Surface tension measurements in air of liquid lubricants to 200 C by the differential maximum bubble pressure technique
Differential-maximum-bubble-pressure apparatus used for surface tension measurements in air of liquid lubricants to 200 C
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Differential-maximum-bubble-pressure apparatus used for surface tension measurements in air of liquid lubricants to 200 C
This experiment was designed to determine the extent of surface tension induced convection caused by a steplike compositional variation in a liquid metal. Preliminary results are presented.
Discussion of the propellant management system requirements derived for the Viking 75 mission, and review of a series of surface tension propellant management system design concepts. The chosen concept is identified and its mission operation described. The ullage bubble and bulk liquid positioning characteristics are presented, along with propellant dynamic considerations entailed by thrust initiation/termination. Pressurization design considerations, required to assure minimum disturbance to the bulk propellant, are introduced as well as those of the tank ullage vent. Design provisions to assure liquid communication between tank ends are discussed. Results of a preliminary design study are presented, including mechanical testing requirements to assure structural integrity, propellant compatibility, and proper installation.
New type of Dewar provides passive, constant-temperature cryogenic cooling for scientific instruments under normal-to low-gravity conditions. Known as Surface-Tension-Contained Liquid Cryogen Cooler (STCLCC), keeps liquid cryogen in known location inside the Dewar by trapping liquid inside spongelike material. Unique sponge material fills most of volume of inner tank. Sponge is all-silica, open-cell material similar to that used for Space Shuttle thermal-protection tiles.
High resolution laboratory experiments with large aspect ratio are being conducted for thin fluid layers heated from below and bounded from above by a free surface. The fluid depths are chosen sufficiently small (less than 0.06 cm) so that surface tension is the dominant driving mechanisms; the Rayleigh number is less than 5 for the results reported here. Shadowgraph visualization reveals that the primary instability leading to hexagons is slightly hysteretic (approximately 1 percent). Preliminary measurements of the convection amplitude using infrared imaging are also presented.
The microgravity environment of the KC-135 aircraft was utilized in three experiments designed to determine the following: (1) the feasibility of measuring critical wetting temperatures; (2) the effectiveness of surface tension as a means of keeping the cushioning heat transfer liquid in the furnace during ampoule translation; and (3) whether a non-wetting fluid would separate from the ampoule wall under low gravity conditions. This trio of investigations concerning surface phenomena demonstrates the effectiveness of the KC-135 as a microgravity research environment for small-scale, hand-held experiments.
The Navier-Stokes-Boussinesq equations governing the transport of momentum, mass and heat in a nonisothermal liquid bridge with a temperature-dependent surface tension are solved using a vorticity-stream-function formulation together with a nonorthogonal coordinate transformation. The equations are discretized using a pseudo-unsteady semi-implicit finite difference scheme and are solved by the ADI method. A Picard-type iteration is adopted which consists of inner and outer iterative processes. The outer iteration is used to update the shape of the free surface. Two schemes have been used for the outer iteration; both use the force balance normal to the free surface as the distinguished boundary condition. The first scheme involves successive approximation by the direct solution of the distinguished boundary condition. The second scheme uses the artificial force imbalance between the fluid pressure, viscous and capillary forces at the free surface which arises when the boundary condition for force balance normal to the surface is not satisfied. This artificial imbalance is then used to change the surface shape until the distinguished boundary condition is satisfied. These schemes have been used to examine a variety of model liquid bridge situations including purely thermocapillary-driven flow situations and mixed thermocapillary- and bouyancy-driven flow.
Experiments have been carried out to determine the critical thermal Rayleigh number for onset of convection in a horizontal layer of density-stratified fluid with a free surface when heated from below. Three different aqueous solutions were used: salt, glycerol, and acetic acid. The rates of change in surface tension with concentration for these three solutions are positive, nearly zero, and negative, respectively. Compared to the rigid-rigid boundaries, the critical thermal Rayleigh number was found to be larger by 11.2 percent for the salt solution and smaller by 10.0 percent for the glycerol solution. With the acetic acid solution, however, the effect of the free surface was found to be negligible.
