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At least 1,423 records · Page 79

Unique intermetallic compounds prepared by shock wave synthesis

Technique compresses fine ground metallic powder mixture beyond crystal fusion point. Absence of vapor pressure voids and elimination of incongruous effects permit application of technique to large scale fabrication of intermetallic compounds with specific characteristics, e.g., semiconduction, superconduction, or magnetic properties.

Otto, G.↗

Improved method for producing metal-reinforced ceramics

Vacuum impregnation process produces metal-reinforced ceramics with only 3 percent void space volumes. Method may be used to produce metal-reinforced ceramics for high temperature or structural applications such as furnace supports and armor.

Landingham, R. L.↗

Trace contaminant adsorption and sorbent regeneration in closed ecological systems

Correlation was obtained for determining sorptive capacity of carbon for pure and mixed contaminants under dry and humid conditions at various temperatures. Vacuum desorption rates were investigated for single particles and for sorbent beds. For sorbent beds, rate-determining step is Knudsen diffusion through interparticle voids.

Arnold, C. R.↗

Development of a highly reliable composite board for printed circuitry for use in space environment

Materials, processes and fabrication techniques have been investigated for the development of a high-temperature circuit-board laminate. High quality, void-free copper-clad laminates have been made using 7628/HS-1 style fiberglas reinforcements with filled polyimide matrices. The fabricating characteristics of P13N resin appear suitable for use as a filled matrix in this circuit board development. High-fired, ball-milled alumina appears to be necessary to obtain the desired effects in the circuit board system. Nickel-clad copper foil bonding surfaces appear to be another requirement for retention of good bond strengths after art work and plating sequences. The fabrication cycle for this circuit board system is very dependent on the heating profile. Very rapid heating with quick loading is recommended. A stack approach to lamination was successfully used.

Bradbury, E. J.↗

Methods of measurement for semiconductor materials, process control, and devices

The development of methods of measurement for semiconductor materials, process control, and devices is discussed. The following subjects are also presented: (1) demonstration of the high sensitivity of the infrared response technique by the identification of gold in a germanium diode, (2) verification that transient thermal response is significantly more sensitive to the presence of voids in die attachment than steady-state thermal resistance, and (3) development of equipment for determining susceptibility of transistors to hot spot formation by the current-gain technique.

Bullis, W. M.↗

Resin/graphite fiber composites

High temperature resin matrices suitable for use in advanced graphite fiber composites for jet engine applications were evaluated. A series of planned, sequential screening experiments with resin systems in composite form were performed to reduce the number of candidates to a single A-type polyimide resin that repetitively produced void-free, high strength and modulus composites acceptable for use in the 550 F range for 1000 hours. An optimized processing procedure was established for this system. Extensive mechanical property studies characterized this single system, at room temperature, 500 F, 550 F and 600 F, for various exposure times.

Cavano, P. J.↗

Study of critical defects in ablative heat shield systems for the space shuttle

Results are presented from an investigation to determine the effects of fabrication-induced defects on the performance of an ablative heat shield material in a simulated space shuttle reentry environment. Nondestructive methods for detecting the defects were investigated. The material considered is a fiber-filled, honeycomb-reinforced, low-density elastomer. Results were obtained for density variations, voids, fiber bundles, crushed honeycomb, undercut honeycomb, unbonded areas, face sheet delaminations, and cure variations. The data indicate that, within reasonable tolerances, the fabrication defects investigated are not critical in terms of reentry performance of the heat shield.

Thompson, R. L.↗

Development of nondestructive testing techniques for plated-through holes in multilayer printed circuit boards

The development of a nondestructive test with the capability to interrogate plated-through holes as small as 0.51 millimeters inside diameter is discussed. The system can detect defects such as holes, voids, cracks, and thin spots that reduce the current carrying capability of plates-through interconnects by 20 percent or more. Efforts were directed toward the design and fabrication of magnetic circuitry mutual coupling probes and to evaluate the effectiveness of these devices for detecting in multilayer board plated-through holes.

