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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 145 records · Page 8
All sourcesNASA NTRSDOE OSTI
DOE OSTI2021

In situ TEM measurement of electrical properties of individual BaTiO 3 nanocubes

We report on the measurement of the electrical properties of individual pristine and doped BaTiO 3 nanocubes by using in situ transmission electron microscopy with a two-electrode configuration. The dimensions of the nanocubes tested are between 10 and 20 nm, which rendered their in situ electrical characterization challenging. We characterized 4%Cr and 5%La (atomic percentage) doped BaTiO 3 nanocubes and compared them with the properties of pristine BaTiO3 nanocubes synthesized by the same solvothermal method. We found that the resistance of all three types of nanocubes when displayed in log-scale shows a nearly linear dependence on the applied electric field (R2 ≥ 0.95) over a wide range of electric fields (50–900 kV/cm). Compared with pristine BaTiO 3 nanocubes, the resistance of both 4%Cr and 5%La doped nanocubes showed reduced variation rates with respect to the electric field, with 5%La doping, demonstrating a better reduction in the variation rate. By developing techniques capable of evaluating the properties of individual BaTiO 3 nanocubes, we expect that our work to open the door to the use of BaTiO 3 nanomaterials in the design of future multilayer ceramic capacitors with improved volumetric efficiency and ferroelectrics-enabled nanodevices with advanced functionality.

36 MATERIALS SCIENCE↗
NASA NTRS1970

A Study of the Electrotransport in Thin Films: An Advanced Method for the Study of Electrotransport in Thin Films Using Electrical Resistance Measurements

To date, very little is understood about electrotransport in thin films. One reason for this is the lack of methods in which electromigration can be adequately monitored dynamically. In this thesis, a new nondestructive method for the study of the electrotransport phenomenon in thin aluminum films is presented. This method makes use of electrical resistance measurements of various regions along the test sample to monitor changes in resistance resulting from electromigration. The advantage of this method is that resistance changes can be observed long before void formation can be seen using standard microscopy methods. In order to achieve the best efficiency using this method, special consideration must be given to the design of the sample. Design problems and their respective solutions are given. The results of the electrical resistance measurements are interpreted by means of photographs taken with an scanning electron microscope. The increase in resistance of the aluminum samples is interpreted to be due to void formation. The expected decrease in resistance near the anode was never observed. It is shown that mass accumulation takes on the form of hillocks and whiskers on the surface of the aluminum film, which does not contribute appreciably to conductivity.

Hummel, R. E.↗
DOE OSTI2021

Qualification of 3-D Printed Mortar With Electrical Conductivity Measurements

Additive manufacturing (AM) or 3D printing of concrete allows for construction of arbitrary shape structures without a mold. Since reproducibility of 3D printed concrete is lower than that of conventional fabrication, each 3D printed structure should be monitored for proper curing. Conventional qualification of concrete is based on several tests, including destructive compressive strength measurements. Because a structure is 3-D printed layer-by-layer, the surfaces of AM concrete structures have significant surface roughness. This limits the applicability of conventional nondestructive testing methods. We investigated qualification of 3D printed mortar by monitoring curing with nondestructive electrical conductivity measurements. Bulk resistance of concrete was extracted from electrochemical impedance spectroscopy (EIS measurements made using custom flexible self-adhesive electrodes, which contour to rough surfaces. We show that bulk resistivity of concrete increases linearly with time. This allows for developing a calibration curve for compressive strength lookup from nondestructive electrical conductivity measurements. Conductivity measurements also allow for estimation of formation factor, which is an indicator of mortar permeability.

36 MATERIALS SCIENCE↗
NASA NTRS1971

Room temperature measurements of electrical resistivity and thermal conductivity of various graphites

Room temperature thermal conductivity measurements were completed on 10 graphite samples selected from the lot of 120 to uniformly span the range of electrical resistivity values. From these data and other measurements a thermal conductivity-electrical conductivity correlation was established to predict room temperature thermal conductivity values for the graphite samples. The correlation, expressed by a parabolic equation, represents available thermal and electrical conductivity data to about + or - 8%.

