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At least 1,387 records · Page 77

Electrodynamic Dust Shield (EDS) Preparation for MISSE-11 Launch

The dusty surfaces of the Moon, Mars, and various asteroids present a significant challenge to NASA’s manned and unmanned space exploration efforts. The fine, electrostatically charged dust is difficult to remove and has resulted in vision obscuration, false instrument readings, contamination, elevated temperatures, performance reduction, and equipment failure. To alleviate these problems, NASA KSC’s Electrostatics and Surface Physics Laboratory (ESPL) is developing active dust mitigation systems for solar system exploration and in situ resource utilization (ISRU). Part of KSC’s Swamp Works system, the lab emphasizes fast-paced, hands-on, cost-effective, and collaborative innovation. The Electrodynamic Dust Shield (EDS) is an ESPL technology being developed to prevent dust accumulation on space components. It consists of a dielectric substrate embedded with parallel electrodes which, when applied with high voltage out-of-phase waveforms, produce a traveling electric field wave that scatters dust particles from its surface via dielectrophoretic and electrostatic forces. The EDS is currently fully functional and has been tested for scalability and endurance in reduced gravity/pressure flight. Next, it will be part of the May 2019 Materials International Space Station Experiment-11 (MISSE-11) payload, which will test small shield samples for performance durability with exposure to the harsh space environment. The summer objective was to test EDS functionality before active and passive dust shield samples launch on MISSE-11, in order to screen for good flight/control samples as well as to compare pre-flight and post-flight clearing efficiencies. I imaged glass and Kapton shields of 2-phase and 3-phase electrode configurations with the Keyence VHX-5000 digital microscope to check for damage before and after all testing for a qualitative pre-flight baseline; helped with vacuum testing of high-voltage shield breakdown; assembled shields and wires using Electrobond 004 silver epoxy; and helped with vacuum and cryogenic dust clearance testing of assembled EDS systems. I learned CAD (computer-aided design) and 3D printing skills to create parts for a shaker table/motor assembly, which will allow for repeatable experiments by evening out EDS dust distribution in a consistent manner prior to dust scattering testing. I will also be improving the interfacing with Alpha Space’s prototype Data Communications Unit (DCU), a payload component to control power to the EDS and store data, by mapping the DCU structure upon power-up and writing shell scripts to improve various processes. Finally, I also CADed and 3D-printed plastic supports for three different geometries of the Electrostatic Precipitator (ESP), a project that aims to use high voltage electrodes to charge and filter out dust from the Martian atmosphere drawn for ISRU devices. This work on dust mitigation technologies will help to support future robotic and human space exploration missions, including NASA’s Journey to Mars; the EDS has especially significant applications to spacecraft solar panels, thermal radiators, viewports, and astronaut visors. This opportunity has also allowed me to become more familiar with various lab equipment and hardware testing, develop key modeling skills in SolidWorks, explore past and present components critical to America’s space program, work with inspiring peers and mentors, and ascertain my dream of working permanently for NASA.

space↗

Empirical Validation of Building Energy Modeling using Flexible Research Platform

Recently, efforts have been made to provide reliable empirical data for ANSI/ASHRAE Standard 140, Standard Method of Test for the Evaluation of Building Energy Analysis Computer Programs, to enable improved accuracy of building energy model (BEM) engines and improved characterization of their accuracy. The motivation for this effort is that the use of reliable empirical validation data sets in the evaluation of building energy modeling tools will lead to more consistent and validated simulation engines across all software vendors. This would expedite the use of building energy modeling in designing new buildings and retrofitting existing buildings, which delivers more energy efficient buildings.As part of a three-year multi-lab empirical validation project sponsored by U.S. DOE, this research project generated cooling season test plans by reviewing ASHRAE Standard 140, and the tests were performed based on the test plan. Finally, the experimental data sets were compared with the EnergyPlus model to demonstrate the validation procedure.

