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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 145 records · Page 8
All sourcesNASA NTRSDOE OSTI
DOE OSTI2015

Synthesis of superparamagnetic silica-coated magnetite nanoparticles for biomedical applications

Multifunctional superparamagnetic iron oxide nanoparticles (SPIONs) coated with silica are widely researched for biomedical applications such as magnetic resonance imaging, tissue repair, cell separation, hyperthermia, drug delivery, etc. In this article synthesis of magnetite (Fe{sub 3}O{sub 4}) nanoparticles and their coating with SiO{sub 2} is reported. Fe{sub 3}O{sub 4} nanoparticles were synthesized by chemical co-precipitation and it was coated with silica by hydrolysis and condensation of tetraethylorthosilicate. XRD, FTIR, TEM and VSM techniques were used to characterize bare and coated nanoparticles. Results indicated that the average size of SPIONS was 8.4 nm. X-ray diffraction patterns of silica coated SPIONS were identical to that of SPIONS confirming the inner spinal structure of SPIONS. FTIR results confirmed the binding of silica with the magnetite and the formation of the silica shell around the magnetite core. Magnetic properties of SPIONS and silica coated SPIONS are determined by VSM. They are superparamagnetic. The major conclusion drawn from this study is that the synthesis route yields stable, non-aggregated magnetite-silica core-shell nanostructures with tailored morphology and excellent magnetic properties.

77 NANOSCIENCE AND NANOTECHNOLOGY↗
DOE OSTI2022

The role of microstructural evolution during spark plasma sintering on the soft magnetic and electronic properties of a CoFe–Al2O3 soft magnetic composite

Abstract For transformers and inductors to meet the world’s growing demand for electrical power, more efficient soft magnetic materials with high saturation magnetic polarization and high electrical resistivity are needed. This work aimed at the development of a soft magnetic composite synthesized via spark plasma sintering with both high saturation magnetic polarization and high electrical resistivity for efficient soft magnetic cores. CoFe powder particles coated with an insulating layer of Al 2 O 3 were used as feedstock material to improve the electrical resistivity while retaining high saturation magnetic polarization. By maintaining a continuous non-magnetic Al 2 O 3 phase throughout the material, both a high saturation magnetic polarization, above 1.5 T, and high electrical resistivity, above 100 μΩ·m, were achieved. Through microstructural characterization of samples consolidated at various temperatures, the role of microstructural evolution on the magnetic and electronic properties of the composite was elucidated. Upon consolidation at relatively high temperature, the CoFe was to found plastically deform and flow into the Al 2 O 3 phase at the particle boundaries and this phenomenon was attributed to low resistivity in the composite. In contrast, at lower consolidation temperatures, perforation of the Al 2 O 3 phase was not observed and a high electrical resistivity was achieved, while maintaining a high magnetic polarization, ideal for more efficient soft magnetic materials for transformers and inductors.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Thermal Analysis of a Superconducting Undulator Cryostat for the APS Upgrade

The Advanced Photon Source Upgrade includes four 4.8-m-long superconducting undulator (SCU) cryostats, each containing two planar undulator NbTi magnets up to 1.9 m long. The cooling is provided by six cryocoolers arranged in three thermal circuits. The magnets are indirectly cooled with LHe penetrating through channels in the magnet cores. This 4 K circuit, which also includes a LHe tank, is cooled by five 4 K cryocooler 2nd stages. A beam vacuum, which is thermally isolated from the magnets, is cooled by one 10 K cryocooler 2nd stage. A thermal shield and warm parts of current leads are cooled by the 1st stages of all six cryocoolers. This paper presents an ANSYS-based thermal analysis of the new SCU cryostat including all thermal circuits. The benchmarked thermal conductance between the cryocooler cold heads and the LHe tank are used in the calculations as well as the measured cryocooler load lines. The model predicts temperatures in the system, total 4 K heat loads, and excess cooling power for various operational modes of the undulator.

Shiroyanagi, Y.↗
DOE OSTI2020

A magnetic sensor using a 2D van der Waals ferromagnetic material

Two-dimensional (2D) van der Waals ferromagnetic materials are emerging as promising candidates for applications in ultra-compact spintronic nanodevices, nanosensors, and information storage. Our recent discovery of the strong room temperature ferromagnetism in single layers of VSe2 grown on graphite or MoS2 substrate has opened new opportunities to explore these ultrathin magnets for such applications. In this paper, we present a new type of magnetic sensor that utilizes the single layer VSe2 film as a highly sensitive magnetic core. The sensor relies in changes in resonance frequency of the LC circuit composed of a soft ferromagnetic microwire coil that contains the ferromagnetic VSe2 film subject to applied DC magnetic fields. We define sensitivity as the slope of the characteristic curve of our sensor, df0/dH, where f0 is the resonance frequency and H is the external magnetic field. The sensitivity of the sensor reaches a large value of 16×106Hz/Oe, making it a potential candidate for a wide range of magnetic sensing applications.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2016

