Combined study program. Volume 5 - Direct entry accumulator cell molecular beam ion source Final report
Molecular beam ion source for spacecraft mass spectrometer atmospheric sensor system
Rotheram, M.↗
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Ion beam texturing
A microscopic surface texture is created by sputter etching a surface while simultaneously sputter depositing a lower sputter yield material onto the surface. A xenon ion beam source has been used to perform this texturing process on samples as large as three centimeters in diameter. Ion beam textured surface structures have been characterized with SEM photomicrographs for a large number of materials including Cu, Al, Si, Ti, Ni, Fe, Stainless steel, Au, and Ag. Surfaces have been textured using a variety of low sputter yield materials - Ta, Mo, Nb, and Ti. The initial stages of the texture creation have been documented, and the technique of ion beam sputter removal of any remaining deposited material has been studied. A number of other texturing parameters have been studied such as the variation of the texture with ion beam power, surface temperature, and the rate of texture growth with sputter etching time.
Hudson, W. R.↗
Rethinking radiation effects in materials science using the plasma-focused ion beam
This work demonstrates the viability of using a plasma-focused ion beam (PFIB) as a new platform to carry out radiation effects studies in solids. While materials subjected to irradiation in either nuclear reactors or energetic particle accelerators experience limitations with respect to inaccuracies in both flux measurements and lack of precise control of irradiation areas, we demonstrate a new irradiation technique that allows the exposure of a single specimen in multiple areas, at multiple doses, and in site-specific dependencies - all with flux variations on the order of only 1%. This versatile technique also allows materials to be exposed to significantly higher irradiation dose rates than conventional accelerators. To validate the new methodology, we selected the classical example of ion-beam-induced amorphization of pure single-crystal Si. By pioneering the use of the PFIB for radiation effects studies in materials science, we were able to exploit, in both micro- and nanometer-sized detail, the differences in electron image contrast arising from crystalline versus amorphous solid-state phases in classical semiconductors subjected to irradiation, thus providing new insights on amorphization mechanisms. This methodology opens new research frontiers at the fringe of materials science with promising applications beyond the scope of materials at extremes such as in nanopatterning, nanodevices and nanoarchitectonics.
36 MATERIALS SCIENCE↗
Characteristics of the ULF waves associated with upstream ion beams
A new class of upstream wave is reported with relatively high frequencies of about 1 Hz and small amplitudes compared to the more common larger amplitude, low-frequency (0.03 Hz) upstream wave. The waves were first noted in association with beams of ions reflected back upstream at the bowshock, and although beam presence appears to be a necessary condition for the observation of the waves, it is not a sufficient condition for the existence of the waves. Magnetometer measurements are used to determine intrinsic properties of the waves, and simultaneous two point measurements are used to calculate and eliminate Doppler shifting effects. Results indicate that the waves are right-hand elliptically polarized whistler mode waves with plasma rest frame frequencies of about 20-100 times the proton gyrofrequency and wavelengths of about 100 km.
Hoppe, M. M.↗
Sputter sample preparation for ion beam delivery of radium-223 at ATLAS
A radium-223 ion beam was delivered to an experiment from the electron cyclotron resonance ion source, ECR2, at the Argonne Tandem Linac Accelerator System (ATLAS). Here, the radium-223 material was in a nitrate salt form within a vial, prior to being converted to a usable sputter sample. The sputter sample was produced using a new sample preparation method, where the radium nitrate was dissolved into a solution and pipetted onto pressed aluminum powder. This sample was then allowed to dry, distributing the radium-223 material throughout the sputter sample. Ion source operation using the radium sputter sample is described with the operating parameters listed. The intensity and energy requirements for this ion beam were 1 × 10 6 particles/s and 1.07 GeV, respectively. Because the intensity is relatively low compared to most experiments at ATLAS, previously developed accelerator mass spectrometry methods were used Scott et al. to avoid the need for tuning of the low-intensity beam of interest. Handling of the radium material, as well as loading and unloading of the sputter sample from ECR2, required collaboration with Health Physics. Procedures were used and dry runs were carried out before, during, and after the experiment to ensure the safety of the workers. The processes used and lessons learned are described within.
07 ISOTOPE AND RADIATION SOURCES↗
Selective patterning of out-of-plane piezoelectricity in MoTe 2 via focused ion beam
Two-dimensional transition-metal dichalcogenides (TMDs) have a strain-sensitive nature and can only exhibit in-plane piezoelectricity, owing to their in-plane inversion symmetry breaking, which limits their practical applications for vertical stimulations. Here, we demonstrated the capability of focused ion beams to create out-of-plane piezoelectricity on multi-layered MoTe 2 . We utilized a focused helium ion beam to selectively pattern the out-of-plane piezoelectricity via defect engineering in a layered MoTe 2 flake. The generated out-of-plane piezoelectricity in the desired area was quantitatively examined using atomic force microscopy, and ion beam irradiation-induced defect formation that gave rise to inversion symmetry breaking was confirmed. These results indicated that the out-of-plane piezoelectricity can be selectively patterned through a focused helium ion beam, and it is expected that this approach can also be applied to other classes of TMDs and can expand the application fields of TMD-based devices.