Im, Piljae↗

Test Report : GS Battery, EPC power HES RESCU

The Department of Energy Office of Electricity (DOE/OE), Sandia National Laboratories (SNL) and the Base Camp Integration Lab (BCIL) partnered together to incorporate an energy storage system into a microgrid configured Forward Operating Base to reduce the fossil fuel consumption and to ultimately save lives. Energy storage vendors will be sending their systems to SNL Energy Storage Test Pad (ESTP) for functional testing and then to the BCIL for performance evaluation. The technologies that will be tested are electro-chemical energy storage systems comprising of lead acid, lithium-ion or zinc-bromide. GS Battery and EPC Power have developed an energy storage system that utilizes zinc-bromide flow batteries to save fuel on a military microgrid. This report contains the testing results and some limited analysis of performance of the GS Battery, EPC Power HES RESCU.

25 ENERGY STORAGE↗

Test report : Raytheon / KTech RK30 Energy Storage System

The Department of Energy Office of Electricity (DOE/OE), Sandia National Laboratories (SNL) and the Base Camp Integration Lab (BCIL) partnered together to incorporate an energy storage system into a microgrid configured Forward Operating Base to reduce the fossil fuel consumption and to ultimately save lives. Energy storage vendors will be sending their systems to SNL Energy Storage Test Pad (ESTP) for functional testing and then to the BCIL for performance evaluation. The technologies that will be tested are electro-chemical energy storage systems comprising of lead acid, lithium-ion or zinc-bromide. Raytheon/KTech has developed an energy storage system that utilizes zinc-bromide flow batteries to save fuel on a military microgrid. This report contains the testing results and some limited analysis of performance of the Raytheon/KTech Zinc-Bromide Energy Storage System.

25 ENERGY STORAGE↗

Machine Learning-Enabled Correlation and Modeling of Multimodal Response of Thin Film to Environment on Macro and Nanoscale Using “Lab-on-a-Crystal”

To close the feedback loop between artificial intellegence-controlled materials synthesis and characterization, material functionality must be rapidly tested. A platform for high-throughput multifunctional materials characterization is developed using a quartz crystal microbalance with auxiliary in-plane electrodes and a custom gas/vapor flow cell, enabling simultaneous scanning probe microscopy and electrical, optical, gravimetric, and viscoelastic characterization on the same film under controlled environment. The lab-on-a-crystal in situ multifunctional output allows direct correlations between the gravimetric/viscoelastic, electrical, and optical responses of polymer film in response to environment. Finally, when multiple film properties are used to augment the training set for machine learning regression, prediction of material response to the environment improves by a factor of 13 when <5% of the total dataset is used for model training.

36 MATERIALS SCIENCE↗

A New Simulator for Assessing Subjective Effects of Sonic Booms

A man rated and computer driven sonic boom simulator which has been constructed and placed in operational use at NASA-Langley is described. The simulator is used to study human subjective reactions to sonic booms and has the capability of producing a wide range of signatures under controlled conditions. Results are presented to illustrate the capability of the simulator to generate user specified N-wave and shaped booms having rise times as low as 0.5 milliseconds and peak overpressures up to 191 Pa (4 psf). The validity of the simulator as a lab research tool for studying human subjective response to sonic booms was demonstrated by successful completion of a preliminary test designed to compare loudness of N-wave sonic booms with results obtained by other investigators. Excellent agreement of the preliminary test data with existing data was observed. This provided confidence in the experimental methodology and established the simulator as a viable tool for performing detailed evaluations of sonic boom loudness and acceptability within the lab. environment.

