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DOE OSTI2022

Hydrocarbon ladder polymers with ultrahigh permselectivity for membrane gas separations

Membranes have the potential to substantially reduce energy consumption of industrial chemical separations, but their implementation has been limited owing to a performance upper bound—the trade-off between permeability and selectivity. Although recent developments of highly permeable polymer membranes have advanced the upper bounds for various gas pairs, these polymers typically exhibit limited selectivity. We report a class of hydrocarbon ladder polymers that can achieve both high selectivity and high permeability in membrane separations for many industrially relevant gas mixtures. Additionally, their corresponding films exhibit desirable mechanical and thermal properties. Tuning of the ladder polymer backbone configuration was found to have a profound effect on separation performance and aging behavior.

Science & Technology - Other Topics↗

DOE OSTI2025

Three-dimensional nucleation and growth of deformation twins in magnesium

At two-thirds the weight of aluminum, magnesium alloys have the potential to reduce the fuel consumption of transportation vehicles. These advancements depend on our ability to optimize the desirable versus undesirable effects of deformation twins, which are three-dimensional (3D) microstructural domains that form under mechanical stresses. Previously only characterized through surface or thin-film measurements, we here present 3D in situ characterization of deformation twinning inside an embedded grain over mesoscopic fields of view using dark-field x-ray microscopy supported by crystal plasticity finite element analysis. The results revealed the role of triple junctions on twin nucleation and the sequence and irregularity of twin growth and showed that twin-grain junctions, twin-twin junctions, and twin boundaries were the sites of localized dislocation accumulation.

Lee, Sangwon [Univ. of Michigan, Ann Arbor, MI (Un↗

DOE OSTI2024

Electrochemical Reactivity of Hydrogen Storage Materials: Exploring Borohydride and Hydrazinium Salt Mixtures

Electrochemical characterization of hydrogen storage materials was conducted in a non-aqueous environment to investigate the direct electrochemical release and consumption of hydrogen and the potential for regeneration. We first address the challenge of minimal solubility of the synthetic precursors, sodium borohydride (NaBH 4 ) and hydrazinium bromide (N 2 H 5 Br), in both organic and inorganic solvents. We next determine and calibrate a reference electrode formulation compatible with our non-aqueous media and analytes that demonstrates a stable reference potential. We employ cyclic voltammetry (CV) to characterize the precursors and mixtures thereof. Each CV peak is assigned to a corresponding electrochemical reaction. Using the rate-dependent CV method and Randles–Ševčík equation, we calculate the diffusion coefficient of each chemical (NaBH 4 and N 2 H 5 Br). Analysis of the CVs, coupled with 11B NMR analysis, reveals a room temperature chemical transformation of NaBH 4 and N 2 H 5 Br mixtures into hydrazine borane (N 2 H 4 BH 3 ). These results are particularly significant, considering the limited information available on the electrochemical characterization of metal borohydride and hydrazinium salt in non-aqueous media. This work establishes a foundation for adapting a non-aqueous electrochemical system to further study the borohydride family of chemistries and to design and develop electrochemical devices for direct electrical and chemical energy interconversion with hydrogen storage materials.

08 HYDROGEN↗

DOE OSTI2026

Tabulated data for Lignin-Derived Phenolic Compounds and Water Are Effective Cosolvents for Reductive Catalytic Fractionation