Structure, dynamics, and deuterium fractionation of massive pre-stellar cores

High levels of deuterium fraction in N{sub 2}H{sup +} are observed in some pre-stellar cores. Single-zone chemical models find that the timescale required to reach observed values (D{sub frac}{sup N{sub 2}H{sup +}}≡N{sub 2}D{sup +}/N{sub 2}H{sup +}≳0.1) is longer than the free-fall time, possibly 10 times longer. Here, we explore the deuteration of turbulent, magnetized cores with 3D magnetohydrodynamics simulations. We use an approximate chemical model to follow the growth in abundances of N{sub 2}H{sup +} and N{sub 2}D{sup +}. We then examine the dynamics of the core using each tracer for comparison to observations. We find that the velocity dispersion of the core as traced by N{sub 2}D{sup +} appears slightly sub-virial compared to predictions of the Turbulent Core Model of McKee and Tan, except at late times just before the onset of protostar formation. By varying the initial mass surface density, the magnetic energy, the chemical age, and the ortho-to-para ratio of H{sub 2}, we also determine the physical and temporal properties required for high deuteration. We find that low initial ortho-to-para ratios (≲0.01) and/or multiple free-fall times (≳3) of prior chemical evolution are necessary to reach the observed values of deuterium fraction in pre-stellar cores.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2019

Soft Magnetic Multilayered FeSiCrB–Fe$_{x}$N Metallic Glass Composites Fabricated by Spark Plasma Sintering

Novel multilayered FeSiCrB–Fe $_{x}$ N ( x = 2–4) metallic glass composites were fabricated using spark plasma sintering of FeSiCrB amorphous ribbons (Metglas 2605SA3 alloy) and Fe $_{x}$ N ( x = 2–4) powder. Crystalline Fe $_{x}$ N can serve as a high magnetic moment, high electrical resistance binder, and lamination material in the consolidation of amorphous and nanocrystalline ribbons, mitigating eddy currents while boosting magnetic performance and stacking factor in both wound and stacked soft magnetic cores. Stacking factors of nearly 100% can be achieved in an amorphous ribbon/iron nitride composite. FeSiCrB–Fe $_{x}$ N multilayered metallic glass composites prepared by spark plasma sintering have the potential to serve as a next-generation soft magnetic material in power electronics and electrical machines.

36 MATERIALS SCIENCE↗
DOE OSTI2024

A Low-Profile Gate Power Supply for a SiC Phase Leg with Reduced Isolation Capacitance

Gate driver power supply (GDPS) for SiC devices needs power to 5 W as the switching frequency increases to hundreds of kHz. Resonant converters with planar magnetics demand GDPS with a lower profile. Also, the isolation capacitance (Cp) needs to be minimized for SiC devices with high dv/dt. This paper proposed a planar 5 W*2, 20 V isolated gate power supply for a SiC phase leg in the EV traction inverter. Air-core magnetics with PCB windings are applied for low profile. A single-switch resonant Class-E topology is proposed with zero-voltage switching at 6.78 MHz to minimize the magnetics footprint for a 6 pF Cp. Compared with commercial power supplies with similar power, the proposed power supply reduced the profile and Cp by more than half without sacrificing its efficiency and power density.

Li, Bo↗
DOE OSTI2014

ALMA results of the pseudodisk, rotating disk, and jet in the continuum and HCO{sup +} in the protostellar system HH 212

HH 212 is a nearby (400 pc) Class 0 protostellar system showing several components that can be compared with theoretical models of core collapse. We have mapped it in the 350 GHz continuum and HCO{sup +} J = 4-3 emission with ALMA at up to ∼0.''4 resolution. A flattened envelope and a compact disk are seen in the continuum around the central source, as seen before. The HCO{sup +} kinematics shows that the flattened envelope is infalling with small rotation (i.e., spiraling) into the central source, and thus can be identified as a pseudodisk in the models of magnetized core collapse. Also, the HCO{sup +} kinematics shows that the disk is rotating and can be rotationally supported. In addition, to account for the missing HCO{sup +} emission at low-redshifted velocity, an extended infalling envelope is required, with its material flowing roughly parallel to the jet axis toward the pseudodisk. This is expected if it is magnetized with an hourglass B-field morphology. We have modeled the continuum and HCO{sup +} emission of the flattened envelope and disk simultaneously. We find that a jump in density is required across the interface between the pseudodisk and the disk. A jet is seen in HCO{sup +} extending out to ∼500 AU away from the central source, with the peaks upstream of those seen before in SiO. The broad velocity range and high HCO{sup +} abundance indicate that the HCO{sup +} emission traces internal shocks in the jet.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2025

