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At least 145 records · Page 8
All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

Calibrating the SPECTACULAR constitutive model using legacy Sandia data for two filled epoxy systems: 828/CTBN/DEA/GMB and 828/DEA/GMB

The SPECTACULAR model is a development extension of the Simplified Potential Energy Clock (SPEC) model. Both models are nonlinear viscoelastic constitutive models used to predict a wide range of time-dependent behaviors in epoxies and other glass-forming materials. This report documents the procedures used to generate SPECTACULAR calibrations for two particulate-filled epoxy systems, 828/CTBN/DEA/GMB and 828/DEA/GMB. No previous SPECTACULAR or SPEC calibration exists for 828/CTBN/DEA/GMB, while a legacy SPEC calibration exists for 828/DEA/GMB. To generate the SPECTACULAR calibrations, a step-by-step procedure was executed to determine parameters in groups with minimal coupling between parameter groups. This procedure has often been deployed to calibrate SPEC, therefore the resulting SPECTACULAR calibration is backwards compatible with SPEC (i.e. none of the extensions specific to SPECTACULAR are used). The calibration procedure used legacy Sandia experimental data stored on the Polymer Properties Database website. The experiments used for calibration included shear master curves, isofrequency temperature sweeps under oscillatory shear, the bulk modulus at room temperature, the thermal strain during a temperature sweep, and compression through yield at multiple temperatures below the glass transition temperature. Overall, the calibrated models fit the experimental data remarkably well. However, the glassy shear modulus varies depending on the experiment used to calibrate it. For instance, the shear master curve, isofrequency temperature sweep under oscillatory shear, and the Young's modulus in glassy compression yield values for the glassy shear modulus at the reference temperature that vary by as much as 15 %. Also, for 828/CTBN/DEA/GMB, the temperature dependence of the glassy shear modulus when fit to the Young's modulus at different temperatures is approximately four times larger than when it is determined from the isofrequency temperature sweep under oscillatory shear. For 828/DEA/GMB, the temperature dependence of the shear modulus determined from the isofrequency temperature sweep under oscillatory shear accurately predicts the Young's modulus at different temperatures. When choosing values for the shear modulus, fitting the glassy compression data was prioritized. The new and legacy calibrations for 828/DEA/GMB are similar and appear to have been calibrated from the same data. However, the new calibration improves the fit to the thermal strain data. In addition to the standard calibrations, development calibrations were produced that take advantage of development features of SPECTACULAR , including an updated equilibrium Helmholtz free energy that eliminates undesirable behavior found in previous work. In addition to the previously mentioned experimental data, the development calibrations require data for the heat capacity during a stress-free temperature sweep to calibrate thermal terms.

36 MATERIALS SCIENCE↗
NASA NTRS2007

High-Temperature Characterization of Alumina Substrates and Folded Slot Antenna

The characterization of 99.6% polycrystalline alumina substrates and folded slot antennas is presented in this paper. Coplanar Waveguide (CPW) calibration standards where fabricated on 99.6% polycrystalline alumina substrates. Thru-Reflect-Line (TRL) calibrations were performed at temperatures of 25 to 400 C over a frequency range from 0.5 to 50 GHz. The effective dielectric constant of the alumina substrates was determined to be relatively constant at 5.4 from 25 to 200 C and then increased steadily to approximately 6 at 400 C. The loss of the CPW lines increased as temperature and frequency increased as well noting that the increase in loss is even more profound as both the temperature and frequency increased simultaneously. A CPW fed folded slot antenna fabricated on the alumina substrates is also presented. The Return Loss (RL) of a CPW fed folded slot antenna exhibits a self impedance matching technique. The RL of the folded slot antenna at 25 C displays a resonance at 3.5 GHz and is approximately 16 dB in magnitude. At 300 C the resonance shifts down in frequency to approximately 3.3 dB and has roughly the same magnitude. However the loss of the antenna response also increases at this elevated temperature. This work is part of the initial stages of an effort at NASA Glenn research Center to develop wireless sensors for harsh environments. This work can reduce cost, space to house all the hard wired connections, and reduce the weight of the overall units such as aerospace engines and allow for the placement of the wireless sensors in the engine which are not possible with hard wired sensors.