Reductive catalytic fractionation (RCF) is an effective lignin-first biorefining method to extract lignin as a stabilized oil from lignocellulosic biomass. To realize RCF at scale, process modeling has shown that minimizing the use of exogenous organic solvents is critical. To this end, here we investigate the ability of lignin-derived monomers to act as either solvents or cosolvents for RCF. We begin by examining the influence of lignin-derived aromatic compounds (4-propylguaiacol, 4-propylphenol, and propylbenzene) on RCF monomer yields and subsequently extend our analysis to mixtures of 4-propylguaiacol and either methanol or water. We demonstrate that 4-propylguaiacol is an effective solvent for lignin extraction and depolymerization during RCF, especially when used in combination with water as a cosolvent. Cosolvent mixtures of 4-propylguaiacol and water enable up to 81% lignin extraction, monomer yields up to 25 wt %, and postreaction phase separation. However, unlike methanol, water as a cosolvent fails to inhibit aromatic ring hydrogenation when conducted over Ru/C as a catalyst, potentially leading to excess hydrogen consumption in a process utilizing this approach. Nonetheless, these results suggest a promising strategy for eliminating external organic solvents from RCF by utilizing mixtures of lignin-derived compounds and water as alternative extraction solvents. This is the tabulated data for the paper

biorefining↗

DOE OSTI2026

Calculation of monomer yields, verification of PG concentration approximation, catalyst comparison for neat aromatic RCF, SEM micrographs for postreaction pulps, yields of aqueous-phase sugar derivatives after PG-H2O RCF, reactor pressure transients, GPC comparing pre- and postreaction organic solvent composition, PG-H2O miscibility testing, GPC probing dimer/oligomer fractionation in PG-H2O mixtures for

biorefining↗

DOE OSTI2026

Lignin-Derived Phenolic Compounds and Water Are Effective Cosolvents for Reductive Catalytic Fractionation

biorefining↗

NASA NTRS1974

Rating aircraft on energy

Questions concerning the energy efficiency of aircraft compared to ground transport are considered, taking into account as energy intensity the energy consumed per passenger statute mile. It is found that today's transport aircraft have an energy intensity potential comparable to that of ground modes. Possibilities for improving the energy density are also much better in the case of aircraft than in the case of ground transportation. Approaches for potential reductions in aircraft energy consumption are examined, giving attention to steps for increasing the efficiency of present aircraft and to reductions in energy intensity obtainable by the introduction of new aircraft utilizing an advanced technology. The use of supercritical aerodynamics is discussed along with the employment of composite structures, advances in propulsion systems, and the introduction of very large aircraft. Other improvements in fuel economy can be obtained by a reduction of skin-friction drag and a use of hydrogen fuel.

Maddalon, D. V.↗

NASA NTRS1989

Comparisons between Intel 386 and i486 microprecessors

A quick and preliminary comparison is made between the Intel 386 and i486 microprocessors. The following topics are discussed: the i486 key elements, comparison of instruction set architecture, the i486 on-chip cache characteristics, the i486 multiprocessor support, comparison of performance, comparison of power consumption, comparison of radiation hardening potential, and recommendations for the Space Station Freedom (SSF) Data Management System (DMS).

Liu, Yuan-Kwei↗

NASA NTRS2011

Effect of Graphene Addition on Shape Memory Behavior of Epoxy Resins

Shape memory polymers (SMPs) and composites are a special class of smart materials known for their ability to change size and shape upon exposure to an external stimulus (e.g. light, heat, pH, or magnetic field). These materials are commonly used for biomedical applications; however, recent attempts have been made towards developing SMPs and composites for use in aircraft and space applications. Implementing SMPs and composites to create a shape change effect in some aircraft structures could potentially reduce drag, decrease fuel consumption, and improve engine performance. This paper discusses the development of suitable materials to use in morphing aircraft structures. Thermally responsive epoxy SMPs and nanocomposites were developed and the shape memory behavior and thermo-mechanical properties were studied. Overall, preliminary results from dynamic mechanical analysis (DMA) showed that thermally actuated shape memory epoxies and nanocomposites possessed Tgs near approximately 168 C. When graphene nanofiller was added, the storage modulus and crosslinking density decreased. On the other hand, the addition of graphene enhanced the recovery behavior of the shape memory nanocomposites. It was assumed that the addition of graphene improved shape memory recovery by reducing the crosslinking density and increasing the elasticity of the nanocomposites.