Electromagnetic Modeling of Lattice Structures in Additively Manufactured Electric Machines

Recent advancements in metal additive manufacturing (AM) show great potential to revolutionize the design and manufacturing of electromagnetic components used in the field of electrical engineering. Lattice structures directly printed by AM processes typically offer better structural performance with reduced weight, such as high stiffness, surface area, elongation, energy absorption, and porosity, than the solid counterpart. This paper aims to study the electromagnetic modeling of lattice structures used in additively manufactured magnetic cores or windings for electric machines. Three dimensional (3D) electromagnetic finite element (FE) analysis with high performance computing (HPC) shows the highest fidelity in predicting the electromagnetic performance of designs with lattice structures by preserving complex geometry details. FE-based homogenization methods have also been explored to potentially speed up concept design. A case study based on an additively manufactured axial-flux permanent magnet machine with a Hilbert pattern stator validates the discussed electromagnetic modeling approaches.

Chung, Shi-Uk [ANSYS, Inc.]↗
DOE OSTI2019

Mechanical Utility Structure for Testing High Field Superconducting Dipole Magnets

The U.S. Magnet Development Program (MDP) collaboration is designing a utility mechanical structure for testing various high-field superconducting dipole coils. The design uses a shell-based structure concept, which allows applying preload in two steps: During a room temperature assembly and during a cool down to a cryogenic temperature. The structure is designed to accommodate various coil designs - including Nb 3 Sn Cosine Theta (CT) and Canted CT magnets as well as hybrid magnets with high temperature superconductor cables. Superconducting coils, enclosed by bolted pads to form an octagonal coil pack, will be inserted into a reusable yoke-shell subassembly and precisely preloaded during the assembly using a bladder-and-key technology. Due to a differential thermal contraction between an external aluminum shell and the magnet core, the coil preload increases during the cool down up to level required for 17-T excitation. Such a reusable structure will serve as a testing fixture supporting goals of the MDP program, decreasing cost and simplifying coil performance testing at different preload levels. We present a finite-element analysis of the structure preloading various coil designs and examine the predicted coil stress at each step of the magnet assembly and excitation.

43 PARTICLE ACCELERATORS↗
DOE OSTI2018

Magnetic properties of superparamagnetic, nanocrystalline cobalt ferrite thin films deposited at low temperature

Bulk cobalt ferrite, being a hard ferrite, shows high magnetization, high resistivity and high coercivity. If thin films of cobalt ferrite can be deposited at a low enough temperature and if its coercivity can be reduced, cobalt ferrite will make a very good candidate for use as a magnetic core of an integrated inductor in RF-CMOS ICs. Though polycrystalline and epitaxial thin films of cobalt ferrite have been made by various techniques, there are no reports of thin films of superparamagnetic cobalt ferrite. In this work, nanocrystalline cobalt ferrite thin films, which are superparamagnetic as deposited, have been prepared in the solution medium at ~190 °C, using microwave irradiation. The as-prepared films have a saturation magnetization (M S ) of 401 emu/cc and coercivity (H C ) of 19 Oe at room temperature for a crystallite size of 2 nm. The cobalt ferrite powder obtained as a by-product during the same process has M S of 50 emu/g and H C of 5 Oe at room temperature, making it superparamagnetic. The as-prepared films were annealed in air at 300 °C for 5 min and 10 min. Annealing for 10 min results in an increase in crystallite size to 36 nm, M S increases from 401 emu/cc to 545 emu/cc, and H C increases from 19 Oe to 860 Oe. In conclusion, the change in magnetic properties can be directly associated with change in the crystallite size and degree of crystallographic inversion, as determined by neutron diffraction and deduced from X-ray photoelectron spectroscopy.

36 MATERIALS SCIENCE↗
DOE OSTI2014

Local modification of the magnetic vortex-core velocity by gallium implantation

The dynamics of magnetic vortices in microsquares with local modifications of magnetic parameters and thickness are investigated. By implanting gallium ions with focussed ion beam into permalloy thin-film elements, we have locally tailored their magnetic properties and the layer thickness. The vortex of the Landau domain pattern of a square is resonantly excited to a gyrotropic motion and crosses regions with and without implantation. With time-resolved scanning transmission x-ray microscopy, we observe an abrupt change in the vortex velocity close to the borders between the two regions.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2017

Magnetized Converging Flows toward the Hot Core in the Intermediate/High-mass Star-forming Region NGC 6334 V

