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At least 145 records · Page 8

Stirling Technology Development at NASA GRC

The Department of Energy, Stirling Technology Company (STC), and NASA Glenn Research Center (NASA Glenn) are developing a free-piston Stirling convertor for a high-efficiency Stirling Radioisotope Generator (SRG) for NASA Space Science missions. The SRG is being developed for multimission use, including providing electric power for unmanned Mars rovers and deep space missions. NASA Glenn is conducting an in-house technology project to assist in developing the convertor for space qualification and mission implementation. Recent testing, of 55-We Technology Demonstration Convertors (TDC's) built by STC includes mapping, of a second pair of TDC's, single TDC testing, and TDC electromagnetic interference and electromagnetic compatibility characterization on a nonmagnetic test stand. Launch environment tests of a single TDC without its pressure vessel to better understand the convertor internal structural dynamics and of dual-opposed TDC's with several engineering mounting structures with different natural frequencies have recently been completed. A preliminary life assessment has been completed for the TDC heater head, and creep testing of the IN718 material to be used for the flight convertors is underway. Long-term magnet aging tests are continuing to characterize any potential aging in the strength or demagnetization resistance of the magnets used in the linear alternator (LA). Evaluations are now beginning on key organic materials used in the LA and piston/rod surface coatings. NASA Glenn is also conducting finite element analyses for the LA, in part to look at the demagnetization margin on the permanent magnets. The world's first known integrated test of a dynamic power system with electric propulsion was achieved at NASA Glenn when a Hall-effect thruster was successfully operated with a free-piston Stirling power source. Cleveland State University is developing a multidimensional Stirling computational fluid dynamics code to significantly improve Stirling loss predictions and assist in identifying convertor areas for further improvements. This paper will update the status and results for these efforts.

Thieme, Lanny G.↗

Magnetic Analysis Techniques Applied to Desert Varnish

Desert varnish is a black or reddish coating commonly found on rock samples from arid regions. Typically, the coating is very thin, less than half a millimeter thick. Previous research has shown that the primary components of desert varnish are silicon oxide clay minerals (~60%), manganese and iron oxides (~20-30%), and trace amounts of other compounds [1]. Desert varnish is thought to originate when windborne particles containing iron and manganese oxides are deposited onto rock surfaces where manganese oxidizing bacteria concentrate the manganese and form the varnish [4,5]. If desert varnish is indeed biogenic, then the presence of desert varnish on rock surfaces could serve as a biomarker, indicating the presence of microorganisms. This idea has considerable appeal, especially for Martian exploration [6]. Magnetic analysis techniques have not been extensively applied to desert varnish. The only previous magnetic study reported that based on room temperature demagnetization experiments, there were noticeable differences in magnetic properties between a sample of desert varnish and the substrate sandstone [7]. Based upon the results of the demagnetization experiments, the authors concluded that the primary magnetic component of desert varnish was either magnetite (Fe3O4) or maghemite ( Fe2O3).

Schmidgall, E. R.↗

Continuous Magnetic Refrigerators for Cooling in the 0.05 to 10 K Range: Progress and Future Development

Low temperature refrigeration is an increasingly vital technology for NASA s Space Science program since most detectors being developed for x-ray, IR and sub-millimeter missions must be cooled to below 100 mK in order to meet the requirements for energy and spatial resolution. For space applications, magnetic refrigeration has an inherent advantage over alternative techniques because it does not depend on gravity. Adiabatic demagnetization refrigerators, or ADRs, are relatively simple, solid state devices. The basic elements are a magnetocaloric refrigerant (usually an encapsulated paramagnetic salt) located in the bore of a superconducting magne$, and a heat switch linking the salt to a heat sink. The alignment of magnetic spins with the magnetic field causes the refrigerant to warm as the magnetic field increases and cool as the field decreases. Thus the simple process of magnetizing the refrigerant to high field with the heat switch closed, then demagnetizing it with the heat switch open allows one to obtain temperatures well below 100 mK using a heat sink as warm as 4.2 K. The refrigerant can maintain a low temperature for a length of time depending on the applied and parasitic heat loads, its mass, and the initial magnetic field strength. Typically ADRs are designed for 12-24 hours of hold time, after which they must be warmed up and recycled. The drawback to single-shot ADRs is that the cooling power per unit mass is relatively low. Refrigerants that are suitable for low temperature operation necessarily have low magnetic ion density, and therefore low entropy density. Since ADRs store entropy, systems with even modest cooling powers (a few microwatts) at temperatures below 100 mK tend to be massive, averaging 10-15 kg.

