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At least 1,387 records · Page 77
All sourcesNASA NTRSDOE OSTI
DOE OSTI2012

Large-scale and shape-controlled synthesis and characterization of nanorod-like nickel powders under microwave radiation

Graphical abstract: The nanorod-like pure nickel were fabricated via hydrothermal liquid phase reduction route under microwave irradiation with hydrazine hydrate as a reducing agent as well as polyvinyl alcohol as a dispersant and/or structure directing agent. The materials were characterized by XRD, SEM, EDS, HRTEM, and selected-area electron diffraction, etc. The lattice expansion for Ni powders was explained in detail. As-prepared Ni sample was of obvious shape anisotropy with length diameter ratio of 5. Magnetic measurements shown that the magnetic properties of Ni nanorod-like (fcc) were quite different from those of hexagonal closed-packed (hcp) Ni nanoparticles. Highlights: Black-Right-Pointing-Pointer The synthesis of nanorod-like nickel under microwave irradiation. Black-Right-Pointing-Pointer Nitrogen generated in reaction as a shielding gas. Black-Right-Pointing-Pointer The lattice expansion for Ni powders was explained in detail. Black-Right-Pointing-Pointer Magnetic properties of Ni were quite different from those of Ni nanoparticles. -- Abstract: The nanorod-like nickel powders were fabricated via hydrothermal liquid phase reduction route under microwave irradiation with hydrazine hydrate as a reducing agent as well as polyvinyl alcohol as a dispersant and/or structure directing agent. The morphology and structure of as-prepared products could be easily tuned by adjusting process parameters such as pH value and microwave irradiation time. The resulting materials were characterized by X-ray diffraction (XRD), scanning electron microscope, transmission electron microscopy and selected-area electron diffraction (SAED). The results demonstrated that pure nickel powders with face-centered cubic (fcc) structure were prepared at relatively mild condition and no characteristic peaks of nickel oxide in the XRD pattern were found. The phenomenon of lattice expansion for Ni powders was explained in details according to the XRD theory. As-prepared Ni sample was of obvious shape anisotropy with length diameter ratio of 5. Magnetic measurements shown that the magnetic properties of nanorod-like (fcc) Ni powders were quite different from those of hexagonal closed-packed (hcp) Ni nanoparticles. Furthermore, it had more strong ferromagnetic properties than that of Ni powders both bulk and nanoparticles.

36 MATERIALS SCIENCE↗
DOE OSTI2020

Observation of Weyl fermions in a magnetic non-centrosymmetric crystal

The absence of inversion symmetry in non-centrosymmetric materials has a fundamental role in the emergence of a vast number of fascinating phenomena, like ferroelectricity, second harmonic generation, and Weyl fermions. The removal of time-reversal symmetry in such systems further extends the variety of observable magneto-electric and topological effects. Here we report the striking topological properties in the non-centrosymmetric spin-orbit magnet PrAlGe by combining spectroscopy and transport measurements. By photoemission spectroscopy below the Curie temperature, we observe topological Fermi arcs that correspond to projected topological charges of ±1 in the surface Brillouin zone. In the bulk, we observe the linear energy-dispersion of the Weyl fermions. We further observe a large anomalous Hall response in our magneto-transport measurements, which is understood to arise from diverging bulk Berry curvature fields associated with the Weyl band structure. These results establish a novel Weyl semimetal phase in magnetic non-centrosymmetric PrAlGe.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
NASA NTRS1985

Magnetohydrodynamic thermal instabilities in cool inhomogeneous atmospheres

The stability of magnetic loops to current-driven filamentation instabilities is investigated. The unperturbed atmosphere is assumed to be composed of an (upper) isothermal optically thin low-density portion and a (lower) higher-density portion which is in radiative equilibrium; in both cases, the atmosphere is in hydrostatic equilibrium, so that gravitational stratification is taken into account. In order to provide specific equilibrium conditions for evaluation of the dispersion relation, conditions appropriate for the surface of a solar-type star are adopted; i.e., a fairly low temperature (T = 5000 K) appropriate for a 'precoronal' state associated, for example, with magnetic flux emerging from photospheric levels under the action of magnetic buoyancy. A linear stability analysis is performed, and numerical results show that physically plausible current densities, which would be generated by typical loop-footpoint motions, are effective in driving MHD instabilities in such a plasma. The instability growth rates are strongly dependent on the assumed current density distribution and on the density scale height.