Scardelletti, Maximilian C.↗
DOE OSTI2018

ANALYTICAL LABORATORY AT IDAHO NATIONAL LABORATORY COUNTING EQUIPMENT STANDARDIZATION AND QUALITY CONTROL IMPROVEMENT

The Analytical Laboratory at Idaho National Laboratory (INL) is a growing program with an emphasis on providing high quality results to customers, and an increasing focus on independent research. The Analytical Laboratory Counting Group has a number of capabilities: six gamma-ray counters, one gamma-ray sample changer, four gas flow proportional counter drawers, an auto-changing gas flow proportional counter, two liquid scintillation counters, and an alpha spectroscopy system. Other capabilities within the Analytical Laboratory include quadrupole inductively coupled plasma mass spectrometry (ICP-MS), high resolution ICP-MS, multi-collector ICP-MS, ICP atomic emission spectrometry (ICP-AES), gas mass spectrometry, thermal ionization mass spectrometry (TIMS), several glove boxes and fume hoods for sample preparation, and six interconnected hot cells for sample receipt and dissolution. In order to position the Analytical Laboratory as a world-class research institution, the Counting Group has recently begun making improvements to its analytical techniques, calibrations, standardization, and quality control procedures. A large part of this effort is to increase the level of documentation of instrument work. One project is to re-calibrate all of the gamma systems with newly purchased standards. One of the changes made in the purchase of the new standards was to lower the total activity so that the dead time of the calibration would more closely match the dead time of typical samples. Similarly, another planned project is to use new standards to re-calibration the gas flow proportional counters. Additional work has focused on testing and improving alpha spectroscopy sample preparation techniques. Plutonium separations have been tested to improve tracer recovery and to verify the separation technique in the presence of typical sample matrices. A final planned area of improvements has focused on liquid scintillation counting. One difficulty the Counting Group has encountered in liquid scintillation counting is an inflated gross alpha count relative to other analysis methods in the presence of high gross beta activity. Ideas include investigating the impact of choice of scintillation cocktail, as well as the effects of sample dilution.

38 RADIATION CHEMISTRY, RADIOCHEMISTRY, AND NUCLEA↗
NASA NTRS1969

Mossbauer vibration calibration systems evaluated

Mossbauer effect vibration calibrator measures the velocity of high frequency, low amplitude vibration at various velocity and frequency ranges. It contains a highly precise calibrations standard unit and a vibration measuring system and may be applied to ultrafine testing and calibrating prezoelectric shakers, and vibration transducers.

Hobbs, J. V.↗
DOE OSTI2021

Preliminary Calibration System Report for High-Temperature Irradiation-Resistant Thermocouples

An established calibration procedure is presented for the high-temperature irradiation-resistant thermocouple (HTIR-TC). Standard calibration curves for both an individual (i.e. case by case basis) and common calibrations is shown. The error limits within ±3 σ are ±1% for the individual calibrations and ±2% for the common calibration.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗
DOE OSTI2019

