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At least 145 records · Page 8

All sources NASA NTRS DOE OSTI

NASA NTRS2003

Preliminary Results of a Microgravity Investigation to Measure Net Charge on Granular Materials

Accurate characterization of the electrostatic charge on granular materials has typically been limited to materials with diameters on the order of 10 microns and below due to high settling velocities of larger particles. High settling velocities limit both the time and the acceptable uncertainty with which a measurement can be made. A prototype device has been developed at NASA Glenn Research Center (GRC) to measure coulombic charge on individual particles of granular materials that are 50 to 500 microns in diameter. This device, a novel extension of Millikan's classic oil drop experiment, utilizes the NASA GRC 2.2 second drop tower to extend the range of electrostatic charge measurements to accommodate moderate size granular materials. A dielectric material with a nominal grain diameter between 1.06 and 250 microns was tribocharged using a dry gas jet, suspended in a 5x10x10 cm enclosure during a 2.2 second period of microgravity and exposed to a known electric field. The response was recorded on video and post processed to allow tracking of individual particles. By determining the particle trajectory and velocity, estimates of the coulombic charge were made. Over 30 drops were performed using this technique and the analysis showed that first order approximations of coulombic charge could successfully be obtained, with the mean charge of 3.4E-14 coulombs measured for F-75 Ottawa quartz sand. Additionally, the measured charge showed a near-Gaussian distribution, with a standard deviation of 2.14E -14 coulombs.

Green, Robert D.↗

NASA NTRS2012

Evaluating Material Flammability in Microgravity and Martian Gravity Compared to the NASA Standard Normal Gravity Test

Drop tower tests are conducted at Martian gravity to determine the flammability of three materials compared to previous tests in other normal gravity and reduced gravity environments. The comparison is made with consideration of a modified NASA standard test protocol. Material flammability limits in the different gravity and flow environments are tabulated to determine the factor of safety associated with normal gravity flammability screening. Previous testing at microgravity and Lunar gravity indicated that some materials burned to lower oxygen concentrations in low gravity than in normal gravity, although the low g extinction limit criteria are not the same as 1g due to time constraints in drop testing. Similarly, the data presented in this paper for Martian gravity suggest that there is a gravity level below Earth s at which materials burn more readily than on Earth. If proven for more materials, this may indicate the need to include a factor of safety on 1g flammability limits.

Oslon, Sandra. L.↗

DOE OSTI2025

Comparison of interlaminar damage modeling strategies for hybrid composite/aluminum laminates subjected to low-velocity impact

Low-velocity impact of hybrid metal-composite structures was investigated experimentally and computationally. Composite laminates consisting of 2D woven glass fiber reinforced polymer (GFRP) and carbon fiber reinforced polymer (CFRP) were joined with a 6061-T6 aluminum plate using an epoxy adhesive. Two variations of the structure were studied; one consisting of all plies oriented at 0° and one consisting of all plies oriented at 45°. A drop tower was used to impact structures at a range of energies, including energies above and below the threshold at which the aluminum layer was perforated. Numerical simulations were implemented using Sierra/SM, an in-house transient dynamics finite element code developed at Sandia National Laboratories. A Hosford plasticity model was used to describe the response of the aluminum layer. A newly implemented orthotropic continuum damage mechanics (CDM) constitutive model was used to represent the composite laminate. This 3D-CDM model was compared to a cohesive zone model (2D-CDM/CZM) to investigate efficacy of aluminum perforation energy prediction, delamination prediction, and computational cost. Accuracy of each model was evaluated using the experimental results. Each showed good agreement with the tests for both the force and velocity histories, as well as the observed damage mechanisms. The 2D-CDM/CZM model was marginally more accurate in capturing both the composite and aluminum behavior — this model averaged error percentages of -11.2% and 10.8% for residual velocity and peak force, respectively. Meanwhile, the 3D-CDM model predictions yielded average error percentages of -35.5% (velocity) and 22.6% (force). However, the 3D-CDM model generally resulted in a decreased computational cost; the average run time was 14% shorter than the 2D-CDM/CZM model and 3x as many timesteps per hour were computed using the same computational resources. In conclusion, new experimental data on the impact and perforation resistance of metal-composite laminates is presented in addition to numerical predictions of the impact behavior.