Shirron, Peter↗

A Comparative Analysis of the Magnetic Field Signals over Impact Structures on the Earth, Mars and the Moon

An improved description of magnetic fields of terrestrial bodies has been obtained from recent space missions, leading to a better characterization of the internal fields including those of crustal origin. One of the striking differences in their crustal magnetic field is the signature of large impact craters. A comparative analysis of the magnetic characteristics of these structures can shed light on the history of their respective planetary-scale magnetic dynamos. This has motivated us to identify impact craters and basins, first by their quasi-circular features from the most recent and detailed topographic maps and then from available global magnetic field maps. We have examined the magnetic field observed above 27 complex craters on the Earth, 34 impact basins on Mars and 37 impact basins on the Moon. For the first time, systematic trends in the amplitude and frequency of the magnetic patterns, inside and outside of these structures are observed for all three bodies. The demagnetization effects due to the impact shock wave and excavation processes have been evaluated applying the Equivalent Source Dipole forward modeling approach. The main characteristics of the selected impact craters are shown. The trends in their magnetic signatures are indicated, which are related to the presence or absence of a planetary-scale dynamo at the time of their formation and to impact processes. The low magnetic field intensity at center can be accepted as the prime characteristic of a hypervelocity impact and strongly associated with the mechanics of impact crater formation. In the presence of an active internal field, the process of demagnetization due to the shock impact is associated with post-impact remagnetization processes, generating a more complex magnetic signature.

Earth↗

Electron-Scale Measurements of Magnetic Reconnection in Space

Magnetic reconnection is a fundamental physical process in plasmas whereby stored magnetic energy is converted into heat and kinetic energy of charged particles. Reconnection occurs in many astrophysical plasma environments and in laboratory plasmas. Using measurements with very high time resolution, NASA's Magnetospheric Multiscale (MMS) mission has found direct evidence for electron demagnetization and acceleration at sites along the sunward boundary of Earth's magnetosphere where the interplanetary magnetic field reconnects with the terrestrial magnetic field. We have (i) observed the conversion of magnetic energy to particle energy; (ii) measured the electric field and current, which together cause the dissipation of magnetic energy; and (iii) identified the electron population that carries the current as a result of demagnetization and acceleration within the reconnection diffusion/dissipation region.

Burch, J. L.↗

Finite Gyroradius Effects in the Electron Outflow of Asymmetric Magnetic Reconnection

We present observations of asymmetric magnetic reconnection showing evidence of electron demagnetization in the electron outflow. The observations were made at the magnetopause by the four Magnetospheric Multiscale (MMS) spacecraft, separated by approximately 15 km. The reconnecting current sheet has negligible guide field, and all four spacecraft likely pass close to the electron diffusion region just south of the X line. In the electron outflow near the X line, all four spacecraft observe highly structured electron distributions in a region comparable to a few electron gyroradii. The distributions consist of a core with T(sub parallel) greater than T(sub perpendicular) and a nongyrotropic crescent perpendicular to the magnetic field. The crescents are associated with finite gyroradius effects of partly demagnetized electrons. These observations clearly demonstrate the manifestation of finite gyroradius effects in an electron-scale reconnection current sheet.

