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At least 1,387 records · Page 77

FRACTURE MECHANICS APPROACH TO ESTIMATE FATIGUE LIVES OF WELDED LAP-SHEAR SPECIMENS

A full range of stress intensity factor solutions for a kinked crack is developed as a function of weld width and the sheet thickness. When used with the associated main crack solutions (global stress intensity factors) in terms of the applied load and specimen geometry, the fatigue lives can be estimated for the laser-welded lap-shear specimens. The estimations are in good agreement with the experimental data. A classical solution for an infinitesimal kink is also employed in the approach. However, the life predictions tend to overestimate the actual fatigue lives. The traditional life estimations with the structural stress along with the experimental stress-fatigue life data (S-N curve) are also provided. In this case, the estimations only agree with the experimental data under higher load conditions.

36 MATERIALS SCIENCE↗

Primary Water Stress Corrosion Cracks in Nickel Alloy Dissimilar Metal Welds: Detection and Sizing Using Established and Emerging Nondestructive Examination Techniques

The U.S. Nuclear Regulatory Commission has established the Program to Assess the Reliability of Emerging Nondestructive Techniques (PARENT) as a follow-on to the international cooperative Program for the Inspection of Nickel Alloy Components (PINC). The goal of PINC was to evaluate the capabilities of various nondestructive evaluation (NDE) techniques to detect and characterize surface-breaking primary water stress corrosion cracks in dissimilar-metal welds (DMW) in bottom-mounted instrumentation (BMI) penetrations and small-bore (≈400-mm diameter) piping components. A series of international blind round-robin tests were conducted by commercial and university inspection teams. Results from these tests showed that a combination of conventional and phased-array ultrasound techniques provided the highest performance for flaw detection and depth sizing in dissimilar metal piping welds. The effective detection of flaws in BMIs by eddy current and ultrasound shows that it may be possible to reliably inspect these components in the field. The goal of PARENT is to continue the work begun in PINC and apply the lessons learned to a series of open and blind international round-robin tests that will be conducted on a new set of piping components including large-bore (≈900-mm diameter) DMWs, small-bore DMWs, and BMIs. Open round-robin testing will engage universities and industry worldwide to investigate the reliability of emerging NDE techniques to detect and accurately size flaws having a wide range of lengths, depths, orientations, and locations. Blind round-robin testing will invite testing organizations worldwide, whose inspectors and procedures are certified by the standards for the nuclear industry in their respective countries, to investigate the ability of established NDE techniques to detect and size flaws whose characteristics range from easy to very difficult to detect and size. This paper presents highlights of PINC and reports on the plans and progress for PARENT round-robin tests.

cracks↗

Quarterly Management Document - FY18, 4th Quarter, Physics-based Creep Simulations of Thick Section Welds in High Temperature and Pressure Applications

During the 4th Quarter of FY18, work on this project focused on determination of the growth behavior of gamma prime precipitates with the intent of determining the growth rate constant as a function of temperature. The derived constitutive equation will be incorporated into the modeling and simulation effort for creep behavior of thick section welds in Alloy 740H for fossil energy power generation applications. Additionally, progress has been made on representing the weld and base metal microstructure using Dream3D which will be used by the modeling and simulation effort to incorporate microstructural effects into the creep behavior.

36 MATERIALS SCIENCE↗

Laser-Welded Seals for Polymer-Free Glass/Glass Modules

This project explored the use of femtosecond laser welding to form strong, hermetic seals for glass/glass modules. The results showed that glass/glass fs laser welds, when coupled to a new module design, are strong enough to enable a polymer-free module, potentially extending warrantees and forming an easily-recycled product.