Williams, Tiffany↗

NASA NTRS2007

Real-Time Wireless Data Acquisition System

Current and future aerospace requirements demand the creation of a new breed of sensing devices, with emphasis on reduced weight, power consumption, and physical size. This new generation of sensors must possess a high degree of intelligence to provide critical data efficiently and in real-time. Intelligence will include self-calibration, self-health assessment, and pre-processing of raw data at the sensor level. Most of these features are already incorporated in the Wireless Sensors Network (SensorNet(TradeMark)), developed by the Instrumentation Group at Kennedy Space Center (KSC). A system based on the SensorNet(TradeMark) architecture consists of data collection point(s) called Central Stations (CS) and intelligent sensors called Remote Stations (RS) where one or more CSs can be accommodated depending on the specific application. The CS's major function is to establish communications with the Remote Stations and to poll each RS for data and health information. The CS also collects, stores and distributes these data to the appropriate systems requiring the information. The system has the ability to perform point-to-point, multi-point and relay mode communications with an autonomous self-diagnosis of each communications link. Upon detection of a communication failure, the system automatically reconfigures to establish new communication paths. These communication paths are automatically and autonomously selected as the best paths by the system based on the existing operating environment. The data acquisition system currently under development at KSC consists of the SensorNet(TradeMark) wireless sensors as the remote stations and the central station called the Radio Frequency Health Node (RFHN). The RFF1N is the central station which remotely communicates with the SensorNet(TradeMark) sensors to control them and to receive data. The system's salient feature is the ability to provide deterministic sensor data with accurate time stamps for both time critical and non-time critical applications. Current wireless standards such as Zigbee(TradeMark) and Bluetooth(Registered TradeMark) do not have these capabilities and can not meet the needs that are provided by the SensorNet technology. Additionally, the system has the ability to automatically reconfigure the wireless communication link to a secondary frequency if interference is encountered and can autonomously search for a sensor that was perceived to be lost using the relay capabilities of the sensors and the secondary frequency. The RFHN and the SensorNet designs are based on modular architectures that allow for future increases in capability and the ability to expand or upgrade with relative ease. The RFHN and SensorNet sensors .can also perform data processing which forms a distributed processing architecture allowing the system to pass along information rather than just sending "raw data points" to the next higher level system. With a relatively small size, weight and power consumption, this system has the potential for both spacecraft and aircraft applications as well as ground applications that require time critical data.

Valencia, Emilio J.↗

NASA NTRS2016

Non-Contacting Finger Seals Static Performance Test Results at Ambient and High Temperatures

The non-contacting finger seal is an advanced seal concept with potential to reduce specific fuel consumption in gas turbine engines by 2 to 3 percent with little to no wear of the seal or rotor. Static performance tests and bind-up tests of eight different non-contacting finger seal configurations were conducted in air at pressure differentials up to 689.4 kPa and temperatures up to 922 K. Four of the seals tested were designed to have lift pads concentric to a herringbone-grooved rotor which generates hydrodynamic lift when rotating. The remaining seals were tested with a smooth rotor; one seal had a circumferential taper and one had an axial taper on the lift pad inner diameter to create hydrodynamic lift during rotation. The effects of the aft finger axial thickness and of the forward finger inner diameter on leakage performance were investigated as well and compared to analytical predictions.

static tests↗

NASA NTRS2016

Non-Contacting Finger Seals Static Performance Test Results at Ambient and High Temperatures

The non-contacting finger seal is an advanced seal concept with potential to reduce specific fuel consumption in gas turbine engines by 2 to 3 with little to no wear of the seal or rotor. Static performance tests and bind-up tests of eight different non-contacting finger seal configurations were conducted in air at pressure differentials up to 689.4 kPa and temperatures up to 922 K. Four of the seals tested were designed to have lift pads concentric to a herringbone-grooved rotor which generates hydrodynamic lift when rotating. The remaining seals were tested with a smooth rotor; one seal had a circumferential taper and one had an axial taper on the lift pad inner diameter to create hydrodynamic lift during rotation. The effects of the aft finger axial thickness and of the forward finger inner diameter on leakage performance were investigated as well and compared to analytical predictions.