Norgren, C.↗

Mechanical Design of a 4-Stage ADR for the PIPER mission

The four 1,280 bolometer detector arrays that will fly on the balloon borne PIPER mission will be cooled by a 4-stage adiabatic demagnetization refrigerator (ADR). Two of the three mechanically independent ADR assemblies provide thermal isolation to their salt pills through Kevlar suspensions while the other provides thermal isolation to its salt pill through the use of bellows and Vespel material. The ADR integrates with the detector arrays and it sits in a large bucket Dewar containing superfluid liquid helium. This paper will describe the complex mechanical design of the PIPER ADR, and summarize the mechanical analysis done to validate the design.The four 1,280 bolometer detector arrays that will fly on the balloon borne PIPER mission will be cooled by a 4-stage adiabatic demagnetization refrigerator (ADR). Two of the three mechanically independent ADR assemblies provide thermal isolation to their salt pills through Kevlar suspensions while the other provides thermal isolation to its salt pill through the use of bellows and Vespel material. The ADR integrates with the detector arrays and it sits in a large bucket Dewar containing superfluid liquid helium. This paper will describe the complex mechanical design of the PIPER ADR, and summarize the mechanical analysis done to validate the design.

Cryogenics↗

In-Orbit Selection of Cryocooler Drive Frequencies for XRISM/Resolve

The XRISM/Resolve instrument cooling system uses adiabatic demagnetization refrigerators (ADRs) to cool the detectors to 50 mK and two types of cryocoolers to reduce heat load on the He tank, Joule-Thomson and Stirling cryocoolers. Resolve was designed with tunable cryocooler frequencies so that any mechanical interference and its effect on performance could be minimized. Measurements at different cryocooler drive frequencies were used to quantify the interference and narrow the acceptable range of frequency options. For Resolve the choice of cryocooler drive frequencies dramatically influences the instrument performance. Poor choices have been shown to degrade ADR cooling power and degrade the spectroscopic performance of the instrument. However, good choices have been shown to be free of undesirable features, allowing the instrument to satisfy its performance requirements with significant margin. Thus, the choice of drive frequencies is a critical factor for overall instrument performance. The drive frequencies of the Joule-Thomson cooler operating near 52 Hz, and the Stirling coolers operating near 15 Hz were adjusted in three distinct scan sequences to efficiently narrow the candidate frequency options. The frequency choices were based on stability of the 50 mK control thermometer, changes in the ADR demagnetization rate, and changes in detector noise. Scans across the drive frequency range of each cryocooler were performed multiple times during ground testing. Surprisingly, the results were not repeatable across test campaigns and did not conform to any discernable trend, but they were repeatable when remeasured within a single cool-down cycle. The conclusion was that the good/bad drive frequencies changed during Dewar warmup/cooldown, and possibly after mechanical vibration tests. Therefore, the settings could not be finalized before launch, and scans during instrument commissioning were necessary. This paper describes the cryocooler frequency scan measurements and compares the results during instrument commissioning to those performed during ground tests.

Gary A. Sneiderman↗

In-Orbit Selection of Cryocooler Drive Frequencies for XRISM/Resolve

The XRISM/Resolve instrument cooling system uses adiabatic demagnetization refrigerators (ADRs) to cool the detectors to 50 mK and Joule-Thomson and Stirling cryocoolers to reduce heat load on the He tank supporting the ADRs. Resolve was designed with tunable cryocooler drive frequencies so that interference could be avoided. The cryocooler generated micro-vibration changes with drive frequency and that micro-vibration causes interference and degrades instrument performance. Poor drive frequency choices have been shown to dramatically impact ADR cooling power, temperature stability, detector noise, and degrading spectroscopic performance. However, some choices are free of these features, allowing the instrument to satisfy its performance requirements with significant margin. Thus, the choice of drive frequencies is critical to achieving peak instrument performance. The drive frequencies of the Joule-Thomson cooler, near 52 Hz, and the Stirling coolers, near 15 Hz, were adjusted in three scan sequences while measuring interference to narrow candidate frequency options. Choices were based on stability of the 50 mK control thermometer, changes in the ADR demagnetization rate, and changes in detector noise. These scans were performed routinely during ground testing. Surprisingly though, the results were not repeatable after the Dewar was warmed and re-cooled but were repeatable when remeasured during the same test campaign. Since the good/bad drive frequencies change during Dewar warmup/cooldown, and possibly after vibration events, the drive frequencies could not be finalized before launch. This paper describes the cryocooler frequency scan measurements and compares the results during instrument commissioning to those performed during ground tests.