Carbon fiber↗

DOE OSTI2022

Elucidating the challenges in extracting ultra-slow flame speeds in a closed vessel - A CH 2 F 2 microgravity case study using optical and pressure-rise data

Refrigerants with a low global warming potential (GWP) possess mild flammability. Hence, a fundamental understanding of their combustion characteristics is required to assess their fire-hazardous potential. The laminar burning velocity is one fundamental property to describe these under safety evaluation aspects. However, measuring laminar burning velocities for slow-burning components, such as low-GWP alternatives, is challenging. This is due to influencing effects such as buoyant flame deformation, stretch, radiation, and confinement, especially at the flammability limits. Here, in the present study, we investigated near-limit flames of the representative refrigerant difluoromethane (CH 2 F 2 ) with nitrogen-enriched oxidizer mixtures to elucidate the potentials and limitations at ultra-slow flame speeds of two widely used flame speed measurement methods in the closed vessel configuration: the optical flame speed measurement in the early quasi-isobaric regime and the flame speed determination from the pressure-rise during the later phase of the isochoric combustion process. Experiments were performed under terrestrial- and microgravity, conducted in a specially designed setup suitable for drop tower applications, using both methods in parallel. Recommendations for the extraction of flame speed data are derived from the non-buoyant reference investigations under microgravity and transferred to ultra-slow flames at terrestrial gravity. Near-limit flames under microgravity were found to be significantly affected by stretch effects for the optical method so that flame speed extrapolations to unstretched conditions are prone to errors. Stretch also affects the pressure method’s lower evaluation limit, and errors can be estimated by combining flame speed data from the pressure method and Markstein lengths from optical experiments.

42 ENGINEERING↗

DOE OSTI2016

A three-layer magnetic shielding for the MAIUS-1 mission on a sounding rocket

Bose-Einstein-Condensates (BECs) can be used as a very sensitive tool for experiments on fundamental questions in physics like testing the equivalence principle using matter wave interferometry. Since the sensitivity of these experiments in ground-based environments is limited by the available free fall time, the QUANTUS project started to perform BEC interferometry experiments in micro-gravity. After successful campaigns in the drop tower, the next step is a space-borne experiment. The MAIUS-mission will be an atom-optical experiment that will show the feasibility of experiments with ultra-cold quantum gases in microgravity in a sounding rocket. The experiment will create a BEC of 10{sup 5} {sup 87}Rb-atoms in less than 5 s and will demonstrate application of basic atom interferometer techniques over a flight time of 6 min. The hardware is specifically designed to match the requirements of a sounding rocket mission. Special attention is thereby spent on the appropriate magnetic shielding from varying magnetic fields during the rocket flight, since the experiment procedures are very sensitive to external magnetic fields. A three-layer magnetic shielding provides a high shielding effectiveness factor of at least 1000 for an undisturbed operation of the experiment. The design of this magnetic shielding, the magnetic properties, simulations, and tests of its suitability for a sounding rocket flight are presented in this article.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

DOE OSTI2023

VIPIR: A High-Throughput Drop-Weight Impact Instrument for Imaging the Initiation and Propagation of Reactions in Energetic Materials

Characterizing the handling safety and sensitivity of explosives has been a challenging area of study for over 60 years. Historically one of the most accessible and widely utilized experiments has been the drop-weight impact test, which involves dropping a weight on a small sample sandwiched between two anvils. Because this experiment generally only utilizes sound thresholds to determine whether or not a sample reacted, the physical and chemical properties governing sensitivity remain convolved. Better understanding of chemical and material characteristics is needed to give the chemistry and engineering communities a predictive tool to determine the handling sensitivity of explosives prior to pursuing expensive and potentially hazardous synthesis and formulation operations. Here, we are developing a high throughput drop tower instrument capable of imaging the deformation and flow of energetic materials during impact and the resulting thermal ignition and propagation events. This instrument is based on previous designs but has been modified for higher throughput and tailorable modifications in the future. Herein, we present key design features that enable high-speed visible and thermal imaging of explosive initiation by sub-shock impacts, as well as preliminary results in which ignition sites were observed in an erythritol tetranitrate sample.