rotors↗

NASA NTRS2018

Exploration of Backscatter Methods for Wireless Avionics

This report describes and characterizes the low-power Jeeva Passive Radio systems, including Wanscatter (passive Chirp Spread Spectrum) and Passive Wi-Fi, with respect to their applicability to wireless avionics. The Wireless Avionics Intra-Communications (WAIC) objectives document, ITU-R M.2197, describes a number of applications of wireless avionics, and lists requirements specifications for each. Additionally, it describes models for compartments and areas of aircraft or vehicles in which wireless avionics would be applied. This exploratory study attempts to map Jeeva's Passive Radio technology to those scenarios outlined in the ITU-R M.2197 operational objectives document, and determine the areas and applications for which it is most suitable. Jeeva Passive Radio operates differently than conventional radios. In a conventional radio, a sensor-connected radio node must actively emit a signal in order to communicate. In a Jeeva Passive Radio system, that node instead simply reflects radio frequency energy which is emitted by another nearby device (called the Companion), which can be "plugged in" or otherwise has access to more power. Using reflections, a data packet can be generated and interpreted by a standard receiver. This method of communication inherently uses less energy, resulting in the potential for far lower power consumption and thus far longer battery life. Overall, 68.4% of use cases described by the ITU-R M.2197 operational objectives document were found to be addressable by Jeeva's Passive Radio systems (26 addressable of 38 total), with 26 of those best addressable by Wanscatter and three found to be best addressable with passive Wi-Fi. See Section 4.2 for a detailed breakdown of application suitability. The most fitting types of applications were in the LI (Low-rate Indoors) and LO (Low-rate Outdoors) categories, where lower rates were acceptable and thus Wanscatter could be applied and its much better uplink sensitivity leveraged. Jeeva has identified the Wanscatter (Chirp Spread Spectrum) system as likely holding the most promise for applications such as those outlined in the ITU-R M.2197 operational objectives document. We recommend that Wanscatter be a technology considered for adoption in wireless avionics.

Backscatter↗

NASA NTRS2017

Hydrazine Conservation for the Dawn Spacecraft Operations at the Dwarf Planet Ceres

Dawn is a low-thrust interplanetary spacecraft currently orbiting the dwarf planet Ceres. After successfully completing its Vesta and Ceres prime missions, Dawn is now in its extended mission, continuously exploring Ceres. After losing the second reaction wheel assembly at the end of the Vesta mission, the feasibility of the Ceres mission was at risk due to the potentially significant increase in hydrazine consumption from using only the reaction control system thrusters. This paper summarizes the intense, collaborative efforts undertaken by the project to conserve hydrazine prior to Vesta departure, during cruise to Ceres, and throughout the Ceres mission. The project’s efforts in minimizing the number of turns are discussed. A special emphasis is given to describing various efforts taken by the Attitude Control Subsystem team in an attempt to reduce hydrazine consumption. These efforts include: changing default slew rates, control gain tuning, changing nadir pointing strategy with Ahead Cross Nadir pointing, hybrid control implementation using hydrazine based thrusters and two remaining reaction wheels, optimal science turn location analysis, and reaction wheel angular momentum management strategies for reducing the number of momentum unloadings. In addition to the Attitude Control Subsystem team’s efforts, the Mission Design and Navigation team’s efforts taken in designing hydrazine friendly orbit transfers are discussed. The trade study performed collaboratively by the Attitude Control Subsystem team and the Science Operations Support Team in choosing hydrazine friendly off-nadir targets is also discussed. Various simulation results are presented and compared against actual flight data obtained. Lastly, remaining hydrazine status at the end of the prime Ceres mission and the hydrazine management planning for the extended mission are discussed.