Leatherwood, Jack D.↗

Proton radius from electron scattering data

Background: The proton charge radius extracted from recent muonic hydrogen Lamb shift measurements is significantly smaller than that extracted from atomic hydrogen and electron scattering measurements. The discrepancy has become known as the proton radius puzzle. Purpose: In an attempt to understand the discrepancy, we review high-precision electron scattering results from Mainz, Jefferson Lab, Saskatoon and Stanford. Methods: We make use of stepwise regression techniques using the F-test as well as the Akaike information criterion to systematically determine the predictive variables to use for a given set and range of electron scattering data as well as to provide multivariate error estimates. Results: Starting with the precision, low four-momentum transfer (Q 2 ) data from Mainz (1980) and Saskatoon (1974), we find that a stepwise regression of the Maclaurin series using the F-test as well as the Akaike information criterion justify using a linear extrapolation which yields a value for the proton radius that is consistent with the result obtained from muonic hydrogen measurements. Applying the same Maclaurin series and statistical criteria to the 2014 Rosenbluth results on GE from Mainz, we again find that the stepwise regression tends to favor a radius consistent with the muonic hydrogen radius but produces results that are extremely sensitive to the range of data included in the fit. Making use of the high-Q 2 data on G E to select functions which extrapolate to high Q 2 , we find that a Pad´e (N = M = 1) statistical model works remarkably well, as does a dipole function with a 0.84 fm radius, G E (Q 2 ) = (1 + Q 2 /0.66 GeV 2 ) -2 . Conclusions: Rigorous applications of stepwise regression techniques and multivariate error estimates result in the extraction of a proton charge radius that is consistent with the muonic hydrogen result of 0.84 fm; either from linear extrapolation of the extreme low-Q 2 data or by use of the Pad´e approximant for extrapolation using a larger range of data. Thus, based on a purely statistical analysis of electron scattering data, we conclude that the electron scattering result and the muonic hydrogen result are consistent. Lastly, it is the atomic hydrogen results that are the outliers.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗

A small satellite design for deep space network testing and training

With the continuing exploration of the Solar System and the reemphasis on Earth focused missions, the need for faster data transmission rates has grown. Ka-band could allow a higher data delivery rate over the current X-band, however the adverse effects of the Earth's atmosphere on Ka are as yet unknown. The Deep Space Network and Jet Propulsion Lab have proposed to launch a small satellite that would simultaneously transmit X and Ka signals to test the viability of switching to Ka-band. The Mockingbird Design Team at the University of Texas at Austin applied small satellite design principles to achieve this objective. The Mockingbird design, named BATSAT, incorporates simple, low-cost systems designed for university production and testing. The BATSAT satellite is a 0.64 m diameter, spherical panel led satellite, mounted with solar cells and omni-directional antennae. The antennae configuration negates the need for active attitude control or spin stabilization. The space-frame truss structure was designed for 11 g launch loads while allowing for easy construction and solar-panel mounting. The communication system transmits at 1 mW by carrying the required Ka and X-band transmitters, as well as an S band transmitter used for DSN training. The power system provides the 8.6 W maximum power requirements via silicon solar arrays and nickel-cadmium batteries. The BATSAT satellite will be lofted into an 1163 km, 70 deg orbit by the Pegasus launch system. This orbit fulfills DSN dish slew rate requirements while keeping the satellite out of the heaviest regions of the Van Allen radiation belts. Each of the three DSN stations capable of receiving Ka-band (Goldstone, Canberra, and Madrid) will have an average of 85 minutes of view-time per day over the satellites ten year design life. Mockingbird Designs hopes that its small satellite design will not only be applicable to this specific mission scenario, but that it could easily be modified for instrument capability for university, government, and/or commercial research.