47 OTHER INSTRUMENTATION↗

DOE OSTI2013

COLLIDING DECIMETER DUST

Collisional evolution is a key process in planetesimal formation and decimeter bodies play a key role in the different models. However, the outcome of collisions between two dusty decimeter bodies has never been studied experimentally. Therefore, we carried out microgravity collision experiments in the Bremen drop tower. The agglomerates consist of quartz with irregularly shaped micrometer-sized grains and the mean volume filling factor is 0.437 {+-} 0.004. The aggregates are cylindrical with 12 cm in height and 12 cm in diameter, and typical masses are 1.5 kg. These are the largest and most massive dust aggregates studied in collisions to date. We observed rebound and fragmentation but no sticking in the velocity range between 0.8 and 25.7 cm s{sup -1}. The critical fragmentation velocity for split up of an aggregate is 16.2 {+-} 0.4 cm s{sup -1}. At lower velocities the aggregates bounce off each other. In this velocity range, the coefficient of restitution decreases with increasing collision velocity from 0.8 to 0.3. While the aggregates are very weak, the critical specific kinetic energy for fragmentation Q{sub {mu}=1} is a factor of six larger than expected. Collisions of large bodies in protoplanetary disks are supposed to be much faster and the generation of smaller fragments is likely. In planetary rings, collision velocities are of the order of a few cm s{sup -1} and are thereby in the same range investigated in these experiments. The coefficient of restitution of dust agglomerates and regolith-covered ice particles, which are common in planetary rings, are similar.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2015

Photophoretic Strength on Chondrules. 2. Experiment

Abstract not provided

Loesche, Christoph↗

DOE OSTI2014

Macroscopic dust in protoplanetary disks—from growth to destruction

The collision dynamics of dusty bodies are crucial for planetesimal formation. Decimeter agglomerates are especially important in the different formation models. Therefore, in continuation of our experiments on mutual decimeter collisions, we investigate collisions of centimeter onto decimeter dust agglomerates in a small drop tower under vacuum conditions (p ≲ 5 × 10{sup –1} mbar) at a mean collision velocity of 6.68 ± 0.67 m s{sup –1}. We use quartz dust with irregularly shaped micrometer grains. Centimeter projectiles with different diameters, masses, and heights are used, their typical volume filling factor is Φ {sub p,} {sub m} = 0.466 ± 0.02. The decimeter agglomerates have a mass of about 1.5 kg, a diameter and height of 12 cm, and a mean filling factor of Φ {sub t,} {sub m} = 0.44 ± 0.004. At lower collision energies, only the projectile gets destroyed and mass is transferred to the target. The accretion efficiency decreases with increasing obliquity and increasing difference in filling factor, if the projectile is more compact than the target. The accretion efficiency increases with increasing collision energy for collision energies under a certain threshold. Beyond this threshold at 298 ± 25 mJ, catastrophic disruption of the target can be observed. This corresponds to a critical fragmentation strength Q* = 190 ± 16 mJ kg{sup –1}, which is a factor of four larger than expected. Analyses of the projectile fragments show a power-law size distribution with an average exponent of –3.8 ± 0.3. The mass distributions suggest that the fraction of smallest fragments increases for higher collision energies. This is interesting for impacts of small particles on large target bodies within protoplanetary disks, as smaller fragments couple better to the surrounding gas and re-accretion by gas drag is more likely.