Anthony, P. L.↗

The particles and fields subsatellite magnetometer experiment

A preliminary analysis of magnetometer data from Apollo 15 subsatellite is concluded. Remanent magnetization is a characteristic property of the moon, and the distribution is such that a complex pattern is produced. A mapping of the distribution is feasible with the present experiment. Lunar induction fields produced by transients in interplanetary magnetic field are detectable at satellite orbit. Magnetometer data will provide estimates of the latitude and longitude dependences of interior conductivity. The plasma void extends to some altitude below the satellite orbit and probably the lunar surface. Solar wind near the limbs is usually strongly disturbed.

Coleman, P. J., Jr.↗

Results of a preliminary experimental investigation of a vapor transport fuel pin

In-Pile experimental tests were conducted on two fuel pins mounted side-by-side in a holder assembly. The fuel pins consisted of stacked fully enriched UO2 pellets enclosed in a type 316 stainless steel clad 1/2 inch outside diameter and 3 inches in length. Each fuel pin contained four pellets for a total of 22 grams of fuel weight. The experiment was operated to maintain the maximum clad temperature at 395 K corresponding to a fuel temperature at the central void surface of 2350 K. Total primary coolant water flow past the pin holder was calculated to be 110 gallons per minute. Forty-four gallons per minute at a velocity of 36.5 feet per second flowed around each fuel pin. Calculations indicated the maximum heat flux was at the point of the highest temperature and was equal to 0.24 kW/sq cm or 7.62 Btu/hr sq ft. A series of high resolution neutron radiographs of the nuclear fueled vapor transport capsule was taken. The thermal neutrons emitted from the core of the 60 megawatt Plum Brook reactor facility were used.

Lanzo, C. D.↗

A systems approach of the nondestructive evaluation techniques applied to Scout solid rocket motors.

Review and appraisal of the status of the nondestructive tests applied to Scout solid-propellant rocket motors, using analytical techniques to evaluate radiography for detecting internal discontinuities such as voids and unbonds. Information relating to selecting, performing, controlling, and evaluating the results of NDE tests was reduced to a common simplified format. With these data and the results of the analytical studies performed, it was possible to make the basic appraisals of the ability of a test to meet all pertinent acceptance criteria and, where necessary, provide suggestions to improve the situation.

Oaks, A. E.↗

Effect of angular quadrature on results of two-dimensional space power reactor shield calculations.

Study of the effect of angular quadrature on the results of two-dimensional transport calculations made to evaluate radiation environment in the vicinity of a shielded space power reactor. The application considered is for a manned space-station; crew shielding must be provided within a 25 deg cone angle. The asymmetric shield layout is evaluated using the two-dimensional transport code DOT. Within the shield, an S sub 6 angular quadrature yields satisfactory results. For regions where the ray effect may occur it is not apparent that an S sub 10 quadrature is adequate. Anomalies in results due to transport of particles in a void and necessary geometric approximations were observed.

Connolley, D. J.↗

Endolithic algae and micrite envelope formation in Bahamian oolites as revealed by scanning electron microscopy.

Examination of Holocene Bahamian ooelites by scanning electron and light microscopy has revealed the morphology and orientation of aragonite crystals in the lamellar ooelitic envelope, and their modification by the boring activities of endolithic algae. The voids produced by these algae are found in progressive stages of being lined and filled with precipitated microcrystalline aragonite, which is similar to the process of micrite envelope formation in molluscan and other skeletal carbonate grains.

Margolis, S.↗

Benchmark gas core critical experiment.

A critical experiment with spherical symmetry has been conducted on the gas core nuclear reactor concept. The nonspherical perturbations in the experiment were evaluated experimentally and produce corrections to the observed eigenvalue of approximately 1% delta k. The reactor consisted of a low density, central uranium hexafluoride gaseous core, surrounded by an annulus of void or low density hydrocarbon, which in turn was surrounded with a 97-cm-thick heavy water reflector.

Kunze, J. F.↗