DuraMAT↗

Microstructural Characteristics, Mechanical Properties, and Corrosion Behavior of Field-Assisted Diffusion Welded Alloy 617

This study investigated the microstructural characteristics, mechanical response, and corrosion resistance of Alloy 617 diffusion welded by electric field-assisted sintering (EFAS). The microstructure exhibited good grain boundary (GB) migration across the interface and flat interface in the samples bonded at different conditions. Graded grain size was observed, with grain coarsening being more significant near sample surface due to EFAS-induced temperature gradient. Tensile testing revealed that the specimens fractured in the matrix away from the interface. The peak strength of 807 MPa was obtained in the samples welded at 1000°C. The materials obtained at 1100°C exhibited reduced tensile strength but improved ductility. Strain maps revealed by digital image correlation showed the flat interfaces were less ductile compared to the matrix. The hardness reduced near sample surfaces due to enlarged grains induced by temperature gradient. The interfaces with GB migration exhibited improved corrosion resistance in molten salt compared to the flat interfaces.

36 - MATERIALS SCIENCE↗

Welding of Stainless Materials

It would appear that welds in some stainless steels, heat-treated in some practicable way, will probably be found to have all the resistance to corrosion that is required for aircraft. Certainly these structures are not subjected to the severe conditions that are found in chemical plants.

WELDING↗

Comparative Study of Oxides Formed on Fusion Zone and Base Metal of Laser Welded Zr-1.0Sn-1.0Nb-0.1Fe Alloy

Numerous studies have primarily focused on the corrosion mechanism of zirconium alloy base metal. However, the corrosion resistance of weld beads or seams is of vital importance in the degradation of structural components in the reactor. In the present work, the corrosion resistance of the fusion zone and base metal of laser welded zirconium alloy joints was comparatively investigated. The microstructure morphologies, phase structures and strain fields of oxide films formed on fusion zone and base metal were observed and analyzed. The oxide thickness of the fusion zone was thicker than that of the base metal with prolonged corrosion. Compared to the base metal, the lower density of dislocations and level of strain values in the oxide film of the fusion zone indicated that the stress in the oxide film was lower. The phase transition from the tetragonal ZrO{sub 2} to the monoclinic ZrO{sub 2} could be suppressed due to the high level of stress, resulting in the better corrosion resistance of the base metal. Moreover, the second phase particles and non-βZr phase in the base metal contributed to the better corrosion resistance.

36 MATERIALS SCIENCE↗

Manufacturing and Performance Assessment of Stamped, Laser Welded, and Nitrided FeCrV Stainless Steel Bipolar Plates for Proton Exchange Membrane Fuel Cells

A manufacturing and single-cell fuel cell performance study of stamped, laser welded, and gas nitrided ferritic stainless steel foils in an advanced automotive bipolar plate assembly design was performed. Two developmental foil compositions were studied: Fee20Cre4V and Fee23Cre4V wt.%. Foils 0.1 mm thick were stamped and then laser welded together to create single bipolar plate assemblies with cooling channels. The plates were then surface treated by pre-oxidation and nitridation in N2e4H2 based gas mixtures using either a conventional furnace or a short-cycle quartz lamp infrared heating system. Single-cell fuel cell testing was performed at 80 C for 500 h at 0.3 A/cm2 using 100% humidification and a 100%/40% humidification cycle that stresses the membrane and enhances release of the fluoride ion and promotes a more corrosive environment for the bipolar plates. Periodic high frequency resistance potential-current scans during the 500 h fuel cell test and posttest analysis of the membrane indicated no resistance increase of the plates and only trace levels of metal ion contamination.

Brady, Michael P↗

Effect of laser welding on deformation mechanisms in irradiated austenitic stainless steel

In this work, deformation mechanism of a laser weld on neutron irradiated AISI 304L stainless steel was studied by in-situ microcompression test at room temperature. The deformation-induced austenite-to-martensite phase transformation occurs in {101}-oriented grains in the irradiated base metal, while deformation twinning prevails in {101}-oriented grains in the weld heat affected zone (HAZ). A high number density of irradiation-induced voids in the base metal provide sufficient nucleation sites for the austenite-to-martensite phase transformation under compression at room temperature. A deformation map is established to predict critical twinning stress for face-centered cubic (fcc) metals and alloys. Our study suggests that irradiation can tailor the deformation-induced phase transformation in austenitic stainless steels.

