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At least 145 records · Page 8
All sourcesNASA NTRSDOE OSTI
DOE OSTI2025

Effect of pattern transfer process on roughness of block copolymer patterns from directed self-assembly

Block copolymer-directed self-assembly (DSA) remains promising for improving pattern quality and reducing the stochastic variations that challenge high numerical aperture extreme ultraviolet lithography. Equally critical is refining pattern transfer methods for accurately transferring the rectified DSA features to the underlying substrate. We compare two atomic layer deposition (ALD)-based techniques: sequential infiltration synthesis (SIS) and dry liftoff, applied to polystyrene-block-poly(methyl methacrylate) (PS-b-PMMA) DSA patterns. Both methods utilize aluminum oxide hard masks, with one synthesized through infiltration into the PMMA domains and the other through conformal ALD coating. High-resolution scanning electron micrographs were analyzed to measure line edge, width, and placement roughness for both the line (PMMA) and space (PS) features. Although both methods yielded similar overall 3σ rms roughness, they differed significantly in the frequency-dependent power spectral density (PSD) profiles. SIS reduced line placement roughness at length scales associated with the polymer pitch, but increased space width roughness at low frequencies, whereas dry liftoff mimicked the frequency content of the original guiding pattern. This study underscores the importance of PSD evaluation in selecting optimal pattern transfer strategies for specific applications.

Block copolymers↗
DOE OSTI2022

Shallow-and-Deep Inelastic Scattering with Neutrinos

In ν/ν-Nucleon/Nucleus interactions Shallow Inelastic Scattering (SIS) is technically defined interms of the four-momentum transfer to the hadronic system as non-resonant meson productionwith predominantly lower Q 2 . This non-resonant meson production intermixes with resonantmeson production in a regime of similar effective hadronic mass W of the interaction. As Q 2 grows non-resonant interactions begin to take place with quarks within the nucleon indicating thestart of Deep Inelastic Scattering (DIS). To essentially separate this resonant plus non-resonantmeson production from DIS quark-fragmented meson production, a cut of 2 GeV in W of theinteractions is generally introduced. However, since experimentally mesons from resonance decaycannot be separated from non-resonant produced mesons, SIS for all practical purposes is definedas inclusive meson production that includes non-resonant plus resonant meson production andthe interference between them. NOTE, this is a mildly modified introduction and overview takenfrom the detailed summary of this topic referenced in the introduction.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2025

Block Copolymer-Templated Synthesis of Fe–Ni–Co-Modified Nanoporous Alumina Films

Despite intense interest in the catalytic potential of transition metal oxide heterostructures, originating from their large surface area and tunable chemistry, the fabrication of well-defined multicomponent oxide coatings with controlled architectures remains challenging. Here, we demonstrate a simple and effective swelling-assisted sequential infiltration synthesis (SIS) strategy to fabricate hierarchically porous multicomponent metal-oxide electrocatalysts with tunable bimetallic composition. A combination of solution-based infiltration (SBI) of transition metals, iron (Fe), nickel (Ni), and cobalt (Co), into a block copolymer (PS73-b-P4VP28) template, followed by vapor-phase infiltration of alumina using sequential infiltration synthesis (SIS), was employed to synthesize porous, robust, conformal and transparent multicomponent metal-oxide coatings like Fe/AlO x , Fe+Ni/AlO x , and Fe+Co/AlO x . Electrochemical assessments for the oxygen evolution reaction (OER) in a 0.1 M KOH electrolyte demonstrated that the Fe+Ni/AlO x composite exhibited markedly superior catalytic activity, achieving an impressive onset potential of 1.41 V and a peak current density of 3.29 mA/cm 2 . This superior activity reflects the well-known synergistic effect of alloying transition metals with a trace of Fe, which facilitates OER kinetics. Overall, our approach offers a versatile and scalable path towards the design of stable and efficient catalysts with tunable nanostructures, opening new possibilities for a wide range of electrochemical energy applications.

conformal films↗
DOE OSTI2023

Accessibility and Mechanical Stability of Nanoporous Zinc Oxide and Aluminum Oxide Coatings Synthesized via Infiltration of Polymer Templates

