Engineering Papers⌕ Search

SEARCH · Engineering Papers

Results for “prepare”

Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.

At least 1,423 records · Page 79

An improved rocket ozonesonde (ROCOZ-A). II - Preparation of stratospheric ozone profiles

The ROCOZ-A radiometer measures ozone by long pathlength photometry in the stratosphere and lower mesosphere. After a rocket launch to an apogee of 70 km, the instrument measures the solar ultraviolet irradiance over its four filter wavelengths as it descends on a parachute. The fundamental values from ROCOZ-A are ozone overburdens versus radar altitude from 53 to 20 km. The slope of these values gives ozone number density. At one standard deviation the repeatability of the ozone overburden measurements averages 2.4 percent. For ozone number density the repeatability averages 3.2 percent with a significant increase at altitudes below the ozone number density maximum. The accuracy limits for overburden and number density are estimated at 5-7 percent. With auxiliary measurements of pressure and temperature, ozone results are also produced in terms of ozone mixing ratio, albeit with a slight broadening of the estimated accuracy limits. The vertical response of ROCOZ-A ozone measurements (full width at half maximum) is 4 km. The assembly of ROCOZ-A profiles can be used to compare with measurements from each of the current NASA and NOAA satellite ozone instruments. In addition, the repeatability of ROCOZ-A allows the use of this instrument as a transfer standard between satellite instruments with different fundamental ozone measurements.

Barnes, Robert A.↗

Changes in pituitary growth hormone cells prepared from rats flown on Spacelab 3

The effect of exposure to microgravity on pituitary gland was investigated by examining cells isolated from anterior pituitaries of rats flown on the 7-day Spacelab 3 mission and, subsequently, cultured for 6 days. Compared with ground controls, flight cells contained more intracellular growth hormone (GH); however, the flight cells released less GH over the 6-day culture period and after implantation into hypophysectomized rats than did the control cells. Compared with control rats, glands from large rats (400 g) contained more somatotrophs (44 percent compared with 37 percent in control rats); small rats (200 g) showed no difference. No major differences were found in the somatotroph ultrastructure (by TEM) or in the pattern of the immunoactive GH variants. However, high-performance liquid chromatography fractionation of culture media indicated that flight cells released much less of a biologically active high-molecular weight GH variant, suggesting that space flight may lead to secretory dysfunction.

Grindeland, R.↗

Preparative electrophoresis for space

A premise of continuous flow electrophoresis is that removal of buoyancy-induced thermal convection caused by axial and lateral temperature gradients results in ideal performance of these instruments in space. Although these gravity dependent phenomena disturb the rectilinear flow in the separation chamber when high voltage gradients or thick chambers are used, distortion of the injected sample stream due to electrohydrodynamic effects cause major broadening of the separated bands. The electrophoresis separation process is simple, however flow local to the sample filament produced by the applied electric field have not been considered. These electrohydrodynamic flows distort the sample stream and limit the separation. Also, electroosmosis and viscous flow combine to further distort the process. A moving wall concept is being proposed for space which will eliminate and control the disturbances. The moving wall entrains the fluid to move as a rigid body and produces a constant residence time for all samples distributed across the chamber thickness. The moving wall electrophoresis chamber can only be operated in space because there is no viscous flow in the chamber to stabilize against thermal convection.

Rhodes, Percy H.↗

Materials preparation and longevity in hyperthermal atomic oxygen

Flight hardware fabrication, the design and fabrication of an atom beam source, construction of a surface science laboratory, and progress in research on processes and mechanisms of interaction of hyperthermal atoms at solid surfaces are discussed.

Bareiss, Lyle E.↗

Guidelines for preparing software user documentation

Clear, easy-to-use software user's manuals make strong demands on special technical communication techniques. Principles and guidelines are given for analyzing the audience and dealing with wide-ranging backgrounds of potential users. Types of information to be included in a complete manual are suggested, with a technique for creating a user-oriented rather than process-oriented organization. Accuracy verification is emphasized. Simple tips are gievn for formatting for quick comprehension and reference, for deciding on packaging, for creating helpful illustrations and examples, and for setting up clear and consistent conventions. Simple guidelines are offered for writing clearly and concisely and for editing.