36 MATERIALS SCIENCE↗

Force reduction of friction stir welding and processing of steel

Friction stir welding and processing (FSW&P) is considered as a new fabrication method for canisters and repair of existing dry cask storage system canisters (generally made of austenitic stainless steel). Low heat input compared to fusion joining processes and grain refinement associated with low-temperature FSW&P result in a material with improved mechanical properties and equivalent generalized corrosion performance relative to the base metal. But FSW&P of austenitic stainless steel requires significant tool forge axis force to produce a weld (or a run). Exploratory runs utilizing forge axis force control were conducted to investigate the minimum force required to achieve defect-free runs. The correlation between forge axis force and resultant plunge depth was also investigated. Furthermore, detailed microstructural characterization was conducted to display the microstructural variation within the nugget zone.

36 MATERIALS SCIENCE↗

MaterialsMap: A CALPHAD-based tool to design composition pathways through feasibility map for desired dissimilar materials, demonstrated with resistance spot welding joining of Ag-Al-Cu

Assembly of dissimilar metals can be achieved by different methods, for example, casting, welding, and additive manufacturing (AM). However, undesired phases formed in liquid-phase assembling processes due to solute segregation during solidification diminish mechanical and other properties of the processed parts. In the present work, an open-source software named MaterialsMap, has been developed based on the CALculation of Phase Diagrams (CALPHAD) approach. The primary objective of MaterialsMap is to facilitate the design of an optimal composition pathway for assembling dissimilar alloys with liquid-phases based on the formation of desired and undesired phases along the pathway. In MaterialsMap, equilibrium thermodynamic calculations are used to predict equilibrium phases formed at slow cooling rate, while Scheil-Gulliver simulations are employed to predict non-equilibrium phases formed during rapid cooling. Additionally, by combining these two simulations, MaterialsMap offers a thorough guide for understanding phase formation in various manufacturing processes, assisting users in making informed decisions during material selection and production. As a demonstration of this approach, a compositional pathway was designed from pure Al to pure Cu through Ag using MaterialsMap. The design was experimentally verified using resistance spot welding (RSW).

36 MATERIALS SCIENCE↗

Altered ion transport in normal human bronchial epithelial cells following exposure to chemically distinct metal welding fume particles

Welding fume inhalation causes pulmonary toxicity, including susceptibility to infection. We hypothesized that airway epithelial ion transport is a target of fume toxicity, and investigated the effects of fume particulates from manual metal arc-stainless steel (MMA-SS) and gas metal arc-mild steel (GMA-MS) on ion transport in normal human bronchial epithelium (NHBE) cultured in air-interface. MMA-SS particles, more soluble than GMA-MS particles, contain Cr, Ni, Fe and Mn; GMA-MS particles contain Fe and Mn. MMA-SS or GMA-MS particles (0.0167–166.7 μg/cm{sup 2}) were applied apically to NHBEs. After 18 h transepithelial potential difference (V{sub t}), resistance (R{sub t}), and short circuit current (I{sub sc}) were measured. Particle effects on Na{sup +} and Cl¯ channels and the Na{sup +},K{sup +},2Cl¯-cotransporter were evaluated using amiloride (apical), 5-nitro-2-[(3-phenylpropyl)amino]benzoic acid (NPPB, apical), and bumetanide (basolateral), respectively. MMA-SS (0.0167–16.7 μg/cm{sup 2}) increased basal V{sub t}. Only 16.7 μg/cm{sup 2} GMA-MS increased basal V{sub t} significantly. MMA-SS or GMA-MS exposure potentiated I{sub sc} responses (decreases) to amiloride and bumetanide, while not affecting those to NPPB, GMA-MS to a lesser degree than MMA-SS. Variable effects on R{sub t} were observed in response to amiloride, and bumetanide. Generally, MMA-SS was more potent in altering responses to amiloride and bumetanide than GMA-MS. Hyperpolarization occurred in the absence of LDH release, but decreases in V{sub t}, R{sub t}, and I{sub sc} at higher fume particulate doses accompanied LDH release, to a greater extent for MMA-SS. Thus, Na{sup +} transport and Na{sup +},K{sup +},2Cl¯-cotransport are affected by fume exposure; MMA-MS is more potent than GMA-MS. Enhanced Na{sup +} absorption and decreased airway surface liquid could compromise defenses against infection. - Highlights: • Welding fume particle toxicity was investigated in human bronchial epithelial cells. • MMA-SS fume particles and GMA-MS particles were compared. • Both fumes activated epithelial Na{sup +} channels, MMA-SS more potent than GMA-SS. • MMA-SS is more cytotoxic than GMA-SS with regard to LDH release. • Observed changes may help explain susceptibility to infection in workers.