XRISM↗

In-Orbit Selection of Cryocooler Drive Frequencies for XRISM/Resolve

The XRISM/Resolve instrument cooling system uses adiabatic demagnetization refrigerators (ADRs) to cool the detectors to 50 mK and two types of cryocoolers to reduce heat load on the He tank, Joule-Thomson and Stirling cryocoolers. Resolve was designed with tunable cryocooler frequencies so that any mechanical interference and its effect on performance could be minimized. Measurements at different cryocooler drive frequencies were used to quantify the interference and narrow the acceptable range of frequency options. For Resolve the choice of cryocooler drive frequencies dramatically influences the instrument performance. Poor choices have been shown to degrade ADR cooling power and degrade the spectroscopic performance of the instrument. However, good choices have been shown to be free of undesirable features, allowing the instrument to satisfy its performance requirements with significant margin. Thus, the choice of drive frequencies is a critical factor for overall instrument performance. The drive frequencies of the Joule-Thomson cooler operating near 52 Hz, and the Stirling coolers operating near 15 Hz were adjusted in three distinct scan sequences to efficiently narrow the candidate frequency options. The frequency choices were based on stability of the 50 mK control thermometer, changes in the ADR demagnetization rate, and changes in detector noise. Scans across the drive frequency range of each cryocooler were performed multiple times during ground testing. Surprisingly, the results were not repeatable across test campaigns and did not conform to any discernable trend, but they were repeatable when remeasured within a single cool-down cycle. The conclusion was that the good/bad drive frequencies changed during Dewar warmup/cooldown, and possibly after mechanical vibration tests. Therefore, the settings could not be finalized before launch, and scans during instrument commissioning were necessary. This paper describes the cryocooler frequency scan measurements and compares the results during instrument commissioning to those performed during ground tests.

XRISM↗

Active magnetic regenerative liquefier using process gas pre-cooling from bypass flow of heat transfer fluid

A process for liquefying a process gas that includes: introducing a heat transfer fluid into an active magnetic regenerative refrigerator apparatus that includes a low magnetic or demagnetized field section; continuously diverting a bypass portion of the heat transfer fluid from a cold side of the low magnetic or demagnetized field section into a bypass flow heat exchanger at a first cold inlet temperature; and continuously introducing the process gas into the bypass flow heat exchanger at a first hot inlet temperature and discharging the process gas or liquid from the bypass flow heat exchanger at a first cold exit temperature; wherein the temperature difference between bypass heat transfer first cold inlet temperature and the process gas first cold exit temperature is 1 to 5 K.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Magnetic Properties of (Pr{sub 1−x}Sm{sub x}){sub 2}Fe{sub 14}B Melt-Spun Ribbons

The magnetic properties of (Pr{sub 1−x}Sm{sub x}){sub 2}Fe{sub 14}B melt-spun ribbons with varying x from 0 to 1.0 have been studied. The optimum magnetic property of Pr{sub 2}Fe{sub 14}B ribbon could be obtained with the surface velocity of copper wheel of 30 m/s. By melt spinning method, the formation of α-Fe impurity phase in the (Pr{sub 1−x}Sm{sub x}){sub 2}Fe{sub 14}B samples could be inhibited, and the grain could be aligned. Sm element could be incorporated into Pr{sub 2}Fe{sub 14}B main crystalline phase and formed (Pr,Sm){sub 2}Fe{sub 14}B phase with space group P4{sub 2}/mnm. The Curie temperature (T{sub c}) of the (Pr{sub 1−x}Sm{sub x}){sub 2}Fe{sub 14}B ribbons increases gradually from 555 to 617 K with the increase of Sm content x. Both the coercivity (H{sub c}) and remanence ratio (M{sub r}/M{sub s}) decrease firstly and then increase with the Sm content increasing. As long as the Sm content x does not exceed 0.1, the squareness of demagnetization curve remains good. The critical value of transition from easy c-axis to easy plane for (Pr{sub 1−x}Sm{sub x}){sub 2}Fe{sub 14}B ribbons is x= 0.6. When the Sm content x is up to 0.6, all the H{sub c} and M{sub r}/M{sub s} achieved the minimum value, i.e., 243 Oe and 0.346, respectively.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

Terahertz inverse spin Hall effect in spintronic nanostructures with various ferromagnetic materials