Mcwilliams, Dennis↗

Quarterly update for VTO XFC project

Since the last update, Sandia has performed additional testing on COTS baseline cells, as well as initial testing of University of Michigan baseline graphite anode cells. The COTS cell testing included an extreme stress test using 12C charging, as well as a non-cooled 6C charging test to determine the effectiveness of cooling plates. The Michigan cells were cycled with increasing charge rates to determine rate capability and possible propensity for lithium plating. The COTS cells are 5Ah NMC/Graphite pouches from Kokam with a modest 112 Wh/kg. The University of Michigan cells are NMC ~2.6Ah NMC/Graphite pouches made at the UM Battery Lab, and were designed with a more aggressive energy density. On the horizon, we will be testing additional cells from University of Michigan, including a baseline hard carbon anode cell. We will also disassemble the graphite anode cell, and continue to analyze the dQdV signals obtained during the graphite cell experiment to further understand evidence of possible plating. We also expect to receive cells with improved anodes for eventual testing against baselines.

25 ENERGY STORAGE↗

A Compton transmission polarimeter for DC and SRF electron photo-injectors

The production of high-current and intense spin polarized electron beams is of great importance in electron-based facilities. Tests are planned to produce such beams in 2023 using GaAs-based photocathodes installed in the Brookhaven National Lab RHIC Coherent electron Cooling superconducting radiofrequency (SRF) photogun [1]. A fast and efficient electron polarimeter operating in the MeV energy range is required to measure the beam spin polarization. While Mott polarimeters provide larger measured asymmetries, a Compton Transmission polarimeter is well suited in the few MeV energy range. In this work, we report on a relatively compact and cost-effective Compton transmission polarimeter which has been built and calibrated at Jefferson Lab (JLab). First, we present the design of the polarimeter radiator, polarized target analyzing magnet, BGO detector assembly and data acquisition system. Next, results of a two-week commissioning study performed at the JLab Upgraded Injector Test Facility will be described. Here, a well-known polarized electron beam produced from a bulk GaAs photocathode in a dc high-voltage photogun was first measured in a 180 keV Mott scattering polarimeter, then used to characterize and calibrate the Compton transmission polarimeter as a function of the polarized target magnetization and beam properties. Finally, we report an effective analyzing power of the Compton polarimeter and compare experimental results with those produced via Geant4 simulations.

Blume, G.↗

A Compton transmission polarimeter for DC and SRF electron photo-injectors

The production of high-current and intense spin polarized electron beams is of great importance in electron-based facilities. Tests are planned to produce such beams in 2023 using GaAs-based photocathodes installed in the Brookhaven National Lab RHIC Coherent electron Cooling superconducting radiofrequency (SRF) photogun [1]. A fast and efficient electron polarimeter operating in the MeV energy range is required to measure the beam spin polarization. While Mott polarimeters provide larger measured asymmetries, a Compton Transmission polarimeter is well suited in the few MeV energy range. In this work, we report on a relatively compact and cost-effective Compton transmission polarimeter which has been built and calibrated at Jefferson Lab (JLab). First, we present the design of the polarimeter radiator, polarized target analyzing magnet, BGO detector assembly and data acquisition system. Next, results of a two-week commissioning study performed at the JLab Upgraded Injector Test Facility will be described. Here, a well-known polarized electron beam produced from a bulk GaAs photocathode in a dc high-voltage photogun was first measured in a 180 keV Mott scattering polarimeter, then used to characterize and calibrate the Compton transmission polarimeter as a function of the polarized target magnetization and beam properties. Finally, we report an effective analyzing power of the Compton polarimeter and compare experimental results with those produced via Geant4 simulations.

Blume, G.↗

Building Model Calibration: Validation of GridLAB-D Thermal Dynamics Modeling

This report investigates how well GridLAB-D’s house model characterizes the thermal dynamics of buildings given the overpredicted diurnal electric load swing observed in the Distribution System Operation with Transactive (DSO+T) study. This study seeks to validate GridLAB-D’s house model by calibrating it to data from the well-instrumented Pacific Northwest National Laboratory Lab Homes in Richland, WA. The datasets chosen included multiple pre-cooling and pre-heating testing periods where the indoor air temperature was allowed to float over a multi-hour length of time to mimic diurnal behavior. The multi-season calibrations were evaluated by comparing the heating/cooling electric power, indoor air temperature, and the rise/decay time during temperature float periods with Lab Homes data. The default GridLAB-D assumptions for latent load fraction, air heat capacity, mass heat capacity, window-to-wall-ratio, overall envelope conductance (assumed as NORMAL thermal integrity level), and solar heat gain coefficient were compared with the calibrated model to confirm when the default assumptions were adequate and the impact of calibration on the accuracy of modeling the thermal dynamics of homes.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

Final Report – Cooperative Research and Development Agreement between National Energy Technology Laboratory and Oxergy, Inc.