Miller, Diane F.↗

McDonnell Douglas Helicopter Company independent research and development: Preparing for the future

During the 1970's and 80's, research has produced the technology that is seen in aircraft such as the LHX and future models. The technology is discussed that is reaching maturity and moving into the application stage of future programs. Technology is discussed in six major areas: advanced concepts, analysis techniques, structures, systems, simulation, and research and development facilities. The partnership of McDonnell Douglas Helicopter Co. and the government in developing these technologies is illustrated in several programs.

Haggerty, Allen C.↗

Preparing for the future

Technologies and programs related to the development, construction, and operation of the Space Station are examined. A phase approach has been chosen for the construction of the Space Station, which is to have a revised baseline configuration. Consideration is given to the use of automation on the Space Station; the assembly and servicing of the Station; user requirements; and Space Station operations. The benefits the Space Station will provide to space exploration are discussed.

Stofan, Andrew J.↗

Recycling isotachophoresis - A novel approach to preparative protein fractionation

The concept of automated recycling isotachophoresis (RITP) as a purification methodology is discussed, in addition to a description of the apparatus. In the present automated RITP, the computer system follows the achievement of steady state using arrays of universal and specific sensors, monitors the position of the front edge of the zone structure, activates the counterflow if the leading boundary passes a specified position along the separation axis, or changes the applied current, accordingly. The system demonstrates high resolution, in addition to higher processing rates than are possible in zone electrophoresis or isoelectric focusing.

Sloan, Jeffrey E.↗

A simple device for the preparation of embedded materials science specimens for ultramicrotomy

A simple hand-held grinding fixture is discussed which can produce microtome mounts of hard materials, oriented interfaces, and powders embedded in a 5/16-in plastic rod. The device has been used for the ultramicrotomy of meteorite samples, 10-50 micron interplanetary dust particles, and thin films on plastic. Results are presented for a layer lattice silicate from the Murchison carbonaceous chondrite, illustrating the resolution and structural detail that can be obtained with the method.

Blake, D. F.↗

Preparing for the 90s using today's communications assets

Such existing NASA/U.S. facilities and spacecraft as those of the Deep Space Network, VLA, and Arecibo are presently judged capable, at modest additional investment during the next five years, to acquire unique space science data, to generate mission planning data for missions to be launched in the early 1990s, and to evaluate and demonstrate communications and navigation technology for missions of the late 1990s and beyond. The more ambitious of these efforts will contribute the continuation of space research attractiveness for students, as well as furnish an important part of their scientific training.

Posner, Edward C.↗

Poly(imide-siloxane) segmented copolymer structural adhesives prepared by bulk and solution thermal imidization

The improved properties that have been demonstrated through thermal solution imidization in the case of polyimides and poly(imide-siloxane) segmented copolymers suggests significant potential for application of these new materials. Specifically, the enhancement in solubility, moisture reduction, and processability observed through this solution technique is quite dramatic. Previous work has shown that the presence of low amounts of siloxane does not detract significantly from the lap shear strength of these materials to titanium in the case of bulk thermal imidization synthesis. In addition, the siloxane incorporation results in the added advantage of resistance to hot, wet environments. This added durability is presumably due to the hydrophobic siloxane segments preventing the uptake of water at the critical interphase between the adhesive and the adherend. This paper discusses the extension of this work to the solution imidization synthesis technique recently developed in our laboratory. Results dealing with the absolute bond strengths as well as durability and failure surface analysis will be presented.

Bott, R. H.↗

Preparation for microgravity - The role of the Microgravity Material Science Laboratory

Experiments at the NASA Lewis Research Center's Microgravity Material Science Laboratory using physical and mathematical models to delineate the effects of gravity on processes of scientific and commercial interest are discussed. Where possible, transparent model systems are used to visually track convection, settling, crystal growth, phase separation, agglomeration, vapor transport, diffusive flow, and polymer reactions. Materials studied include metals, alloys, salts, glasses, ceramics, and polymers. Specific technologies discussed include the General Purpose furnace used in the study of metals and crystal growth, the isothermal dendrite growth apparatus, the electromagnetic levitator/instrumented drop tube, the high temperature directional solidification furnace, the ceramics and polymer laboratories and the center's computing facilities.