60 APPLIED LIFE SCIENCES↗

Effect of hook characteristics on the fracture behaviour of dissimilar friction stir welded aluminium alloy and mild steel sheets

Under tensile shear loading, fracture modes of dissimilar lap welds produced by friction stir scribe technology were studied. Three fracture modes were observed. For zone A fracture, the initial crack was restrained, and the joint ultimately fractured in the base mild steel. For zone B fracture, the initial crack progressed through the aluminium sheet just above the Al/steel interface. For zone C fracture, the initial crack proceeded along the steel hook to the aluminium sheet surface. Fracture mode and joint strength were greatly influenced by steel hook size, and the steel hook size was affected by welding parameters and tool scribe height. In this study, the experimental joint strength achieved the calculated joint load limit.

Wang, Tianhao↗

Diffusion-Welded Microchannel Heat Exchanger for Industrial Processes

The goal of next generation reactors is to increase energy ef?ciency in the production of electricity and provide high-temperature heat for industrial processes. The ef?cient transfer of energy for industrial applications depends on the ability to incorporate effective heat exchangers between the nuclear heat transport system and the industrial process. The need for ef?ciency, compactness, and safety challenge the boundaries of existing heat exchanger technology. Various studies have been performed in attempts to update the secondary heat exchanger that is downstream of the primary heat exchanger, mostly because its performance is strongly tied to the ability to employ more ef?cient industrial processes. Modern compact heat exchangers can provide high compactness, a measure of the ratio of surface area-to-volume of a heat exchange. The microchannel heat exchanger studied here is a plate-type, robust heat exchanger that combines compactness, low pressure drop, high effectiveness, and the ability to operate with a very large pressure differential between hot and cold sides. The plates are etched and thereafter joined by diffusion welding, resulting in extremely strong all-metal heat exchanger cores. After bonding, any number of core blocks can be welded together to provide the required ?ow capacity. This study explores the microchannel heat exchanger and draws conclusions about diffusion welding/bonding for joining heat exchanger plates, with both experimental and computational modeling, along with existing challenges and gaps. Also, presented is a thermal design method for determining overall design speci?cations for a microchannel printed circuit heat exchanger for both supercritical (24 MPa) and subcritical (17 MPa) Rankine power cycles.

42 ENGINEERING↗

Torch End-Effector and TIG Electrode Changeout Design for a TIG Welding Robot Used in Metal Big Area Additive Manufacturing

Metal Big Area Additive Manufacturing (mBAAM) is a promising approach to large-scale metal additive manufacturing (AM) or 3D printing. The mBAAM system uses an arc-based wire-fed welding robot to build metal parts. A multi-degree-of-freedom robotic arm is known for its extensive range of motion and reliable tool handling. Attaching a torch end-effector to a robotic arm gives it welding capabilities; however, this decreases the motion range and dynamics of the robot. As a result, build volume and printing accuracy are decreased. Additionally, only a portion of time is spent printing in an arc-based process. Maintenance leads to downtime on the system. In a tungsten inert gas (TIG)-based process, the torch electrode wears out over time and must be changed to avoid defective deposition. This paper proposes an approach for a compact torch end-effector to improve the robot’s build volume. This paper also proposes an approach to reducing non-printing process time by designing and implementing a semi-automated electrode changing system.