36 MATERIALS SCIENCE↗
Transfer Casting From Ion-Beam-Textured Surfaces
Textured surfaces created on metals, ceramics, and polymers. Electron-bombardment ion thrustor used as neutralized-ion-beam source. Beam of directed, energetic ions alter surface chemistry and/or morphology of many materials. By adjusting ion energy and ion-beam current density impinging upon target, precise surface modifications obtained without risk of targetmaterial melting or bulk decomposition. Technique developed to generate precise, controllable, surface microstructures on metals, ceramics, and polymers.
Banks, B. A.↗
Broadband electrostatic noise produced by ion beams in the earth's magnetotail
Spacecraft observations in the earth's magnetotail at distances of 30 to 40 R(E) have revealed the presence of broadband electrostatic waves. These waves are generally most intense in the regions just outside of the plasma sheet and are correlated with the observations of relatively cold and energetic ion beams traveling in either the earthward or the tailward direction. These waves are observed to propagate obliquely to the geomagnetic field with wave normal angles around 70 deg. Because the broadband electrostatic noise is the most intense of the waves observed in the magnetotail, it is important to understand the generation mechanism of these waves. The purpose of this study is to provide for the first time a correct solution to the dispersion equation for ion beams observed in the magnetotail. By numerically solving this equation, it is shown that obliquely propagating waves have growth rates that can be an order of magnitude larger than those of parallel propagating waves, in agreement with observations. In addition, the effect of beam temperature on the ion beam instability is studied, and it is shown that this instability can be a viable generation mechanism only when the ion beam has a relatively small thermal spread.
Omidi, N.↗
Plasma waves produced by the xenon ion beam experiment on the Porcupine sounding rocket
The production of electrostatic ion cyclotron waves by a perpendicular ion beam in the F-region ionosphere is described. The ion beam experiment was part of the Porcupine program and produced electrostatic hydrogen cyclotron waves just above harmonics of the hydrogen cyclotron frequency. The plasma process may be thought of as a magnetized background ionosphere through which an unmagnetized beam is flowing. The dispersion equation for this hypothesis is constructed and solved. Preliminary solutions agree well with the observed plasma waves.
Kintner, P. M.↗
Ion-beam focusing in a double-plasma device
The authors studied the propagation of a low-energy charge-neutralized ion beam injected into the target region of a long double-plasma device. A magnetic field of up to about 180 G may be applied along the axis of the device. As a result of charge exchange collisions, the ion beam is attenuated as it propagates into the target region. However, under certain conditions of magnetic field strength and neutral gas pressure, the authors have observed a `reemergence' of the beam on axis far downstream in the target. This reemergence of the ion beam is attributed to a focusing of the ions by a self-consistently produced radial ambipolar electric field. The effect may be expected to occur in other types of plasma devices as well, whenever a sufficiently large radially inward electric field is present.
Johnson, James C.↗
Electrostatic ion (hydrogen) cyclotron and ion acoustic wave instabilities in regions of upward field-aligned current and upward ion beams
An investigation is made into the stability of electrostatic hydrogen ion cyclotron and ion acoustic waves in a model plasma where an ion beam, population 2, and oppositely directed drifting electrons pass through a stationary ion background, population 1. The excited wave properties are then compared with the characteristics of the unstable modes observed on the S3-3 satellite. Three temperature regimes are studied: (1) Te greater than Ti2 much greater than Ti1, (2) Ti2 greater than Te not less than Ti1, and (3) Te approximately equal to Ti1 greater than Ti2. It is found that the ion beam acts as a free energy source only in regime 1. This regime is also highly unstable to the electrons as a free energy source. Unstable modes in regimes 2 and 3 seem to best satisfy the electrostatic hydrogen cyclotron wave (EHC) properties at 1 earth radius. For these cases the electrons are the free energy source, the beam supplies damping.
Bergmann, R.↗
Optical and electrical properties of ion beam textured Kapton and Teflon
Results are given for ion beam texturing of polyimide (Kapton) and fluorinated ethylene propylene (Teflon) by means of a 30-cm diam electron bombardment argon ion source. Ion beam-textured Kapton and Teflon surfaces are evaluated for various beam energies, current densities, and exposure times. The optical properties and sheet resistance are measured after each exposure. Provided in the paper are optical spectral data, resistivity measurements, calculated absorptance and emittance measurements, and surface structure SEM micrographs for various exposures to argon ions. It is found that Kapton becomes conducting and Teflon nonconducting when ion beam-textured. Textured Kapton exhibits large changes in the transmittance and solar absorptance, but only slight changes in reflectance. Surface texturing of Teflon may allow better adherence of subsequent sputtered metallic films for a high absorptance value. The results are valuable in spacecraft charging applications.