Bodo, G.↗
DOE OSTI2019

Effect of Ce{sup 3+} Ion on Structural and Hyperfine Interaction Studies of Co{sub 0.5}Ni{sub 0.5}Fe{sub 2−x}Ce{sub x}O{sub 4} Ferrites: Useful for Permanent Magnet Applications

Nanoparticles of Co{sub 0.5}Ni{sub 0.5}Fe{sub 2−x}Ce{sub x}O{sub 4} (where x = 0.0, 0.01, 0.015 and 0.02) ferrites are prepared by the modified solution combustion method using a mixture of fuels and are characterized to understand their structural, microstructural and magnetic properties. The X-ray diffraction is used to confirm the formation of a single-phase cubic spinel structure. The average crystallite sizes are calculated using the Scherrer formula and are found to be less than 50 nm. The microstructural features are obtained by the scanning electron microscopy, and the compositional analysis is done by using the energy-dispersive spectroscopy. The transmission electron microscopy (TEM) investigations show that the synthesized ferrites are made up of very fine spherical nanoparticles. The influence of a rare-earth element (Ce{sup 3+}) on the magnetic properties of the samples was studied using the Mössbauer spectroscopy. The Mössbauer spectroscopy reveals the formation of broadened Zeeman lines and quadrupole-split lines and the presence of the Fe{sup 3+} charge state at B sites in the samples. The quadrupole splitting shows that the orientation of the magnetic hyperfine field with respect to the principle axes of the electric field gradient was random. The magnetic hyperfine field values indicate that the A sites have more A-O-B superexchange interactions than the B sites. The coexistence of magnetic sextet and a doublet component on the room-temperature spectra suggests superparamagnetic properties of the nanoparticles. The low-temperature (15 K) Mössbauer spectroscopy explores the paramagnetic relaxation in the nanoparticles. The area under the sextet refers to Fe{sup 3+} concentrations in the tetrahedral and octahedral sites of the ferrite. This study confirms that the Ce{sup 3+} substitution of Fe{sup 3+} only for octahedron sites causes the decrease in Fe-O-Fe arrangement. The effect of Ce{sup 3+} doping on the magnetic properties of Co{sub 0.5}Ni{sub 0.5}Fe{sub 2}O{sub 4} is examined from the vibrating sample magnetometry (VSM) spectra. Saturation magnetization values are decreased initially and then increased, as result of Ce{sup 3+} doping. This can be explained by Neel’s two-sub-lattice model. Further, the value of coercivity is found to be increasing with increasing Ce{sup 3+} concentration. The obtained results of M-H loop with improved coercivity (from 851 to 1039 Oe) by Ce{sup 3+} doping of Co{sub 0.5}Ni{sub 0.5}Fe{sub 2}O{sub 4} demonstrate the usefulness for permanent magnet applications.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2011

Heliopause Instabilities Driven by Plasma-Neutral Interaction: Linear Analysis from Fluid Model

The heliopause (HP) is the outer edge of the heliosphere that separates the tenuous and hot heliosheath plasma from the relatively dense and cool magnetized plasma of the local interstellar medium (LISM). As a surface of tangential discontinuity, the HP is subject to both Rayleigh-Taylor (RT) and Kelvin-Helmholtz (KH) instabilities. The coupling between plasma ions and neutral atoms through charge exchange provides an ''effective gravity'' for RT, while shear flows due to the velocity difference between the heliosheath and the interstellar flows can drive KH modes. We derive the linearized dispersion relations for waves propagating along the surface of this discontinuity using a fluid picture, to study the possibility for both RT and KH instabilities, including a second population of energetic neutrals produced by charge exchange interactions between the hot solar wind plasma in the heliosheath with interstellar hydrogen. We show that due to charge exchange interactions, the HP is unconditionally unstable to all perturbations.