The conformal nanoporous inorganic coatings with accessible pores that are stable under applied thermal and mechanical stresses represent an important class of materials used in the design of sensors, optical coatings, and biomedical systems. Here, we synthesize porous AlO x and ZnO coatings by the sequential infiltration synthesis (SIS) of two types of polymers that enable the design of porous conformal coatings—polymers of intrinsic microporosity (PIM) and block co-polymer (BCP) templates. Using quartz crystal microbalance (QCM), we show that alumina precursors infiltrate both polymer templates four times more efficiently than zinc oxide precursors. Using the quartz crystal microbalance (QCM) technique, we provide a comprehensive study on the room temperature accessibility to water and ethanol of pores in block copolymers (BCPs) and porous polymer templates using polystyrene-block-poly-4-vinyl pyridine (PS75-b-P4VP25) and polymers of intrinsic microporosity (PIM-1), polymer templates modified by swelling, and porous inorganic coatings such as AlO x and ZnO synthesized by SIS using such templates. Importantly, we demonstrate that no structural damage occurs in inorganic nanoporous AlO x and ZnO coatings synthesized via infiltration of the polymer templates during the water freezing/melting cycling tests, suggesting excellent mechanical stability of the coatings, even though the hardness of the inorganic nanoporous coating is affected by the polymer and precursor selections. We show that the hardness of the coatings is further improved by their annealing at 900 °C for 1 h, though for all the cases except ZnO obtained using the BCP template, this annealing has a negligible effect on the porosity of the material, as is confirmed by the consistency in the optical characteristics. These findings unravel new potential for the materials being used across various environment and temperature conditions.

36 MATERIALS SCIENCE↗
NASA NTRS1981

Interstellar silicon sulfide

Silicon sulfide has been observed in Sgr B2 at 108.92 GHz and 90.77 GHz and in Orion A at 108.92 GHz. The column density is 1-2 x 10 to the 13th/sq cm in both sources. SiS was not seen in two other molecular clouds where SiO has been detected; nor was it seen in a variety of late-type stars with varying C/O ratios. It appears that SiS is significantly less abundant than SiO in the interstellar medium and probably at least somewhat less abundant in oxygen-rich late-type variable stars.

Dickinson, D. F.↗
NASA NTRS1984

Advanced CID array multispectral pushbroom scanner

An optical imager, called the Scanning Imaging Spectroradiometer (SIS), was built for NASA in the early 1970's. Later, the Solidstate Array Spectroradiometer (SAS) was developed on the basis on a substitution of a Charge Injection Device (CID) array for the vidicon of the SIS. The Advanced Solidstate Array Spectroradiometer (ASAS) represents an improvement of the SAS. ASAS is a solidstate multispectral optical imaging radiometer which is currently the most versatile instrument of its type in the visible part of the spectrum. The instrument is capable of absolute radiometric measurements in all of its 32 bands. ASAS can be easily mounted in small aircraft as well as high altitude craft such as the U-2, taking into account also the possibility of a use in the Space Shuttle. The instrument consists of three separate subsystems. Attention is given to the optics, the detector array, data storage, data retrieval, and system performance.

Stewart, S. E.↗
NASA NTRS1985

Design and optimization of NbCN/PbBi mixer elements for heterodyne receivers

Superconductor-Insulator-Superconductor (SIS) quantum mixers provide a relatively new approach to millimeter wave mixing potentially offering conversion gain, a low local oscillator power demand and potential mixer temperatures near the quantum limit. This paper presents device modeling and fabrication development for NbCN lead-alloy submicron edge-contact SIS mixers for use at 115 GHz.

Lichtenberger, A. W.↗
NASA NTRS1988

A steam inerting system for hydrogen disposal for the Vandenberg Shuttle

A two-year feasibility and test program to solve the problem of unburned confined hydrogen at the Vandenberg Space Launch Complex Six (SLC-6) during Space Shuttle Main Engine (SSME) firings is discussed. A novel steam inerting design was selected for development. Available sound suppression water is superheated to flash to steam at the duct entrance. Testing, analysis, and design during 1987 showed that the steam inerting system (SIS) solves the problem and meets other flight-critical system requirements. The SIS design is complete and available for installation at SLC-6 to support shuttle or derivative vehicles.

Belknap, Stuart B.↗
NASA NTRS1990

High angular resolution mm- and submm-observations of dense molecular gas in M82

Researchers observed CO(7-6), CO(3-2), HCN(3-2) and HCO+(3-2) line emission toward the starburst nucleus of M82 and have obtained an upper limit to H13CN(3-2). These are the first observations of the CO(7-6), HCN(3-2) and HCO+(3-2) lines in any extragalactic source. Researchers took the CO(7-6) spectrum in January 1988 at the Infrared Telescope Facility (IRTF) with the Max Planck Institute for Extraterrestrial Physics/Univ. of California, Berkeley 800 GHz Heterodyne Receiver. In March 1989 researchers used the Institute for Radio Astronomy in the Millimeter range (IRAM) 30 m telescope to observe the CO(3-2) line with the new MPE 350 GHz Superconductor Insulator Superconductor (SIS) receiver and the HCN(3-2) and HCO+(3-2) lines with the (IRAM) 230 GHz SIS receiver (beam 12" FWHM, Blundell et al. 1988). The observational parameters are summarized.