NGEE Arctic Leaf Spectral Absorptance, Utqiagvik (Barrow), Alaska, 2015-2016

Leaf level reflectance on each sample leaf was measured using a portable, full range (i.e. 0.35 to 2.5 microns) Spectra Vista Corporation (SVC) HR-1024i spectroradiometer, together with a leaf clip assembly with an internal, calibrated light source (SVC, Poughkeepsie, NY, USA). Each measurement was referenced against a LabSphere Spectralon (R) standard (LabSphere, Inc., North Sutton, NH, USA) to calculate leaf reflectance from the ratio of target and standard calibrated radiance measurements for each leaf. For each leaf, we collected two to five measurements over the leaf adaxial surface to calculate an average, depending on the leaf size and morphology. Spectral discontinuities in the detector overlap areas were corrected using the SVC instrument software prior to sample averaging and other quality control steps, as described previously (Serbin et al., 2014) using the R-FieldSpectra package (https://github.com/serbinsh/R-FieldSpectra). Refer to Serbin et al (2017) for the complete spectral reflectance dataset. We then calculated leaf spectral absorptance using the measured leaf reflectance following the approach of Wu et al., (2018), based on the original method derived by Shiklomanov et al., (2016) using the PEcAnRTM package (https://github.com/PecanProject/pecan/tree/develop/modules/rtm). This dataset contains one xlsx file, one csv file, and one pdf file.The Next-Generation Ecosystem Experiments: Arctic (NGEE Arctic), was a research effort to reduce uncertainty in Earth System Models by developing a predictive understanding of carbon-rich Arctic ecosystems and feedbacks to climate. NGEE Arctic was supported by the Department of Energy's Office of Biological and Environmental Research.The NGEE Arctic project had two field research sites: 1) located within the Arctic polygonal tundra coastal region on the Barrow Environmental Observatory (BEO) and the North Slope near Utqiagvik (Barrow), Alaska and 2) multiple areas on the discontinuous permafrost region of the Seward Peninsula north of Nome, Alaska.Through observations, experiments, and synthesis with existing datasets, NGEE Arctic provided an enhanced knowledge base for multi-scale modeling and contributed to improved process representation at global pan-Arctic scales within the Department of Energy's Earth system Model (the Energy Exascale Earth System Model, or E3SM), and specifically within the E3SM Land Model component (ELM).

54 ENVIRONMENTAL SCIENCES↗
NASA NTRS1989

DSN 70-meter antenna microwave optics design and performance improvements. Part 2: Comparison with measurements

The measured Deep Space Network (DSN) 70-meter antenna performance at S- and X-bands is compared with the design expectations. A discussion of natural radio-source calibration standards is given. New estimates of DSN 64-meter antenna performance are given, based on improved values of calibration source flux and size correction. A comparison of the 64- and 70-meter performances shows that average S-band peak gain improvement is 1.94 dB, compared with a design expectation of 1.77 dB. At X-band, the average peak gain improvement is 2.12 dB, compared with the (coincidentally similar) design expectation of 1.77 dB. The average measured 70-meter S-band peak gain exceeds the nominal design-expected gain by 0.02 dB; the average measured 70-meter X-band peak gain is 0.14 dB below the nominal design-expected gain.

Bathker, D. A.↗
NASA NTRS1992

Radiometric calibration and monitoring of NOAA AVHRR data for ISCCP

The methodology developed to monitor the radiometric calibration of NOAA AVHRR data and to normalize succeeding polar orbiters for the International Satellite Cloud Project (ISCCP) is described. Results are given for NOAA-7, -8, and -9 Channel 1 (visible) data. The successful normalization of NOAA-8, and -9, to NOAA-7 permits the ISCCP calibration standard to be maintained over time. A correction for the degradation of NOAA-9 data and an absolute calibration for the entire ISCCP dataset are presented.

Brest, Christopher L.↗
NASA NTRS1993

FTIR quantification of industrial hydraulic fluids in perchloroethylene

The purpose of this summer research project was to investigate whether perchloroethylene can be used as a solvent for the quantitative analysis of industrial hydraulic fluids by infrared spectroscopy employing Beer's law. Standard calibration curves using carbon-hydrogen stretching (generic) and ester absorption peaks were prepared for a series of standard dilutions at low ppm levels of concentration of seven hydraulic fluids in perchloroethylene. The absorbance spectras were recorded with 1.5-10 mm fixed and variable path length sample cells made of potassium bromide. The results indicate that using ester infrared spectral peak, it is possible to detect about 20 ppm of the hydraulic fluid in perchloroethylene.