Bilayers of ferromagnetic and heavy metal nanolayers excited with femtosecond laser pulses emit subpicosecond bursts of electromagnetic radiation with spectral frequencies up to several THz. We fabricated such spintronic THz emitters containing various ferromagnetic materials with vastly different magnetic remanence, saturation magnetization, and coercive fields. In all cases, the THz amplitude versus magnetic-field dependence follows the independently measured magnetization hysteresis loops and the THz polarization direction is perpendicular to the sample’s magnetization M, both consistent with the inverse spin Hall effect (ISHE) as the physical origin. The mV-level signals of observed THz transient also favor the ISHE over the anomalous Nernst effect (ANE). The M(T) variation governs the temperature dependence of the THz generation. Emitters with weakly remanent ferromagnets are magnetic-field tunable, while moderately and strongly remanent ferromagnets, once magnetized, allow intense THz generation even without an external field, nevertheless exhibiting low susceptibility to magnetic perturbations if the hysteresis loop is square. Hence, exploiting the magnetic properties of the ferromagnetic layer enables tailoring of weakly temperature-dependent spintronic THz emitters. Finally, we explored the applicability of perovskite oxide materials such as La-Sr-Mn-O (LSMO) for THz transient generation. We detected weak (<40-μV amplitude) THz emissions from both LSMO/Au and pure LSMO nanostructures with no sign flip upon the sample reversal. Furthermore, we excluded the ISHE and believe it was likely governed by the ANE in the thick-film regime, although we cannot exclude the transient demagnetization mechanism.

36 MATERIALS SCIENCE↗

Structural elucidation, and morphological and magnetic behavior evaluations, of low-temperature sintered, Ce-doped, nanostructured garnet ferrites

Highlights: • Ce{sub x}Gd{sub 3.5-x}Fe{sub 4.5}O{sub 12} were synthesized via sol gel self-combustion route. • Crystallite size was found in the range of 20–38 nm. • Morphology of Ce-Gd doped and undoped garnets were observed systematically. • Switching field distribution was calculated for further applications of the nanoferrites. • These garnets also have potential applications in microwave high frequency devices. - Abstract: Low-temperature sintered Ce{sub x}Gd{sub 3.5-x}Fe{sub 4.5}O{sub 12} (x = 0.0, 0.4, 0.8, 1.2, 1.6, 2.0 and 2.4) garnet ferrites were synthesized via a sol-gel self-combustion route. Phase, structure, morphology and magnetic investigations were done using FTIR, XRD, FESEM, and VSM, respectively. Single-phase structures of all Ce{sup 3+} substituted nano-sized garnet ferrites were confirmed through XRD. The crystallite size was decreased with Ce{sup 3+}incorporation. Relevant structural parameters such as site radii, bond lengths, ionic radii, and shared edges were calculated using XRD. The vibrational spectroscopy stretching band studies were also done using FTIR. The grain size and morphology were also analyzed using FESEM. The magnetic remanance, saturation, and coercivity were found to increase systematically with an increase in Ce{sup 3+} concentration in these garnets. Switching field distribution curves were also plotted using the first derivative of the demagnetization data from MH loops. The better magnetic properties of these nanogarnets suggest their use for miniaturization of the devices in various applications.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

A Novel $In-Situ$ Radiation Damage Diagnostic System for Undulators

Radiation damage has been a known problem at many synchrotron radiations and free-electron lasers facilities, especially those that use hybrid or pure permanent magnet undulators to produce high brightness light. Field strength loss due to demagnetization makes it necessary to remove the insertion device from the tunnel for inspection and repair, which brings several inconveniences. We aimed to develop an in situ radiation damage detection system for undulators capable of diagnosing relative field changes of 10 -4 (100 ppm) or smaller. The system measures the flux change in a flexible printed circuit board coil attached to the undulator magnet array by periodically measuring the integral flux change during the opening and closing of the undulator gap. If the magnet block damage occurs, the signal from the coil will decrease proportionally to the damage. First tests performed on variable gap hybrid undulators for the Linac Coherent Light Source II (LCLS-II) at SLAC National Accelerator Laboratory showed that the system is capable of measuring flux changes with a relative precision of approximately 0.7 × 10 -4 over several days. Relative field changes smaller than 10 -4 were detected in short-term measurements. Here, the novel system that we propose here opens the possibility of detecting radiation damage in undulators during operation.