The NETL Raman Gas Analyzer (RGA) has been demonstrated to have an extremely fast response (<1 second) multi-gas analysis capability. All but the noble gases are Raman active, although the Raman interaction is weak. The RGA uses a reflectively lined capillary as the optical cell, providing both a small sample volume for fast gas exchange, and a much greater Raman signal collection than traditional instrument configurations. This allows very fast measurement of fuel gases (hydrogen, methane, ethane, propane) as well as other common industrial gases (carbon monoxide, carbon dioxide, nitrogen, oxygen, and water). This provides a new enabling technology for faster, smarter process control based on the chemical composition of the gases in the process – including improved fuel flexibility and efficiency for power generation systems. Research and development up to 2016 resulted in the construction of two field prototypes of the NETL RGA, which has been in applied to various laboratory applications for testing. The results of the testing have been used to improve the RGA design, with the intent to support technology transfer. The quality of the optical capillary used in the RGA is critical to its performance, and prior work at NETL produced a few optical capillaries superior to those commercially available. The production of high optical quality capillaries, however, was inconsistent in its results. With the support of the DOE Office of Technology Transitions, through the Technology Commercialization Fund program, this project was undertaken to address this commercialization barrier and to also evaluate the possible application of Raman gas analysis to a supercritical water gasification process being developed by Oxergy Inc. Oxergy, a small business located in Fairbanks, Alaska, is developing ultra-compact thermochemical reaction devices built with advanced manufacturing processes. Chief Technology Officer Jonathan Kamler holds the (pending) patent to Oxergy’s core reactor technology. Oxergy maintains wet-lab and combustion-lab space at the University of Alaska Fairbanks Center for Sustainable Living in Palmer, Alaska, where Mr. Kamler operates a pilot-scale, supercritical water gasification system designed and built by Oxergy. Mr. Kamler also operates an All Powers Labs Power Pallet gasifier coupled to a 10KW electrical generator as a dry biomass test platform at the Palmer facility. Both systems are suitable for real-world, collaborative testing of Raman gas analysis applications. The objectives of the CRADA include making the production of high-quality optical capillaries consistent and high yield, investigating other options for optical waveguides, and testing the capillaries for measurements in supercritical water gasification. Success on these objectives will support commercialization of both the RGA and supercritical water gasification technologies. Through the work performed on this project, a new apparatus was constructed and optimized to provide consistent production of high-quality optical capillaries. Several thick-walled capillaries were coated using this apparatus and shipped to Oxergy in September 2018 for testing in both dry gasification and supercritical water gasification process monitoring applications at University of Alaska Fairbanks facilities in Palmer. The strong earthquake near Anchorage and Palmer in November 2018 caused extensive damage and closure of the facilities used by Oxergy, preventing Oxergy from proceeding with experimental testing before the end of the project; the facility has been closed indefinitely. Earthquake damage prohibited the completion of all the project objectives prior to the end of the project. However, significant progress was made toward addressing a core technology commercialization barrier. The largest and most mature potential market for Raman gas analysis is its use in analytical instruments, which require sensitivity and low detection limits, and Oxergy’s market research found that market inertia is a barrier to commercial success in this market. Although NETL’s innovations in capillary coating have substantially improved Raman gas analysis capability, the likely market is expected to be niche applications that value the fast detection of real-time changes in gas composition.