Mcelroy, D. L.↗
NASA NTRS1993

Electric field measurements with an airplane - Problems caused by emitted charge

The temporal variation of electric field components deduced from measurements made with airplanes penetrating electrified clouds is often complex, especially when the airplane experiences strong electrical charging. However, unusually simple electric field variations were obtained for penetrations involving severe charging of an airplane on flights over Kennedy Space Center, Florida, on August 19, 1989. Analysis of these results suggests that plumes of ions were emitted from the airplane. The electric field from these plumes was more intense than the ambient field from the cloud at the location of the aft electric field sensor. As a consequence, the deduced component of the ambient electric field in the direction of flight was severely distorted. These findings emphasize (1) the importance of careful evaluation of electric field data obtained with airplanes and (2) the need for improved measurements.

Jones, J. J.↗
NASA NTRS1986

Electric field measurements during the Condor critical velocity experiment

The instrumentation of the Condor critical velocity Ba experiment (Wescott et al., 1986) for the measurements of the energetic particles and the electric field associated with a Ba explosion is described. The Ba explosion created a complex electric field pulse detected in situ by a single-axis double electric-field probe on a separate spacecraft. The measurements provide evidence of several important links in the critical-velocity chain, and are consistent with two hypotheses. The first hypothesis involves the creation of large polarization electric field due to charge separation; the second hypothesis implies a polarization of the beam by currents flowing across it. The chain of physical processes inferred from the observations is in agreement with most theories for the Alfven process.

Kelley, M. C.↗
NASA NTRS1978

Instrumentation for dc and low-frequency electric-field measurements on ISEE-A

It has been found that systematic measurements of the various properties of electric fields existing in space are required for an understanding of the plasma environment. Progress has, however, been limited by a lack of opportunities to fly the long antenna-probes required for double-probe measurements. The improved capabilities of ISEE-A should make it possible to conduct systematic studies of the spatial extent and variability of the zone of strong E-fields, or fast convection, in adjacent magnetospheric regions. The objectives of the ISEE-A measurements are discussed along with the symmetric double-probe floating-potential technique and the antenna-probe design. A description of the electronic design is also provided, giving attention to dc-field measurements, spin coupled dc-field measurements, and calibration and plasma impedance measurements.

Heppner, J. P.↗
DOE OSTI2022

Electric Field Measurements at the Surface of a Piezoelectric Transformer for Plasma Jet Formation using the Plasma Research Facility at Sandia National Laboratory (Final Report)

The overall goal of this research is to understand how low-temperature non-equilibrium plasmas form directly off the surface of piezoelectric crystals. Specifically, this project aims to temporally and spatially resolve how the electric field evolves on and near the surface of a piezoelectric transformer (PT) at conditions that produce an atmospheric-pressure air plasma jet emanating from the corner of the PT. In this work, we used the Plasma Research Facility (PRF) at Sandia National Laboratory to conduct temporally- and spatially-resolved electric field induced second harmonic (E-FISH) measurements of the electric field at and near the surface of a piezoelectric transformer, providing a fundamental understanding of how piezoelectric crystals can be used for plasma generation. We carried out two Objectives: Objective 1 – The first objective was to measure the temporal and spatial evolution of the electric field along the surfaces approaching the corner of a rectangular PT just below conditions that lead to plasma jet formation. Such a measurement can be used to explain when and where the electric field peaks, leading to plasma formation; Objective 2 – The second objective was to measure the temporal and spatial evolution of the electric field along the surfaces approaching the corner of a rectangular PT just at conditions of plasma jet formation. This, in principle, gives a more accurate determination of how the electric field leads to plasma formation but is more difficult due to the relatively stochastic plasma jet behavior of a PT. This work was complemented by an award from the Sandia PRF, and we worked with Dr. Edward Barnat at the Sandia PRF to carry out these objectives.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗
NASA NTRS1993

Critical review of electrical conductivity measurements and charge distribution analysis of magnesium oxide