In this paper a numerical procedure for simulating two-fluid flows is presented. This procedure is based on the Volume of Fluid (VOF) method proposed by Hirt and Nichols and the continuum surface force (CSF) model developed by Brackbill, et al. In the VOF method fluids of different properties are identified through the use of a continuous field variable (color function). The color function assigns a unique constant (color) to each fluid. The interfaces between different fluids are distinct due to sharp gradients of the color function. The evolution of the interfaces is captured by solving the convective equation of the color function. The CSF model is used as a means to treat surface tension effect at the interfaces. Here a modified version of the CSF model, proposed by Jacqmin, is used to calculate the tension force. In the modified version, the force term is obtained by calculating the divergence of a stress tensor defined by the gradient of the color function. In its analytical form, this stress formulation is equivalent to the original CSF model. Numerically, however, the use of the stress formulation has some advantages over the original CSF model, as it bypasses the difficulty in approximating the curvatures of the interfaces. The least-squares finite element method (LSFEM) is used to discretize the governing equation systems. The LSFEM has proven to be effective in solving incompressible Navier-Stokes equations and pure convection equations, making it an ideal candidate for the present applications. The LSFEM handles all the equations in a unified manner without any additional special treatment such as upwinding or artificial dissipation. Various bench mark tests have been carried out for both two dimensional planar and axisymmetric flows, including a dam breaking, oscillating and stationary bubbles and a conical liquid sheet in a pressure swirl atomizer.
A program was conducted to provide the technology base for the SS/RCS flight tankage. Through a combination of analysis, subscale testing and computer predictions, a surface tension acquisition/expulsion system design was developed for the Orbiter RCS application. A full-scale tank system was fabricated and ground verification testing was conducted. Cleaning, inspection, fill and drain, and one-g expulsion performance were demonstrated. Results show that the fine-mesh screen, compartmented tank system provides the performance, flexibility, reusability, and other characteristics required by the pulsing, high flowrate RCS. It provides the required expulsion under widely differing high-g boost abort and reentry vectors oriented 119 deg apart and during on-orbit operation under omnidirectional low-g conditions.
System for studying capillary action uses pressure transducer and chart recorder instead of manometer. Apparatus enables measurements to be made under controlled atmospheres. It also may be remotely operated. These features are particularly useful when dealing with noxious liquids and for study of surface tension under high-pressure conditions that require use of all-metal apparatus.
A cryogenic cooler is provided for use in craft such as launch, orbital, and space vehicles subject to substantial vibration, changes in orientation, and weightlessness. The cooler contains a small pore, large free volume, low density material to restrain a cryogen through surface tension effects during launch and zero-g operations and maintains instrumentation within the temperature range of 10 to 140 K. The cooler operation is completely passive, with no inherent vibration or power requirements.
This final technical report covers the work accomplished (under NAG3-1300) from 1 October 1991 to 1 October 1993. The grant is a direct result of Dr. H. Philip Stahl's (of Rose-Hulman Institute of Technology) participation in the NASA/ASEE Summer Faculty Fellowship Program at NASA Lewis Research Center sponsored by Case Western Reserve University and the Ohio Aerospace Institute. The Surface Tension Driven Convection Experiment (STDCE) is a fundamental fluid physics experiment designed to provide quantitative data on the thermocapillary flow of fluid under the influence of an increased localized surface temperature. STDCE flew on the Space Shuttle Columbia in the First United States Microgravity Laboratory (USML-1) in June 1992. The second flight of this experiment (STDCE-2) is scheduled for 1995. The specific science objectives of STDCE-2 are to determine the extent and nature of thermocapillary flows, the effect of heating mode and level, the effect of the liquid free-surface shape, and the onset conditions for and nature of oscillatory flows. In order to satisfy one of these objectives, an instrument for measuring the shape of an air/oil free surface must be developed.
Thermocapillary flows are known to become oscillatory (time-periodic), but how and when they become oscillatory in containers of unit-order aspect ratio are not yet fully understood. The present work is a part of our continuous effort to obtain a better understanding of the phenomenon. Thermocapillary flow experiments in normal gravity are limited to a narrow parametric range in order to minimize gravity and buoyancy effects, which is an important reason for our lack of full understanding of the oscillation phenomenon. One important unanswered question is what role, if any, free surface deformation plays in the oscillation mechanism. For that reason we performed thermocapillary flow experiments, called the Surface Tension Driven Convection Experiment-2 (STDCE-2), aboard the USML-2 Spacelab in 1995. The main objectives of the experiments were to investigate oscillatory thermocapillary flows in microgravity and to clarify the importance of free surface deformation in such flows. Steady and oscillatory thermocapillary flows were generated in cylindrical containers by employing two heating modes. A CO2 laser with adjustable power and beam diameter was used in the Constant Flux (CF) configuration to heat the free surface. The other configuration investigated in STDCE-2 was the Constant Temperature (CT) configuration in which a submerged cylindrical cartridge heater placed at the symmetry (axial) axis of the test container heated the fluid. Both heating modes cause non-uniform temperature distributions on the free surface, which generates thermocapillary flow. The flow field was investigated by flow visualization, and the temperature field was measured by thermistors and an infrared imager. The free surface shape and motion were measured by a Ronchi system. The hardware performed well and we were able to conduct more tests than originally planned. From the successful experiments a large amount of data was acquired. The analysis of the data is now nearly complete. Some important results are presented and discussed herein.