Chorpening, Benjamin↗

Oak Ridge National Laboratory Current Magnitude and Frequency Response of SIPROTEC Relays

This project examined the current magnitude and frequency response of 7SJ61 and 7SJ62 SIPROTEC relays. The measured sample frequencies for the 7SJ61 and 7SJS62 relays were 800 and 960 Hz, respectively. The relays were tested at frequencies of up to 1 and 20.16 kHz. Two experiments were run in a lab environment. The first experiment was run at frequencies of up to 1 kHz every 10 Hz. The second one was run at frequencies of up to 20.16 kHz every 200 and 240 Hz (common factors of sample rate frequency) for the 7SJ61 and 7SJ62 SIPROTEC relays, respectively. Both experiments were set at a current magnitude of 0.1 and 0.5 Arms. A testbed with a Relay Test Equipment (RTE) was set to run the experiment at frequencies of up to 1 kHz, while a testbed with a RTE and High Frequency Power Source/ Amplifier (HFPS/A) was set to run at frequencies of up to 20.16 kHz. Currents of 0.1 and 0.5 Arms at different frequencies were connected at Phase A of the relays, and a current of 1 Arms (60 Hz) was connected at Phase B of relays. The 1 Arms current allowed the relays to trip and saved their record events by setting both relays at a definite-time overcurrent protection function. The record events were collected after the 7SJ61 and 7SJ62 relays tripped, and the current magnitude and frequency were plotted. The record events from the relays were collected using the DIGSI® 4 software. The SYNCHROWAVE® Event and MATLAB® software were then used to plot the current magnitude and frequency, respectively, from the relay record events. The current magnitude and frequency were plotted at time and frequency domain, respectively.The 7SJ61 and 7SJ62 relays measured source frequencies of up to 400 and 480 Hz, respectively. The percentage error of frequency for the relays increased after 400 and 480 Hz, respectively. The 7SJ62 relay with 0.1 and 0.5 Arms measured the alias frequency up to 1440 Hz. The 7SJ61 relay with 0.1 and 0.5 Arms measured the alias frequency up to 1000 and 1200 Hz, respectively. At frequencies higher than the alias frequency, the relays measured a DC amplitude current instead of an AC amplitude current. In the DC amplitude current zone, non-desired frequencies were measured by both relays. The current magnitude intensity (dB) for the 7SJ61 and 7SJ62 relays from 1 to 20.16 kHz were plotted. The current magnitude intensity for the 7SJ61 relay decreased up to 2600 and 1200 Hz for 0.5 and 0.1 Arms tests, respectively. However, the current magnitude intensity for the 7SJ62 relay decreased up to 4800 and 2640 Hz for 0.5 and 0.1 Arms tests, respectively. The current magnitude and frequency response study for the 7SJ61 and 7SJ62 relays was performed satisfactorily, observing the source, alias, and non-desired measured frequency zones for both relays.

24 POWER TRANSMISSION AND DISTRIBUTION↗

A Framework for Intelligent Rocket Test Facilities with Smart Sensors

A long-term center goal at the John C. Stennis Space Center (SSC) is the formulation and implementation of a framework for an Intelligent Rocket Test Facility (IRTF), which incorporates distributed smart sensor elements. The IRTF is to provide reliable, high-confident measurements. Specific objectives include: 1. Definition of a framework and architecture that supports implementation of highly autonomous methodologies founded on basic physical principles and embedded knowledge. 2. Modeling of autonomous sensors and processes as self-sufficient, evolutionary elements. 3. Development of appropriate communications protocols to enable the complex interactions that must take place to allow timely and high-quality flow of of information among all the autonomous elements of the system. 4. Development of lab-scale prototypes of key system elements. Though our application is next-generation rocket test facilities, applications for the approach are much wider and include monitoring of shuttle launch operations, air and spacecraft operations and health monitoring, and other large-scale industrial system operations such as found in processing and manufacturing plans. Elements of prototype IRTF have been implemented in preparation for advanced development and validation using rocket test stand facilities as SSC. This work has identified issues that are important to further development of complex network and should be of interest to other working with sensor networks.