Masuo, Chris↗

Use of Mini-CT specimens for Fracture Toughness Characterization of Low Upper-Shelf Linde 80 Weld Before and After Irradiation

Mini-CT specimens are becoming highly anticipated geometry for use in reactor pressure vessel (RPV) community for direct measurement of fracture toughness in transition region using the Master Curve methodology. In the present study, Mini-CT specimens were machined from previously tested Charpy specimens of Midland low upper-shelf Linde 80 weld in both, unirradiated and irradiated condition. The irradiated specimens have been characterized as part of join ORNL-EPRI-CRIEPI collaborative program. The Linde 80 weld was selected based on the facts that it has been previously extensively characterized in the irradiated condition by conventional specimens and because of the awareness to validate application of Mini-Ct specimens for material with lower upper shelf which is more likely will be the case for irradiated material of older generation of RPVs. It is shown that the reference transition fracture toughness temperatures, To, derived from these Mini-CT specimens are in good agreement with To values previously recorded for this material in the unirradiated and irradiated conditions. However, this study indicates that in real practice it is highly advisable to use a much larger number of specimens than the minimum amount prescribed in ASTM E1921.

Sokolov, Mikhail↗

Development of Helium Vessel Welding Process for SNS PPU Cavities

The Spallation Neutron Source Proton Power Upgrade cavities are produced by Research Instrument with all the cavity processing done at vendor sites with final chemistry applied to the cavity to be electropolishing. Cavities are delivered to Jefferson Lab, ready to be tested. One of the tasks to be completed before the arrival of production-ready PPU cavities is to develop a robust helium vessel welding protocol. We have successfully developed the process and applied it to three six-cell high beta cavities. Here, we present the summary of RF results, welding process development, and post helium vessel RF results.

Dhakal, P.↗

Fundamental Study of Micro-Defects in Electropolished EB-Welded and Hydroformed SRF Accelerating Structures

In the area of niobium elecropolishing fundamentals, we focused on understanding the influence of the surface topology, and geometry (with effects from gravity included. The formation of a viscous film is essential for the electropolishing process to take place. The exact nature and composition of the film formed on niobium is still unknown because of its solubility in the electrolyte. Extensive pitting may take place at surface where a stable film cannot form. This has to be taken into consideration while determining the speed with which the SRF cavities are rotated while EP. Hydrodynamic aspects must be taken into consideration while optimizing the polishing parameters. There is improvement in surface finish with polishing time. There is a huge change in surface quality when the EP time is increased from 2 hours to 4 hours but not much change takes place when the time is further increased to 6 hours. So keeping the economic points in view, about 100 um defect layer removal may be sufficient to get the desired performance. In the area of Electropolishing of untreated and treated niobium with Weld Joints we studied untreated and treated Nb, especially for the heat affected areas next to welded bumps, electropolished for different durations. The electropolishing of the untreated Nb caused the formation of pits on the surface at about 15 min but they disappeared when the electropolishing duration was more than 15 min. Electropolishing for 120 min smoothened the surface of untreated Nb by levelling the surface, but the severe formation of pits on the whole surface was found after 240 min. The treatment of Nb significantly changed the Nb surface morphology which was covered by grains of different size that looked light or dark in the optical microscope. The treated Nb was susceptible to pitting during the entire electropolishing starting from 15 min and the dark grains had more susceptibility to pitting than the light grains. In addition, electropolishing for 240 min again resulted in severe pit formation. In the area of Bulge test and microstructure studies, we worked to create a useful constitutive relationship for the complex stress state that accompanies SRF cavity formation. To do so, bulge tests were performed on Cu and Nb tube samples that exhibited the greatest degrees of uniaxial elongation after HT. The data from the bulge tests and an accompanying set of tensile tests provided input to a finite-element model that recreated the bulge tests numerically. As expected the model based on the bulge test results fit the experimental data well at least at low stress levels safely below the bursting pressure. Not so for that based on the tensile results. The results of the study emphasize the importance of for bulge testing rather than tensile testing when deriving the constitutional relationships eventually needed for modelling the hydroforming of Nb SRF cavities.

43 PARTICLE ACCELERATORS↗