Mirtich, M. J.↗
Optical and scratch resistant properties of diamondlike carbon films deposited with single and dual ion beams
Amorphous diamondlike carbon (DLC) films were deposited using both single and dual ion beam techniques utilizing filament and hollow cathode ion sources. Continuous DLC films up to 3000 A thick were deposited on fused quartz plates. Ion beam process parameters were varied in an effort to create hard, clear films. Total DLC film absorption over visible wavelengths was obtained using a Perkin-Elmer spectrophotometer. An ellipsometer, with an Ar-He laser (wavelength 6328 A) was used to determine index of refraction for the DLC films. Scratch resistance and frictional and adherence properties were determined for select films. Applications for these films range from military to the ophthalmic industries.
Kussmaul, Michael T.↗
Harvesting 88 Zr from heavy-ion beam irradiated tungsten at the National Superconducting Cyclotron Laboratory
Tungsten is a commonly used material at many heavy-ion beam facilities, and it often becomes activated due to interactions with a beam. Many of the activation products are useful in basic and applied sciences if they can be recovered efficiently. In order to develop the radiochemistry for harvesting group (IV) elements from irradiated tungsten, a heavy-ion beam containing 88 Zr was embedded into a stack of tungsten foils at the National Superconducting Cyclotron Laboratory and a separation methodology was devised to recover the 88 Zr. The foils were dissolved in 30% hydrogen peroxide, and the 88 Zr was chemically purified from the tungsten matrix and from other co-implanted radionuclides (such as 85 Sr and 88 Y) using strong cation-exchange (AG MP-50) chromatographic resin in sulfuric acid media. The procedure provided 88 Zr in approximately 60 mL 0.5 M sulfuric acid with no detectable radio-impurities. The overall recovery yield for 88 Zr was (92.3 ± 1.2)%. In conclusion, this proof-of-concept experiment has facilitated the development of methodologies to harvest from tungsten and tungsten-alloy parts that are regularly irradiated at heavy-ion beam facilities.
07 ISOTOPE AND RADIATION SOURCES↗
Ion beam deposited protective films
Sputter deposition of adherent thin films on complex geometric surfaces by ion beam sources is examined in order to evaluate three different types of protective coatings for die materials. In the first experiment, a 30 cm diameter argon ion source was used to sputter deposit adherent metallic films up to eight microns thick on H-13 steel, and a thermal fatigue test specimen sputter deposited with metallic coatings one micron thick was immersed in liquid aluminum and cooled by water for 15,000 cycles to simulate operational environments. Results show that these materials do protect the steel by reducing thermal fatigue and thereby increasing die lifetime. The second experiment generated diamond-like carbon films using a dual beam ion source system that directed an eight cm argon ion source beam at the substrates. These films are still in the process of being evaluated for crystallinity, hardness and infrared absorption. The third experiment coated a fiber glass beam shield incorporated in the eight-cm diameter mercury ion thruster with molybdenum to ensure proper electrical and thermal properties. The coating maintained its integrity even under acceleration tests.
Mirtich, M. J.↗
Diffuse ions produced by electromagnetic ion beam instabilities
The evolution of the electromagnetic ion beam instability driven by the reflected ion component backstreaming away from the earth's bow shock into the foreshock region is studied by means of computer simulation. The linear and quasi-linear stages of the instability are found to be in good agreement with known results for the resonant mode propagating parallel to the beam along the magnetic field and with theory developed in this paper for the nonresonant mode, which propagates antiparallel to the beam direction. The quasi-linear stage, which produces large amplitude delta B approximately B, sinusoidal transverse waves and 'intermediate' ion distributions, is terminated by a nonlinear phase in which strongly nonlinear, compressive waves and 'diffuse' ion distributions are produced. Additional processes by which the diffuse ions are accelerated to observed high energies are not addressed. The results are discussed in terms of the ion distributions and hydromagnetic waves observed in the foreshock of the earth's bow shock and of interplanetary shocks.
Winske, D.↗
NEUTRALIZATION OF ION BEAMS FROM ENGINES OF ANNULAR GEOMETRY
Neutralization of ion beams from engines of annular geometry
ION ENGINE↗
Ion beam microtexturing of surfaces
Some recent work in surface microtecturing by ion beam sputtering is described. The texturing is accomplished by deposition of an impurity onto a substrate while simultaneously bombarding it with an ion beam. A summary of the theory regarding surface diffusion of impurities and the initiation of cone formation is provided. A detailed experimental study of the time-development of individual sputter cones is described. A quasi-liquid coating was observed that apparently reduces the sputter rate of the body of a cone compared to the bulk material. Experimental measurements of surface diffusion activation energies are presented for a variety of substrate-seed combinations and range from about 0.3 eV to 1.2 eV. Observations of apparent crystal structure in sputter cones are discussed. Measurements of the critical temperature for cone formation are also given along with a correlation of critical temperature with substrate sputter rate.
Robinson, R. S.↗