Mehta, Narinder K.↗
NASA NTRS1979

Millimeter wavelength spectroscopy and continuum studies of the planets

Careful observations were made at 86.1 GHz to derive the absolute brightness temperatures of the Sun (7914 + or - 192 K), Venus (357.5 + or - 13.1 K), Jupiter (179.4 + or - 4.7K), and Saturn (153.4 + or - 4.8 K) with a standard error of about 3%. This is a significant improvement in accuracy over previous results. A stable transmitter and novel superheterodyne receiver were constructed and used to determine the effective collecting area of the MWO 4.9 m antenna relative to a previously calibrated standard gain horn. The thermal scale was set by calibrating the radiometer with carefully constructed and tested hot and cold loads. The brightness temperatures may be used to establish an absolute calibration scale and to determine the antenna aperture and beam efficiencies of other radio telescopes at 3.5 mm wavelength.

Vandenbout, P. A.↗
DOE OSTI2025

Thermal expansion of LaB 6 from 298 to 998 K

We propose LaB 6 as a temperature calibration standard for high-temperature (HT) X-ray diffractometry owing to its high temperature stability. Such HT applications require a reliable HT lattice parameter or, equivalently, peak position data, which have not been readily accessible to the diffraction community to date. As such, the thermal expansion behavior of NIST SRM 660a LaB6 was assessed in the temperature range 298–998 K using HT Bragg–Brentano parafocusing θ:θ X-ray diffractometry in conjunction with Rietveld analysis. Data were collected in the 2θ range 20–150° at a data collection rate of 0.5° θ min −1 in air and at 1 atm. The temperature was stepped in 50 K increments. The cubic unit-cell lattice parameter [a(T)] of LaB 6 in Å was found to vary as a(T) = 4.15678 (±0.00001) + Ξ(T − 298 K) + Ψ(T − 298 K) 2 , where Ξ = 2.4645 × 10 −5 (±4.8904 × 10 −8 ) Å K −1 and Ψ = 1.0325 × 10 −8 (±6.7376 × 10 −11 ) Å K −1 . The isobaric volume thermal expansion coefficient (TEC) was obtained as α V P = (5.9291 × 10 −6 ) + (4.9680 × 10 −9 )(T − 298 K) K −1 , from which the corresponding linear TEC was obtained as α L P = (1.9764 × 10 −6 ) + (1.6560 × 10 −9 )(T − 298 K) K −1 . The 3 × 3 matrix representations of the single-crystal isobaric linear TEC and the volume expansivity were obtained for the cubic crystal class to which LaB 6 belongs. Also, the temperature dependence of the lattice parameter data of this study was compared with past landmark studies on LaB 6 by Dutchak et al. [Inorg. Mater. (1972), 8, 1877–1880] and Aivazov et al. [Inorg. Mater. (1979), 15, 1015–1016].

LaB6 standard material↗
NASA NTRS2004

Innovative Technology Transfer Partnerships

The National Aeronautics and Space Administration (NASA) seeks to license its Advanced Tire and Strut Pressure Monitor (TSPM) technology. The TSPM is a handheld system to accurately measure tire and strut pressure and temperature over a wide temperature range (20 to 120 OF), as well as improve personnel safety. Sensor accuracy, electronics design, and a simple user interface allow operators quick, easy access to required measurements. The handheld electronics, powered by 12-VAC or by 9-VDC batteries, provide the user with an easy-to-read visual display of pressure/temperature or the streaming of pressure/temperature data via an RS-232 interface. When connected to a laptop computer, this new measurement system can provide users with automated data recording and trending, eliminating the chance for data hand-recording errors. In addition, calibration software allows for calibration data to be automatically utilized for the generation of new data conversion equations, simplifying the calibration processes that are so critical to reliable measurements. The design places a high-accuracy pressure sensor (also used as a temperature sensor) as close to the tire or strut measurement location as possible, allowing the user to make accurate measurements rapidly, minimizing the amount of high-pressure volumes, and allowing reasonable distance between the tire or strut and the operator. The pressure sensor attaches directly to the pressure supply/relief valve on the tire and/or strut, with necessary electronics contained in the handheld enclosure. A software algorithm ensures high accuracy of the device over the wide temperature range. Using the pressure sensor as a temperature sensor permits measurement of the actual temperature of the pressurized gas. This device can be adapted to create a portable calibration standard that does not require thermal conditioning. This allows accurate pressure measurements without disturbing the gas temperature. In-place calibration can save considerable time and money and is suitable in many process applications throughout industry.

