondestructive technique detects internal variations in arrays of small holes. Inspection method checks laser-bored holes for accuracy. Combines computed tomography and digital laminography. Both types of views made at many parallel planes within plate. System prints out tables of measured and standard deviation of diameter at all planes for each hole.

Willenberg, James D.↗

Summary of Activities for Health Monitoring of Composite Overwrapped Pressure Vessels

This new start project (FY12-14) will design and demonstrate the ability of nondestructive evaluation sensors for the measurement of stresses on the inner diameter of a Composite Overwrapped Pressure Vessel overwrap. Results will be correlated with other nondestructive evaluation technologies such as Acoustic Emission. The project will build upon a proof of concept study performed at KSC which demonstrated the ability of Magnetic Stress Gages to measure stresses at internal overwraps and upon current acoustic emission research being performed at WSTF; The gages will be produced utilizing Maundering Winding Magnetometer and/or Maundering Winding Magnetometer-array eddy current technology. The proof-of-concept study demonstrated a correlation between the sensor response and pressure or strain. The study also demonstrated the ability of Maundering Winding Magnetometer technology to monitor the stresses in a Composite Overwrapped Pressure Vessel at different orientations and depths. The ultimate goal is to utilize this technology for the health monitoring of Composite Overwrapped Pressure Vessels for all future flight programs.

Russell, Rick↗

Proceedings of the First Annual Symposium for Nondestructive Evaluation of Bond Strength

Quantitative adhesive bond strength measurement has been an issue for over thirty years. Utilization of nonlinear ultrasonic nondestructive evaluation methods has shown more effectiveness than linear methods on adhesive bond analysis, resulting in an increased sensitivity to changes in bondline conditions. Correlation to changes in higher order material properties due to microstructural changes using nonlinear ultrasonics has been shown and could relate to bond strength. Nonlinear ultrasonic energy is an order of magnitude more sensitive than linear ultrasound to these material parameter changes and to acoustic velocity changes caused by the acoustoelastic effect when a bond is prestressed. This increased sensitivity will assist in getting closer to quantitative measurement of adhesive bond strength. Signal correlations between non-linear ultrasonic measurements and initialization of bond failures have been successfully measured. This paper reviews nonlinear bond strength research efforts presented by university and industry experts at the First Annual Symposium for Nondestructive Evaluation of Bond Strength organized by the NDE Sciences Branch at NASA Langley in November 1997.

Roberts, Mark J.↗

Analytical capabilities for iodine detection: Review of possibilities for different applications

This Review summarizes a range of analytical techniques that can be used to detect, quantify, and/or distinguish between isotopes of iodine (e.g., long-lived 129 I, short-lived 131 I, stable 127 I). One reason this is of interest is that understanding potential radioiodine release from nuclear processes is crucial to prevent environmental contamination and to protect human health as it can incorporate into the thyroid leading to cancer. It is also of interest for evaluating iodine retention performances of next-generation iodine off-gas capture materials and long-term waste forms for immobilizing radioiodine for disposal in geologic repositories. Depending upon the form of iodine (e.g., molecules, elemental, and ionic) and the matter state (i.e., solid, liquid, and gaseous), the available options can vary. In addition, several other key parameters vary between the methods discussed herein, including the destructive vs nondestructive nature of the measurement process (including in situ vs ex situ measurement options), the analytical data collection times, and the amount of sample required for analysis.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Workshop on Improving Holdup Monitoring in the US

The characterization and quantification of nuclear deposits, or residual nuclear material retained in process equipment, generally referred to as holdup, continues to challenge nuclear processing facilities in DOE program areas such as nuclear criticality safety, material control and accountability, environmental management. The efficiency and effectiveness of nuclear operations in these facilities depends heavily on the results from nondestructive techniques designed to measure nuclear materials in situ. The traditional methods used to measure holdup were established more than 30 years ago and assume unrealistic conditions for most measurement cases. These blind, in situ measurements present unique challenges due to the following attributes: unique, non-ideal geometries; unknown deposit thicknesses; lack of representative calibration standards; large number of holdup deposit locations; and poor accessibility for many measurement locations. These difficulties and the poor assumptions made to handle them have resulted in measurement uncertainties that are often too large for many programs to effectively utilize. In an effort to address and identify solutions to the current holdup challenges facing the US nuclear industry, Oak Ridge National Laboratory hosted the Technical Workshop on Improving Holdup Monitoring in the US. The two-day workshop held August 21–22, 2019, was attended by 35 holdup measurement practitioners, program managers, stakeholders from US Department of Energy sites, the Nuclear Regulatory Commission, and representatives from commercial industry. The primary objectives were to identify critical elements of a successful and defensible holdup measurement program; identify technical challenges, needs, and potential improvements associated with measurement of holdup; and share best practices and lessons learned from recent accumulation events. Fourteen presentations were delivered on holdup topics including necessary elements for effective program management, measurement needs, emerging technologies and other measurement solutions, and lessons learned from recent events. These presentations highlighted best practices related to accumulation monitoring, considerations and proactive steps to facilitate holdup in new facility designs, imaging solutions to improve holdup assumptions, and new software developed in support of holdup measurements. Breakout sessions were also employed to determine additional needs and identify potential solutions to common holdup challenges. The primary discussions focused on causes and prevention of material accumulations, needs for uranium and plutonium measurements, and reduction of measurement uncertainty, all of which were explicitly identified as critical needs during the 2018 Workshop on Technical and Programmatic Needs for a Sustainable NDA Program for the US DOE.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Initial Refinement and Optimization of the Image Reconstruction (U-MBIR) Algorithm to Optimize its Performance in Detecting Damage and Flaws

Concrete is a critical component of nuclear power plants; thus, its safety and reliability must be thoroughly examined throughout the life cycle of the structural system. During the life cycle of this infrastructure, monitoring of the concrete for signs of degradation should be performed through nondestructive evaluation (NDE). Ultrasonic measurements have been an industry standard for both surface and subsurface inspections. As such, Oak Ridge National Laboratory (ORNL) is developing advanced image reconstruction algorithms to overcome the limitations of traditional ultrasonic NDE methodologies. The results and discussion presented herein summarize the current state of the ultrasonic model–based iterative reconstruction (U-MBIR) algorithm developed at ORNL.

36 MATERIALS SCIENCE↗