Johnston, J. Christopher↗

Characterization of Ba2YCu3O(7-x) prepared in an inert atmosphere

Reaction data, X-ray data, and critical temperature measurements have been used to show that superconducting Ba2YCu3O(7-x) can be produced in an inert atmosphere using BaO2 as the barium source. Weight loss data are presented for samples produced in O2 and N2. The use of BaO2 is found to result in decreased levels of intergrain BaCO3. The necessity for total inert atmosphere handling and tighter control of the carbon content of starting materials is pointed out. It is shown that materials made with BaO2 and handled in inert atmospheres can be used to improve the J sub c of melt processed materials.

Hepp, A. F.↗

Comparison of sulfuric and oxalic acid anodizing for preparation of thermal control coatings for spacecraft

The development of thermal control surfaces, which maintain stable solar absorptivity and infrared emissivity over long periods, is challenging due to severe conditions in low-Earth orbit (LEO). Some candidate coatings are second-surface silver-coated Teflon; second-surface, silvered optical solar reflectors made of glass or quartz; and anodized aluminum. Sulfuric acid anodized and oxalic acid anodized aluminum was evaluated under simulated LEO conditions. Oxalic acid anodizing shows promise of greater stability in LEO over long missions, such as the 30 years planned for the Space Station. However, sulfuric acid anodizing shows lower solar absorptivity.

Le, Huong G.↗

Preparation of non-metals properties for data base

The development of non-metallic material properties data bases is discussed. The data bases consist of the non-metallic material classes of adhesives, adhesive/sealants, plastics, and elastomers. A specifications data base was also developed to incorporate material specifications data as a supplement to the Elastomers Data Base. Examples of the forms used are provided to show the properties of the materials which appear in the data base.

Source record↗

Preparative electrophoresis for space

A premise of continuous flow electrophoresis is that removal of buoyance-induced thermal convection caused by axial and lateral temperature gradients results in ideal performance of these instruments in space. Although these gravity dependent phenomena disturb the rectilinear flow in the separation chamber when high voltage gradients or thick chamber are used, distortion of the injected sample stream due to electrodynamic effects cause major broadening of the separated bands. The electrophoresis separation process is simple, however flow local to the sample filament produced by the applied electric field were not considered. These electrohydrodynamic flows distort the sample stream and limit the separation. Also, electroosmosis and viscous flow combine to further distort the process. A moving wall concept is being proposed for space which will eliminate and control the disturbances. The moving wall entrains the fluid to move as a rigid body and produces a constant residence time for all samples distributed across the chamber thickness. The moving wall electrophoresis chamber can only be operated in space because there is no viscous flow in the chamber to stabilize against thermal convection.

Rhodes, Percy H.↗

Preparation and evaluation of silicon nitride matrices for silicon nitride-SiC fiber composites

Continuous silicon carbide (SiC) fiber was added to three types of silicon nitride (Si3N4) matrices. Efforts were aimed at producing a dense Si3N4 matrix from reaction-bonded silicon nitride (RBSN) by hot-isostatic-pressing (HIP) and pressureless sintering, and from Si3N4 powder by hot-pressing. The sintering additives utilized were chosen to allow for densification, while not causing severe degradation of the fiber. The ceramic microstructures were evaluated using scanning optical microscopy. Vickers indentation was used to determine the microhardness and fracture toughness values of the matrices. The RBSN matrices in this study did not reach more than 80 percent of theoretical density after sintering at various temperatures, pressures, and additive levels. Hot-pressing Si3N4 powder produced the highest density matrices; hardness and toughness values were within an order of magnitude of the best literature values. The best sintering aid composition chosen included Y2O3, SiO2, and Al2O3 or AlN. Photomicrographs demonstrate a significant reduction of fiber attack by this additive composition.

Axelson, Scott R.↗

The preparation of new perfluoro ether fluids exhibiting excellent thermal-oxidative stabilities

A series of low molecular weight perfluoroalkyl ethers (PFAEs) were synthesized by direct fluorination. Viscosity-temperature properties and oxidation stabilities were determined. Viscosity-temperature correlations indicated that increases in branching and increases in the size of the branching substituent caused a deterioration in viscometric properties (i.e., an increase in ASTM slope). In addition, increasing the ratio of carbon to oxygen in these compounds also increased the ASTM slope. Preliminary oxidation stability measurements indicated that highly branched PFAE fluids (i.e., those containing quaternary carbons) may be less stable than either those containing a single trifluoromethyl pendant group or those containing no branching at all.

Jones, William R., Jr.↗