Kohler, Jeff↗
NASA NTRS2018

A Quick Summary of IMERG Versions and Features

This talk will summarize the shifts in IMERG (Integrated Multi-satellitE Retrievals for GPM (Global Precipitation Measurement)) from Version 03 to 04 in early Spring 2016, and to Version 05 in late Summer 2017. For example, Version 04 replaced approximate pre-launch calibrations with GPM Core Observatory-based calibrations, while Version 05 introduced improved estimates for the primary GPM instrument products (DPR, GMI, and Combined Instrument). In Version 04 the IR estimates were routinely calibrated to the passive microwave estimates. As analysis showed that the Combined Instrument estimates (the IMERG calibration standard) tend to be biased high over land and low over ocean at higher latitudes, in Version 04 we climatologically calibrated IMERG to the Global Precipitation Climatology Project (GPCP) monthly Satellite-Gauge product, except in low- and mid-latitude ocean regions. This calibration leaves the relative time series intact, and only adjusts the mean of the entire series. In Version 05 the primary GPM instrument products have reduced biases, but calibration to GPCP continues to be necessary to achieve the most realistic estimates. Finally, retrospective processing back into the TRMM (Tropical Rainfall Measuring Mission) era is expected in early 2018, after which the legacy TMPA (TRMM Multi-satellite Precipitation Analysis) dataset will be retired.

Huffman, George J.↗
NASA NTRS2004

Analysis of He I 1083 nm Imaging Spectroscopy Using a Spectral Standard

We develop a technique. for the analysis of He I 1083 nanometer spectra which addresses several difficulties through determination of a continuum background by comparison with a well calibrated standard and through removal of nearby solar and telluric blends by differential comparison to an average spectrum. The method is compared with earlier analysis of imaging spectroscopy obtained at the National Solar Observatory/Kitt Peak Vacuum Telescope (NSO/KPVT) with the NASA/NSO Spectromagnetograph (SPM). We examine distributions of Doppler velocity and line width as a function of central intensity for an active region, filament, quiet Sun, and coronal hole. For our example, we find that line widths and central intensity are oppositely correlated in a coronal hole and quiet Sun. Line widths are comparable to the quiet sun in the active region, are systematically lower in the filament, and extend to higher values in the coronal hole. Outward velocities of approximately equal to 2 to 4 kilometers per second are typically observed in the coronal hole. The sensitivity of these results to analysis technique is discussed.

Malanushenko, Elena V.↗
NASA NTRS1980

Absolute brightness temperature measurements at 3.5-mm wavelength

Careful observations have been made at 86.1 GHz to derive the absolute brightness temperatures of the sun (7914 + or - 192 K), Venus (357.5 + or - 13.1 K), Jupiter (179.4 + or - 4.7 K), and Saturn (153.4 + or - 4.8 K) with a standard error of about three percent. This is a significant improvement in accuracy over previous results at millimeter wavelengths. A stable transmitter and novel superheterodyne receiver were constructed and used to determine the effective collecting area of the Millimeter Wave Observatory (MWO) 4.9-m antenna relative to a previously calibrated standard gain horn. The thermal scale was set by calibrating the radiometer with carefully constructed and tested hot and cold loads. The brightness temperatures may be used to establish an absolute calibration scale and to determine the antenna aperture and beam efficiencies of other radio telescopes at 3.5-mm wavelength.