Figueroa, Fernando↗

Hands-On, Heads-Up: Blending Cyber T&E with Data Science-Driven Training in Jupyter Notebooks

In an era of increasingly sophisticated threats to critical infrastructure, cybersecurity professionals must be more than just aware; they must be immersed, agile, and equipped to operate in environments where failure is not an option. Nowhere is this truer than in the nuclear sector, where cyber-physical systems, regulatory scrutiny, and insider threat potential demand a new generation of hands-on, technically fluent defenders. This paper presents a unified training approach that integrates Cybersecurity Test and Evaluation (T&E) with data science techniques using Jupyter Notebooks as the interactive lab environment. The program centers on a modular, scenario-driven curriculum designed to build not just knowledge but practical capability in the assessment and defense of radiation detection systems, firmware interfaces, and operational security postures.

98 - NUCLEAR DISARMAMENT, SAFEGUARDS, AND PHYSICAL↗

An exploration of benchtop X–ray emission spectroscopy for precise characterization of the sulfur redox state in cementitious materials

The evolution of sulfur chemistry in cements is best known in the bailiwick of failure mechanisms via sulfate attack but is equally important for its contributions to the reduction capacity of cementitious materials often used for immobilizing nuclear waste streams destined for long-term storage, e.g., cementitious waste forms (CWF). The total reduction capacity of CWFs, encompassing contributions from both S and Fe reductants, and its implications toward radionuclide immobilization is most often studied by destructive wet chemistry methods requiring acid digestion in the presence of Ce(IV) and subsequent titration and colorimetric interpretation. Here, we investigate a similarly analytical but nondestructive alternative, benchtop high resolution wavelength-dispersive x-ray fluorescence spectroscopy, most commonly known as x-ray emission spectroscopy (XES), for probing the bulk sulfur oxidation state distribution. We present here an initial investigation of S XES, including an improved experimental protocol for lab XES of inhomogeneous samples, both as a complement to the Ce(IV) test and for new scientific opportunities that it enables for observing changes in sulfur chemistry. We discuss future improvements and opportunities, including: (1) the practical challenges associated with coordinating XES and Ce(IV) liquid extraction for a more comprehensive perspective on reduction capacity and for a high-precision evaluation of uncertainties in the Ce(IV) test; and (2) new opportunities, due to the nondestructive nature of XES, for controlled evolution studies aimed at elucidating specific chemical responses of CWF’s exposed to invasive gas or liquid species or to accelerated aging by radiative dose or thermal treatment.

36 MATERIALS SCIENCE↗

Empirical validation and comparison of methodologies to simulate micro and macro-encapsulated PCMs in the building envelope

Thermal Energy Storage (TES) has the potential to shift peak electricity demand. Passive TES is usually implemented in building envelope as micro and macro encapsulated phase change materials (PCM) to shift electric energy demand and therefore requires careful heat transfer analysis. Whole building energy modelling with simplified heat transfer analysis has become extremely important for designers, architects, engineers, and researchers to predict energy performance of buildings. It is important to validate PCM modelling algorithms used in building energy programs to quantify their error and prove their capacity to model different PCM encapsulation types. This study uses data from a microencapsulated PCM and two macroencapsulated PCMs (Bio based PCM and hydrate salts) tested in full-scale using the Advanced Multiscale Building Energy Research (AMBER) Lab located at the Colorado School of Mines and is used to validate a numerical algorithm written in MATLAB language. To approximate the heat transfer through a wall assembly with macroencapsulated PCM pouches, several modelling techniques that can reduce 3D heat transfer characteristics to 1D are explored in this research. A parallel path heat transfer modelling approach is found to give the closest agreement with the experimental data for the pouched PCMs in building envelope applications.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