47 OTHER INSTRUMENTATION↗

Unusual Behavior of the Coercive Field in a (CoFeB){sub x}(LiNbO{sub y}){sub 100 –x} Nanocomposite with a High Content of Magnetic Ions in an Insulating Matrix

The temperature behavior of the coercive field H{sub c}(T) and the magnetic anisotropy in (CoFeB){sub x}(LiNbO{sub y}){sub 100 –x} nanocomposite films with a ferromagnetic alloy content x = 33–48 at % near the metal–insulator transition (x{sub c} ≈ 42 at %) have been studied by the magnetometry and ferromagnetic resonance methods. The films were ensembles of CoFe granules with lateral sizes of 2–4 nm, which are highly elongated (up to 10–15 nm) in the nanocomposite growth direction and embedded in a LiNbO{sub y} matrix with a high content of magnetic Fe{sup 2+} and Co{sup 2+} ions (up to 3 × 10{sup 22} cm{sup –3}). A nonmonotonic behavior of H{sub c}(T), viz., a sharp minimum at a temperature T{sub F} ≈ 50 K close to the blocking temperature (T{sub b}{sup ∗} ≈ 70 K) of the granule magnetic moment, has been detected in samples with x < 42 at %. The effective field of the perpendicular growth anisotropy (0.4–0.8 kOe) turns out to be an order of magnitude lower than the field of the granule shape anisotropy (about 7 kOe) and increases with x. The revealed peculiarities are explained by the fact that, apart from the ferromagnetic intergranular exchange interaction in an infinite cluster, the surface anisotropy effects involving magnetic ions in a thin layer adjacent to the cluster and responsible for the surface interaction fluctuations play a big role in the investigated percolation nanocomposites, enhancing the nanocomposite demagnetization at T ≈ T{sub F} ~ T{sub b}{sup ∗}.

36 MATERIALS SCIENCE↗

Performance Testing of the Astro-H Flight Model 3-Stage ADR

The Soft X-ray Spectrometer (SXS) is one of four instruments that will be flown on the Japanese Astro-H satellite, planned for launch in late 2015early 2016. The SXS will perform imaging spectroscopy in the soft x-ray band using a 6x6 array of silicon micro calorimeters operated at 50 mK, cooled by an adiabatic demagnetization refrigerator (ADR). NASAGSFC is providing the detector array and ADR, and Sumitomo Heavy Industries, Inc. is providing the remainder of the cryogenic system (superfluid helium dewar (1.3 K), Stirling cryocoolers and a 4.5 K Joule-Thomson (JT) cryocooler). The ADR is unique in that it is designed to use both the liquid helium and the JT cryocooler as it heat sink. The flight detector and ADR assembly have successfully undergone vibration and performance testing at GSFC, and have now undergone initial performance testing with the flight dewar at Sumitomo Heavy Industries, Inc. in Japan. This presentation summarizes the performance of the flight ADR in both cryogen-based and cryogen-free operating modes.

adiabatic demagnetization refrigerator↗

Optimization Strategies for Single-Stage, Multi-Stage and Continuous ADRs

Adiabatic Demagnetization Refrigerators (ADR) have many advantages that are prompting a resurgence in their use in spaceflight and laboratory applications. They are solid-state coolers capable of very high efficiency and very wide operating range. However, their low energy storage density translates to larger mass for a given cooling capacity than is possible with other refrigeration techniques. The interplay between refrigerant mass and other parameters such as magnetic field and heat transfer points in multi-stage ADRs gives rise to a wide parameter space for optimization. This paper first presents optimization strategies for single ADR stages, focusing primarily on obtaining the largest cooling capacity per stage mass, then discusses the optimization of multi-stage and continuous ADRs in the context of the coordinated heat transfer that must occur between stages. The goal for the latter is usually to obtain the largest cooling power per mass or volume, but there can also be many secondary objectives, such as limiting instantaneous heat rejection rates and producing intermediate temperatures for cooling of other instrument components.

sub-kelvin cooling↗