Ulich, B. L.↗
DOE OSTI2022

Computer Model Calibration with Time Series Data Using Deep Learning and Quantile Regression

Computer models play a key role in many scientific and engineering problems. One major source of uncertainty in computer model experiments is input parameter uncertainty. Computer model calibration is a formal statistical procedure to infer input parameters by combining information from model runs and observational data. The existing standard calibration framework suffers from inferential issues when the model output and observational data are high-dimensional dependent data, such as large time series, due to the difficulty in building an emulator and the nonidentifiability between effects from input parameters and data-model discrepancy. To overcome these challenges, we, in this work, propose a new calibration framework based on a deep neural network (DNN) with long short-term memory layers that directly emulates the inverse relationship between the model output and input parameters. Adopting the “learning with noise” idea, we train our DNN model to filter out the effects from data-model discrepancy on input parameter inference. We also formulate a new way to construct interval predictions for DNN using quantile regression to quantify the uncertainty in input parameter estimates. Through a simulation study and real data application with the Weather Research and Forecasting Model Hydrological modeling system (WRF-Hydro), we show our approach can yield accurate point estimates and well-calibrated interval estimates for input parameters.

97 MATHEMATICS AND COMPUTING↗
NASA NTRS2011

Preliminary Error Budget for the Reflected Solar Instrument for the Climate Absolute Radiance and Refractivity Observatory

The Climate Absolute Radiance and Refractivity Observatory (CLARREO) plans to observe climate change trends over decadal time scales to determine the accuracy of climate projections. The project relies on spaceborne earth observations of SI-traceable variables sensitive to key decadal change parameters. The mission includes a reflected solar instrument retrieving at-sensor reflectance over the 320 to 2300 nm spectral range with 500-m spatial resolution and 100-km swath. Reflectance is obtained from the ratio of measurements of the earth s surface to those while viewing the sun relying on a calibration approach that retrieves reflectance with uncertainties less than 0.3%. The calibration is predicated on heritage hardware, reduction of sensor complexity, adherence to detector-based calibration standards, and an ability to simulate in the laboratory on-orbit sources in both size and brightness to provide the basis of a transfer to orbit of the laboratory calibration including a link to absolute solar irradiance measurements. The Climate Absolute Radiance and Refractivity Observatory (CLARREO) mission addresses the need to observe high-accuracy, long-term climate change trends and to use decadal change observations as the most critical method to determine the accuracy of climate change projections such as those in the IPCC Report. A rigorously known accuracy of both decadal change observations as well as climate projections is critical in order to enable sound policy decisions. The CLARREO Project will implement a spaceborne earth observation mission designed to provide rigorous SI traceable observations (i.e., radiance, reflectance, and refractivity) that are sensitive to a wide range of key decadal change variables, including: 1) Surface temperature and atmospheric temperature profile 2) Atmospheric water vapor profile 3) Far infrared water vapor greenhouse 4) Aerosol properties and anthropogenic aerosol direct radiative forcing 5) Total and spectral solar irradiance 6) Broadband reflected and emitted radiative fluxes 7) Cloud properties 8) Surface albedo There are two methods the CLARREO mission will rely on to achieve these critical decadal change benchmarks: direct and reference inter-calibration. A quantitative analysis of the strengths and weaknesses of the two methods has led to the recommended CLARREO mission approach. The project consists of two satellites launched into 90-degree, precessing orbits separated by 90 degrees. The instrument suite receiver on each spacecraft includes one emitted infrared spectrometer, two reflected solar spectrometers: dividing the spectrum from ultraviolet through near infrared, and one global navigation receiver for radio occultation. The measurements will be acquired for a period of three years minimum, with a five-year lifetime goal, enabling follow-on missions to extend the climate record over the decades needed to understand climate change. The current work concentrates on the reflected solar instrument giving an overview of its design and calibration approach. The calibration description includes the approach to achieving an SI-traceable system on orbit. The calibration overview is followed by a preliminary error budget based on techniques currently in place at the National Institute of Standards and Technology (NIST).

Thome, Kurtis↗