Wild, W.↗
NASA NTRS1990

Spatial variation of the physical conditions of molecular gas in galaxies

Multi-line studies of CO-12, CO-13, C-18O, HCN, and HCO(+) at 3 mm, 1.3 mm, and 0.8 mm using the Institute for Radio Astronomy in the Millimeter range (IRAM) 30 m telescope, with the IRAM superconductor insulator superconductor (SIS) receivers and the Max Planck Institute for External Physics (MPE) 350 GHz SIS receiver, show that the densities and temperatures of molecular gas in external galaxies change significantly with position. CO-12 measures the densities and temperature of diffuse interclump molecular gas, but not the bulk of the molecular gas. Simple one-component models, with or without external heating, cannot account for the weakness of the CO-12 J = 3 to 2 line relative to J = 2 to 1 and J = 1 to 0. CO-12 does not trace the bulk of the molecular gas, and optical depth effects obviate a straightforward interpretation of CO-12 data. Instead, researchers turned to the optically thin CO isotopes and other molecular species. Isotopic CO lines measure the bulk of the molecular gas, and HCN and HCO(+) pick out denser regions. Researchers find a warm ridge of gas in IC 342 (Eckart et al. 1989), denser gas in the starburst nucleus of IC 342, and a possible hot-spot in NGC 2903. In IC 342, NGC 2146, and NGC 6764, the CO-13 J = 2 to 1 line is subthermally populated, implying gas densities less than or equal to 10(exp 4) cm(-3).

Jackson, James M.↗
NASA NTRS1991

Characterization of NbN films and tunnel junctions

Properties of NbN films and NbN/MgO/NbN tunnel junctions are discussed. NbN junctions are being developed for use in high-frequency, SIS quasiparticle mixers. To properly design mixer circuits, junction and film properties need to be characterized. The specific capacitance of NbN/MgO/NbN junctions has been measured as a function of the product of the normal-state resistance and the junction area (RnA), and it is found to vary by more than a factor of two (35-85 fF/sq microns) over the range of RnA measured (1000-50 ohm sq microns). This variation is important because the specific capacitance determines the RC speed of the tunnel junction at a given RnA value. The magnetic penetration depth of NbN films deposited under different conditions is also measured. The magnetic penetration depth affects the design of microstrip line used in RF tuning circuits. Control of the magnetic penetration depth is necessary to fabricate reproducible tuning circuits. Additionally, the critical current uniformity for arrays of 100 junctions has been measured. Junction uniformity will affect the design of focal-plane arrays of SIS mixers. Finally, the relevance of these measurements to the design of Josephson electronics is discussed.

Stern, J. A.↗
NASA NTRS1991

The Space Exploration Initiative - An information system perspective

The authors look at the Space Exploration Initiative (SEI) from an information system perspective an discuss information system definition effort being conducted in support of NASAs Lunar Mars Exploration Program Office (LMEPO) Johnson Space Center (JSC). The development of an integrated, effective SEI information system (SIS) is recognized as crucial to the success of the SEI missions. Some of the new and unique challenges for the SIS as evidenced in the Lunar and the Mars missions are outlined along with some preliminary conceptual approaches, both architectural and technological, being investigated to address them.

Hartenstein, Ray↗
NASA NTRS1992

A demonstration of motion base design alternatives for the National Advanced Driving Simulator

A demonstration of the capability of NASA's Vertical Motion Simulator to simulate two alternative motion base designs for the National Advanced Driving simulator (NADS) is reported. The VMS is located at ARC. The motion base conditions used in this demonstration were as follows: (1) a large translational motion base; and (2) a motion base design with limited translational capability. The latter had translational capability representative of a typical synergistic motion platform. These alternatives were selected to test the prediction that large amplitude translational motion would result in a lower incidence or severity of simulator induced sickness (SIS) than would a limited translational motion base. A total of 10 drivers performed two tasks, slaloms and quick-stops, using each of the motion bases. Physiological, objective, and subjective measures were collected. No reliable differences in SIS between the motion base conditions was found in this demonstration. However, in light of the cost considerations and engineering challenges associated with implementing a large translation motion base, performance of a formal study is recommended.