We extended the previous analysis of detached solidification of InSb based on the moving meniscus model. We found that for steady detached solidification to occur in a sealed ampoule in zero gravity, it is necessary for the growth angle to exceed a critical value, the contact angle for the melt on the ampoule wall to exceed a critical value, and the melt-gas surface tension to be below a critical value. These critical values would depend on the material properties and the growth parameters. For the conditions examined here, the sum of the growth angle and the contact angle must exceed approximately 130, which is significantly less than required if both ends of the ampoule are open.
The Microgravity Science Glovebox (MSG) on the International Space Station (ISS) is used for fluid transfer in many types of experiments. Reagents are handled in the MSG to prevent their accidental release into the cabin. However, the MSG is currently over-subscribed, creating a backlog of users in flight. As a recourse, current experiments are underway to assess the possibility of moving certain science operations from the MSG into the open cabin of the ISS. The experiments are designed to assess the efficacy of exploiting surface tension as a control to prevent the unwanted release of liquids. Dyed water currently serves as an ersatz for potentially more hazardous liquids. Common wet-lab operations such as de/mating wetted Luer-Lok fittings, liquid-bearing container lid removal, and pipetting between well plates are performed illustrating the facility and challenges imposed by the microgravity environment. Concerning the latter, various pipette cannula sizes are deployed at various injection, withdrawal, and translations rates to map the existence, size, velocity, and trajectory of satellite droplets expected to form when breaking contact between the water surface and the pipette tip. Though such drops frequently form in terrestrial operations, they are nearly imperceptible and inconsequential—due in part to their speed and because gravity quickly returns them to the well plate from which they came. The use of airflow to capture and collect such satellite droplets is demonstrated. The dynamic stability of the liquid-filled well plates is quantified in response to a variety of crew-imparted disturbances. From a safety perspective, the results from the STCE are of immediate practical value. If such routine low-gravity capillary fluidic operations can be established as mundane, their performance may be moved out of the MSG and into the cabin, significantly increasing the efficiency of experiments performed on ISS.
The effects of g-jitter on nonencapsulated and encapsulated liquid bridges were investigated numerically, using fluid characteristics and parameters from three fluid systems: a silicone oil bridge, a methanol bridge, and a silicon melt. Results showed that complex flow patterns can arise in g-jitter environment which significantly modify the heat-transfer characteristics of the system. It was found that the nonencapsulated liquid bridges and float zone melts were dominated by surface-tension driven convection, with very little impact on the flows by residual and g-jitter accelerations. Zone encapsulation resulted in a sizeable drop in the maximum fluid velocities. The g-jitter computations on the encapsulated float zones resulted in significant augmentation of the maximum velocities and heat transfer, with the silicon melt being the least sensitive to g-jitter acceleration.
During an icing encounter of an aircraft in flight, super-cooled water droplets impinging on an airfoil may splash before freezing. This paper reports tests performed to determine if this effect is significant and uses the results to develop an improved scaling method for use in icing test facilities. Simple laboratory tests showed that drops splash on impact at the Reynolds and Weber numbers typical of icing encounters. Further confirmation of droplet splash came from icing tests performed in the NaSA Lewis Icing Research Tunnel (IRT) with a surfactant added to the spray water to reduce the surface tension. The resulting ice shapes were significantly different from those formed when no surfactant was added to the water. These results suggested that the droplet Weber number must be kept constant to properly scale icing test conditions. Finally, the paper presents a Weber-number-based scaling method and reports results from scaling tests in the IRT in which model size was reduced up to a factor of 3. Scale and reference ice shapes are shown which confirm the effectiveness of this new scaling method.