We present Submillimeter Array (SMA) observations at 345 GHz toward the intermediate/high-mass cluster-forming region NGC 6334 V. From the dust emission we spatially resolve three dense condensations, the brightest one presenting the typical chemistry of a hot core. The magnetic field (derived from the dust polarized emission) shows a bimodal converging pattern toward the hot core. The molecular emission traces two filamentary structures at two different velocities, separated by 2 km s{sup −1}, converging to the hot core and following the magnetic field distribution. We compare the velocity field and the magnetic field derived from the SMA observations with magnetohydrodynamic simulations of star-forming regions dominated by gravity. This comparison allows us to show how the gas falls in from the larger-scale extended dense core (∼0.1 pc) of NGC 6334 V toward the higher-density hot core region (∼0.02 pc) through two distinctive converging flows dragging the magnetic field, whose strength seems to have been overcome by gravity.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2013

Reversible Single Spin Control of Individual Magnetic Molecule by Hydrogen Atom Adsorption

The reversible control of a single spin of an atom or a molecule is of great interest in Kondo physics and a potential application in spin based electronics. Here we demonstrate that the Kondo resonance of manganese phthalocyanine molecules on a Au(111) substrate have been reversibly switched off and on via a robust route through attachment and detachment of single hydrogen atom to the magnetic core of the molecule. As further revealed by density functional theory calculations, even though the total number of electrons of the Mn ion remains almost the same in the process, gaining one single hydrogen atom leads to redistribution of charges within 3d orbitals with a reduction of the molecular spin state from S 5 3/2 to S 5 1 that directly contributes to the Kondo resonance disappearance. This process is reversed by a local voltage pulse or thermal annealing to desorb the hydrogen atom.

36 MATERIALS SCIENCE↗
DOE OSTI2014

Collapse and fragmentation of magnetic molecular cloud cores with the Enzo AMR MHD code. II. Prolate and oblate cores

We present the results of a large suite of three-dimensional models of the collapse of magnetic molecular cloud cores using the adaptive mesh refinement code Enzo2.2 in the ideal magnetohydrodynamics approximation. The cloud cores are initially either prolate or oblate, centrally condensed clouds with masses of 1.73 or 2.73 M {sub ☉}, respectively. The radial density profiles are Gaussian, with central densities 20 times higher than boundary densities. A barotropic equation of state is used to represent the transition from low density isothermal phases, to high density optically thick phases. The initial magnetic field strength ranges from 6.3 to 100 μG, corresponding to clouds that are strongly to marginally supercritical, respectively, in terms of the mass to magnetic flux ratio. The magnetic field is initially uniform and aligned with the clouds' rotation axes, with initial ratios of rotational to gravitational energy ranging from 10{sup –4} to 0.1. Two significantly different outcomes for collapse result: (1) formation of single protostars with spiral arms, and (2) fragmentation into multiple protostar systems. The transition between these two outcomes depends primarily on the initial magnetic field strength, with fragmentation occurring for mass to flux ratios greater than about 14 times the critical ratio for prolate clouds. Oblate clouds typically fragment into several times more clumps than prolate clouds. Multiple, rather than binary, system formation is the general rule in either case, suggesting that binary stars are primarily the result of the orbital dissolution of multiple protostar systems.

79 ASTRONOMY AND ASTROPHYSICS↗
DOE OSTI2015

Micromagnetic model analysis of integrated single-pole-type head with tilted spin-torque oscillator for high-frequency microwave-assisted magnetic recording

The spin-torque oscillator (STO) is the most important component in microwave-assisted magnetic recording. Some requirements for the STO are: large amplitude and stable oscillation, small injected current, and oscillation at a frequency that excites resonance in a recording medium. It is also necessary for the STO oscillation to closely follow the head coil current. In this paper, STOs were integrated into write heads and micromagnetic analyses carried out to obtain a write head structure with stable STO oscillation that could follow a high-frequency head coil current.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2024

Core inductive electric field during sawtooth crashes on DIII-D

Sawtooth crashes on tokamak plasmas exhibit relaxation much faster than resistive time scales via a mechanism not fully understood. Using core magnetic measurements from the Radial Interferometer-Polarimeter (RIP) diagnostic on the DIII-D tokamak, Grad–Shafranov equilibria constrained by internal magnetic measurements that have high time resolution (<1μs) can be computed, allowing analysis of how equilibrium parameters such as safety factor q, current density J, and parallel electric field E ∥ , particularly on-axis, evolve. At the sawtooth crash, on-axis safety factor q 0 is observed to rise by 5% but remain below 1 throughout the cycle, and on-axis current density J 0 is observed to drop by 5%. On-axis parallel electric field E ∥ (0) is found to be balanced by ηJ 0 (resistivity times on-axis current density) except during the 200 µs crash period, where E ∥ (0) reaches 22 V m –1 , exceeding ηJ 0 by a factor of more than 2000. These first measurements in tokamak plasmas verify that generalized Ohm's law is not balanced during the crash by resistive effects alone; this is a finding expected due to the relaxation being much faster than resistive timescales. As a result, measurement of the electric field during the tokamak sawtooth serves to illuminate the physical mechanisms at work.

70 PLASMA PHYSICS AND FUSION TECHNOLOGY↗