Mccauley, Michael E.↗
NASA NTRS1992

Fabrication and characterization of high current-density, submicron, NbN/MgO/NbN tunnel junctions

At near-millimeter wavelengths, heterodyne receivers based on SIS tunnel junctions are the most sensitive available. However, in order to scale these results to submillimeter wavelengths, certain device properties should be scaled. The tunnel-junction's current density should be increased to reduce the RC product. The device's area should be reduced to efficiently couple power from the antenna to the mixer. Finally, the superconductor used should have a large energy gap to minimize RF losses. Most SIS mixers use Nb or Pb-alloy tunnel junctions; the gap frequency for these materials is approximately 725 GHz. Above the gap frequency, these materials exhibit losses similar to those in a normal metal. The gap frequency in NbN films is as-large-as 1440 GHz. Therefore, we have developed a process to fabricate small area (down to 0.13 sq microns), high current density, NbN/MgO/NbN tunnel junctions.

Stern, J. A.↗
NASA NTRS1993

Contamination design of a Scientific Instrument Protective Enclosure for the Hubble Space Telescope Servicing Mission

A Scientific Instrument Protective Enclosure (SIPE) was designed to accommodate second generation science instruments (SIs) for the Hubble Space Telescope (HST) First Servicing Mission (FSM). One of the main design drivers for the SIPE is to provide a protective environment for the SIs against particulate and molecular contaminants that pose a viable threat to the SI performance. The focus of this paper will detail the methodology incorporated in the design of the SIPE to provide a controlled environment for SI protection at the launch site, during pre-launch/launch activities, and during on-orbit operations in the Shuttle bay.

Hedgeland, Randy J.↗
NASA NTRS1993

Aerodynamic heating in hypersonic flows

Aerodynamic heating in hypersonic space vehicles is an important factor to be considered in their design. Therefore the designers of such vehicles need reliable heat transfer data in this respect for a successful design. Such data is usually produced by testing the models of hypersonic surfaces in wind tunnels. Most of the hypersonic test facilities at present are conventional blow-down tunnels whose run times are of the order of several seconds. The surface temperatures on such models are obtained using standard techniques such as thin-film resistance gages, thin-skin transient calorimeter gages and coaxial thermocouple or video acquisition systems such as phosphor thermography and infrared thermography. The data are usually reduced assuming that the model behaves like a semi-infinite solid (SIS) with constant properties and that heat transfer is by one-dimensional conduction only. This simplifying assumption may be valid in cases where models are thick, run-times short, and thermal diffusivities small. In many instances, however, when these conditions are not met, the assumption may lead to significant errors in the heat transfer results. The purpose of the present paper is to investigate this aspect. Specifically, the objectives are as follows: (1) to determine the limiting conditions under which a model can be considered a semi-infinite body; (2) to estimate the extent of errors involved in the reduction of the data if the models violate the assumption; and (3) to come up with correlation factors which when multiplied by the results obtained under the SIS assumption will provide the results under the actual conditions.

Reddy, C. Subba↗
NASA NTRS1994

X-ray color analysis of the spectra of active galactic nuclei

The identification and detection of X-ray absorption and emission features depends on the resolution and the signal-to-noise ratio (S/N) of the observation, the understanding of the instrument response, and the Galactic line-of-sight absorption. Since many of the active galactic nucleus (AGN) data sets are limited in their S/N and full modeling of the physical conditions is rather complicated, we suggest a new analysis method based on 'X-ray colors.' The two sets of X-ray colors, defined for low (ROSAT Position Sensitive Proportional Counter (PSPC)) and medium (Broad Band X-Ray Telescope (BBXRT)) and ASCA Solid-State Imaging Spectrometers (SIS) resolution experiments, are used to separate regions of different physical conditions in a two-dimensional color-color plane. They are similar but superior to previous methods using the X-ray 'hardness ratio' in being able to reveal more of the physical properties of the source. We illustrate the use of such diagrams by studying a number of AGNs suspected of showing absorption features. A sample of 14 AGNs observed by the ROSAT PSPC is presented which includes several objects with suspected 'warm absorbers' along the line-of-sight to the nucleus, several others exhibiting intrinsic continuum variations, and a number of control objects thought to be featureless. Our new observations show, for the first time, the color variation as a function of time for three of the Seyfert 1 sources: NGC 4051, Mrk 335, and Mrk 766. The variations suggest that in two sources we are witnessing real changes in continuum shape, while one (NGC 4051) is consistent with having a warm absorber. Four of the objects observed by BBXRT are reanalyzed using our X-ray colors. Out of these, we discuss in detail the case of NGC 4151 and show that the color-color analysis agrees very well with previous, detailed spectral fitting methods. In particular, we confirm that the observed BBXRT observation of this source is not consistent with the warm absorber explanation and must be interpreted as a combination of a variable hard component and another component. We explain the limitations in measuring low-energy emission features in ASCA SIS observations and present color-color diagrams which can be used as a powerful diagnostic tool in the analysis of data collected by this experiment.

Netzer, Hagai↗