The electrical conductivity sigma of MgO single crystals shows a sharp increase at 500-800 C, in particular of sigma surface, generally attributed to surface contamination. Charge Distribution Analysis (CDA), a new technique providing information on fundamental properties that was previously unavailable, allows for the determination of surface charges, their sign and associated internal electric field. Data on 99.99% purity, arc-fusion grown MgO crystals show that mobile charge carriers start to appear in the bulk of the MgO crystals between 200 and 400 C when sigma (measured by conventional techniques) is in t he 10(exp -14) to 10(exp -16) /omega/cm range. Above 500 C, as sigma increases to 10(exp -6) to 10(exp -7)/omega/cm, more charges appear giving rise to a strong positive surface charge supported by a strong internal field. This indicates that charges are generated in the bulk and diffuse to the surface by an internally controlled process. On the basis of their positive sign they are identified as holes (defect electrons). Because of the low cation content of these very pure MgO crystals, theses holes cannnot be associated with transition metal impurties. Instead, they are associated with the O(2-) sublattice, e.g. consist of O(-) states or positive holes. This conclusion is supported by magnetic susceptibility data showing the appearance of 1000 +/- 500 ppm paramagnetic species between 200-500 C. The magnetic data are consistent with strongly coupled, diamagnetic O(-) pairs below 200-500 C, chemically equivalent to peroxy anions, O2(2-), and probably associated with cation vacancies in the MgO matrix. The formation of O2(2-) in arc-fusion grown MgO crystals is very unexpected because of the highly reducing growth conditions. Their presence implies an internal redox reaction involving dissolved 'water' by which OH(-) pairs convert to O2(2-) plus H2 molecules. This redox conversion is supported by mass spectroscopic measurements of the H2 release from highly OH(-)-doped, finely divided MgO and by wet-chemical analysis of its oxidant concentration.

Freund, Friedemann↗
NASA NTRS1973

Extendible-retractable electric field measurement antenna for IMP J

An antenna dispenser mechanism for the IMP J spacecraft was designed, fabricated, and tested. Upon command the mechanism deploys or retracts a conductor for use as a receiving antenna for an electric field measurement experiment. Five identical units were fabricated and tested to the IMP H & J environmental test specification. Of these, four are designated for flight on the IMP J spacecraft and one as a prototype flight spare. The testing program was successfully completed although certain design modifications were required as problems were uncovered by the testing; particularly thermal vacuum operation. The antenna mechanism functions well under the expected environmental and loading conditions. The wear life and load capability of the dry molybdenum disulphide lubricant originally used on the heavily loaded worm and gear pair were disappointing and a substitute material was applied. The lubricant finally applied performed well; although other problems were generated.

Larrick, W.↗
DOE OSTI2023

Direct in situ measurements of electrical properties of solid–electrolyte interphase on lithium metal anodes

The solid–electrolyte interphase (SEI) critically governs the performance of rechargeable batteries. An ideal SEI is expected to be electrically insulative to prevent persistently parasitic reactions between the electrode and the electrolyte and ionically conductive to facilitate Faradaic reactions of the electrode. However, the true nature of the electrical properties of the SEI remains hitherto unclear due to the lack of a direct characterization method. Here we use in situ bias transmission electron microscopy to directly measure the electrical properties of SEIs formed on copper and lithium substrates. We reveal that SEIs show a voltage-dependent differential conductance. A higher rate of differential conductance induces a thicker SEI with an intricate topographic feature, leading to an inferior Coulombic efficiency and cycling stability in Li||Cu and Li||LiNi 0.8 Mn 0.1 Co 0.1 O 2 cells. Further, our work provides insight into the targeted design of the SEI with desired characteristics towards better battery performance.