79 ASTRONOMY AND ASTROPHYSICS↗

DOE OSTI2014

A novel drop weight impact setup for testing reinforced concrete beams

A novel method of testing reinforced concrete beams under impact using a drop tower is described. The method consists of configuring the support conditions and instrumenting both the loading end of the hammer and support points in such a way that a proper dynamic analysis of the impact event can be performed and rational data can be derived.

42 ENGINEERING↗

DOE OSTI2018

Battery Safety Testing

25 ENERGY STORAGE↗

DOE OSTI2017

Battery Testing FY 2017 Annual Progress Report

Abuse tests are designed to determine the safe operating limits of HEV\PHEV energy storage devices. Testing is intended to achieve certain worst-case scenarios to yield quantitative data on cell\module\pack response, allowing for failure mode determination and guiding developers toward improved materials and designs. Standard abuse tests with defined start and end conditions are performed on all devices to provide comparison between technologies. New tests and protocols are developed and evaluated to more closely simulate real-world failure conditions. When scaling from cell to the battery level, a detailed understanding of cell interactions provides insight on safety performance. Single point failures from a cell or group of cells can be initiated by a number of triggers including internal short circuit, misuse or abuse, or component failure at the battery or system level. Propagation of a single failure event (regardless of the initiation trigger) through an entire battery, system, or vehicle is an unacceptable outcome with regards to EV battery safety. In this FY, our work has focused on evaluating the propagation of a single cell thermal runaway event through a battery using a variety of design considerations with an emphasis on passive thermal management impacts. This has been coupled with thermal modeling by NREL for these testing conditions. In addition, alternative failure initiation methods have been evaluated to provide direct comparisons of possible energy injection between modes. This data was compiled to better identify what propagation test method is appropriate given certain battery designs. Expanding the analysis of short circuit current during failure propagation has been done for EV relevant chemistries. Ongoing test development and validation to obtain these values has been achieved. While robust mechanical models for vehicles and vehicle components exist, there is a gap for mechanical modeling of EV batteries. The challenge with developing a mechanical model for a battery is the heterogeneous nature of the materials and components (polymers, metals, metal oxides, liquids). Our work will provide empirical data on the mechanical behavior of batteries under compressive load to understand how a battery may behave in a vehicle crash scenario. This work is performed in collaboration with the U.S. Council for Automotive Research (USCAR) and Computer Aided Engineering of Batteries (CAEBAT). These programs have supported the design and development of a drop tower testing apparatus to close the gap between cell/string level testing and full scale crash testing with true dynamic rate effects.

25 ENERGY STORAGE↗

DOE OSTI2020

Battery Abuse Testing

25 ENERGY STORAGE↗

DOE OSTI2020

Combustion of Butyl acetate as an alternative additive to petroleum fuels

Blending petroleum fuels with oxygenates is a common approach to stem the depletion of crude oil while also mitigating the impact of their combustion on the environment. It has recently been considered that butyl acetate (BA, C6H12O2 , boiling point of 399K) could be a viable oxygenate additive to diesel fuel. The platform used to study combustion of commercial and synthesized BA was an isolated droplet burning with spherical symmetry. The experiments were carried out in a drop tower to minimize buoyant convection. Restricting motion by supporting droplets on 14 micrometer fibers eliminated forced convection. Precise control of the initial diameter was achieved by first deploying large droplets and letting them evaporate to the size of interest, here being between 0.3 mm to 0.8 mm. The experimental results show that commercial and the newly synthesized BA burned almost identically for the evolution of droplet and flame diameters. Droplets burned slower as the initial diameter was increased and soot formation was noted for the larger sizes studied due to a residence size effect. Burning in a buoyant convective field showed higher burn rates due to the convective effect and that the asymmetric flames became nearly spherical as diameter decreased. The study illustrates the significant value that the microgravity environment brings to evaluating performance of oxygenated fuels synthesized by new production methods.

Wang, Yujie↗

NASA NTRS1968