Salami, Mana↗

DOE OSTI2021

An enterprise control assessment case study of the energy–water nexus for the ISO New England system

Not Available

Muhanji, Steffi Olesi↗

NASA NTRS1975

An early glimpse at long-term subsonic commercial turbofan technology requirements

This paper reports on the exploratory investigation and initial findings of the study of future turbofan concepts to conserve fuel. To date, these studies have indicated a potential reduction in cruise thrust specific fuel consumption in 1990 turbofans of approximately 15% relative to present day new engines through advances in internal aerodynamics, structure-mechanics, and materials. Advanced materials also offer the potential for fuel savings through engine weight reduction. Further studies are required to balance fuel consumption reduction with sound airlines operational economics.

Gray, D. E.↗

DOE OSTI2022

Regionalized Life-Cycle Water Impacts of Microalgal-Based Biofuels in the United States

While algal biofuels have the potential to reduce the national reliance on fossil fuels, high water consumption associated with algal biomass cultivation represents a major concern potentially compromising the sustainable commercialization of this technology. This study focuses on quantifying the water footprint (WF) and water scarcity footprint (WSF) of renewable diesel derived from algal biomass and provides insights into where algal cultivation is less water-intensive than traditional ethanol and biodiesel feedstocks. Results are generated with an engineering process model developed to predict the life-cycle water consumption, considering green, blue, and gray water, of algae facilities across the United States at a high spatiotemporal resolution. The total WFs for Florida and Arizona are determined to be 13.1 and 17.6 m 3 GJ –1 , respectively. The blue WF in Arizona is shown to be 8.5 times larger than in Florida, while the green WF is 4.5 times smaller, but when combined into a total WF, there is just a 26% difference between the two locations. The analysis reveals that the total life-cycle WFs of algal renewable diesel are smaller than the optimal WFs of corn ethanol and soybean biodiesel. Algal systems benefit from higher growth rates and offer the opportunity to manage wastewater streams, therefore generating smaller green and gray WFs than those of conventional biofuels. Here, the WSF analysis identifies the Gulf Coast as the most suitable region for algal cultivation, with cultivation in the western US shown to exacerbate local water stress levels.

54 ENVIRONMENTAL SCIENCES↗

NASA NTRSDate not supplied

The Microbiology of Microgreens Grown in Controlled Environment Chambers under ISS Conditions

Microgreens have been identified as a new type of pick-and-eat salad crop that can be utilized in space crop production systems. The majority of traditionally grown leafy green crops can be grown as microgreens, in addition to crops such as legumes, sunflower, buckwheat, most herbs, and corn, presenting hundreds of microgreen crop options. Notably, microgreens are nutrient dense, high in beneficial compounds like antioxidants, Vitamins C and K, and exhibit a variety of desirable flavors and textures.The short growth cycles (7-14 days), low water requirements and volume optimization potential make them a viable option for sustainable production of nutritious and flavorful crops in space.The crop production team at Kennedy Space Center is investigating the food safety aspects of microgreens grown under spaceflight relevant conditions for crew consumption. Microbiological analysis and screening for potential foodborne pathogens was performed on over 20 varieties of microgreens that have demonstrated positive horticultural attributes.Additionally, a comparison of microgreens grown hydroponically under ISS environmental conditions and similar varieties from local markets was completed to collect baseline data on the microbial load on microgreens. In aneffort to improve microgreen quality, strategies to reduce the microbial load were tested, including bulk seed sanitization, harvest age, exposure to high blue light, and post-harvest chemical disinfection. The efficacy of a citric acid-based produce wash currently used for ISS grown produce and 1% H2O2were investigated at different exposure times for reduction in bacterial and fungal counts on a variety of microgreens. Limited log reduction was achieved depending on exposure time.Our testing also demonstrated that seed sanitization impacted microbial load on microgreens and systems.

Mary E. Hummerick↗