25 ENERGY STORAGE↗
NASA NTRS2013

Flow Control and Measurement in Electric Propulsion Systems: Towards an AIAA Reference Standard

Accurate control and measurement of propellant flow to a thruster is one of the most basic and fundamental requirements for operation of electric propulsion systems, whether they be in the laboratory or on flight spacecraft. Hence, it is important for the electric propulsion community to have a common understanding of typical methods for flow control and measurement. This paper addresses the topic of propellant flow primarily for the gaseous propellant systems which have dominated laboratory research and flight application over the last few decades, although other types of systems are also briefly discussed. While most flight systems have employed a type of pressure-fed flow restrictor for flow control, both thermal-based and pressure-based mass flow controllers are routinely used in laboratories. Fundamentals and theory of operation of these types of controllers are presented, along with sources of uncertainty associated with their use. Methods of calibration and recommendations for calibration processes are presented. Finally, details of uncertainty calculations are presented for some common calibration methods and for the linear fits to calibration data that are commonly used.

thrust measurement↗
DOE OSTI2025

Measurement of electrical characteristics of Ge-based diodes with thermal GeO2 films exposed to controlled humidity conditions

We investigated the impact of the interaction between gas-phase water molecules and thermally oxidized GeO2 on Ge on the performance of metal–oxide–semiconductor (MOS) structures. A vacuum-integrated setup was developed to form MOS diodes with a GeO2/Ge structure that had been exposed to controlled humidity conditions and to subsequently measure their electrical characteristics in situ. The capacitance–voltage (C–V) curves exhibited a significant negative shift, indicating the generation of positive charges at the GeO2/Ge interface when the GeO2 surface was exposed to humidity levels above approximately 1%. According to a previous study using electron spectroscopy, this threshold corresponds to the humidity level at which molecular water begins to grow on a GeO2/Ge structure. It is likely that gas-phase water molecules infiltrating the GeO2 film bind to local OH sites via hydrogen bonding, leading to the formation of positive fixed charges at the GeO2/Ge interface.

Sano, Shuto↗
NASA NTRS1982

A thundercloud electric field sounding - Charge distribution and lightning

An instrumented free balloon measured electric fields and field changes as it rose through a thundercloud above Langmuir Laboratory, New Mexico. The variation of the electric field with altitude implied that the cloud contained negative space charge of density -0.6 to -4 nC/cu m between 5.5 and 8.0 km MSL. The environmental temperature at these levels ranged from -5 to -20 C. The measurements imply that the areal extent of this negative charge center was significantly greater than that of the cloud's intense precipitation shafts. At altitudes greater than 8 km, the instrument ascended past net positive charge. In addition, positive space charge adjacent to the earth's surface (concentration 0.6 nC/cu m and in the lowest portion of the cloud (1.0 nC/cu m) is inferred from the measurements. Electric field changes from intracloud lightning were interpreted by using a simple model for the developing streamer of the initial phase. Thunder source reconstructions provided estimates for the orientation of lightning channels. Seven 'streamers' so analyzed propagated on the average, at 50,000 m/s and carried a current of 390 A. The mean charge dissipated during a flash was 30 C.

Weber, M. E.↗
NASA NTRS2004

Classification of Tropical Oceanic Precipitation Using High Altitude Aircraft Microwave and Electric Field Measurements

A physically intuitive and computationally simple precipitation mapping algorithm has been developed for use with the airborne Advanced Microwave Precipitation Radiometer (AMPR). The algorithm is based on microwave emission and scattering properties of precipitation. Specifically, emission by liquid water allows increasing brightness temperatures at low frequencies to be interpreted as increasing rain rates. Scattering by large hydrometeors (particularly graupel and hail) causes relative minima in the brightness temperatures, with progressively larger hydrometeors scattering progressively longer wavelengths. The vigor of convection is therefore ascertained according to which wavelengths are being significantly scattered. The combination of emission and scattering information from four microwave channels is used to assign a precipitation category, which is related to the liquid rain rate, the vertical extent of precipitation, and the vigor of convection. The qualitative precipitation categories output by the passive microwave algorithm have been verified using coincident radar (ER-2 Doppler Radar - EDOP) and electric field measurements (Lightning Instrument Package - LIP). These coincident measurements can subsequently be used to quantify rain rates, hydrometeor contents, and vertical profiles that are typical for each precipitation category. This algorithm has been developed using an airborne platform. Comparisons are being made with other airborne, satellite, and ground-based radar and radiometer data. This technique shows promise both as a research tool and potentially as a real-time analysis tool, which could be applied to either traditional or uninhabited aerial vehicles.

Cecil, Daniel J.↗