71 CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSIC↗
DOE OSTI2019

Anomalous magnetic behavior of Ba 2 CoO 4 with isolated CoO 4 tetrahedra

The dimensionality of the electronic and magnetic structure of a given material is generally predetermined by its crystal structure. Here, using elastic and inelastic neutron scattering combined with magnetization measurements, we discover unusual magnetic behavior in three-dimensional (3D) Ba 2 CoO 4 . In spite of isolated CoO 4 tetrahedra, the system exhibits a 3D noncollinear antiferromagnetic order in the ground state with an anomalously large Curie-Weiss temperature of 110 K compared to T N =26 K. More unexpectedly, spin dynamics displays quasi-two-dimensional spin-wave dispersion with an unusually large spin gap, and one-dimensional magnetoelastic coupling. Our results postulate that Ba 2 CoO 4 is a unique system for exploring the interplay between isolated polyhedra, low-dimensional magnetism, and spin states in oxides.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2014

Preparation of graphene-Fe{sub 3}O{sub 4} nanocomposites using Fe{sup 3+} ion-containing magnetic ionic liquid

Graphene-Fe{sub 3}O{sub 4} (GN-Fe{sub 3}O{sub 4}) magnetic nanocomposites were prepared, GN-coated magnetic ionic liquid (MIL) as its precursors, which were used as both a magnetic resource and solvent. The method has proved to be valuable for the Fe{sub 3}O{sub 4} nanoparticles (NPs) well dispersed in the solution through strong interactions with GN, which are of interest because of their stability and chemical properties. In the process, strong interactions creates a condition for uniform dispersion in GN and [BMIm]FeCl{sub 4} (MIL) solution, and accelerate the formation of Fe{sub 3}O{sub 4} NPs. A transmission electron microscopy image has shown that the as-formed Fe{sub 3}O{sub 4} NPs with a diameter as small as 5–7 nm were deposited on GN sheets. Furthermore, the final material showed a superior properties than conventional method, which can be ascribed to the fact that [BMIm]FeCl{sub 4} plays a vital role in the process of producing small NPs size.

36 MATERIALS SCIENCE↗
DOE OSTI2019

Synthesis and Characterization of Single Phase Metal Dodecaboride Solid Solutions: Zr 1-x Y x B 12 and Zr 1-x U x B 12

Single-phase metal dodecaboride solid solutions, Zr 0.5 Y 0.5 B 12 and Zr 0.5 U 0.5 B 12 , were arranged by arc melting from pure elements. The phase purity and composition were established by powder X-ray diffraction (PXRD), energy-dispersive X-ray spectroscopy (EDS), X-ray photoelectron spectroscopy (XPS), and 10 B and 11 B solid-state nuclear magnetic resonance (NMR) spectroscopy. The effects of carbon addition to Zr 1-x Y x B 12 were studied and it was found that carbon causes fast cooling and as a result rapid nucleation of grains, as well as “templating” and patterning effects of the surface morphology. The hardness of the Zr 0.5 Y 0.5 B 12 phase is 47.6 ± 1.7 GPa at 0.49 N load, which is ~17% higher than that of its parent compounds, ZrB 12 and YB 12 , with hardness values of 41.6 ± 2.6 and 37.5 ± 4.3 GPa, respectively. The hardness of Zr 0.5 U 0.5 B 12 is ~54% higher than that of its UB 12 parent. The dodecaborides were confirmed to be metallic by band structure calculations, diffuse reflectance UV–vis, and solid-state NMR spectroscopies. The nature of the dodecaboride colors—violet for ZrB 12 and blue for YB 12 —can be applied to charge-transfer. XPS indicates that the metals are in the following oxidation states: Y 3+ , Zr 4+ , and U$^{{5+}/^{6+}}$. The superconducting transition temperatures (T c ) of the dodecaborides were determined to be 4.5 and 6.0 K for YB 12 and ZrB 12 , respectively, as shown by resistivity and superconducting quantum interference device (SQUID) measurements. The T c of the Zr 0.5 Y 0.5 B 12 solid solution was suppressed to 2.5 K.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
DOE OSTI2017

Structure of spin excitations in heavily electron-doped Li 0.8 Fe 0.2 ODFeSe superconductors

Heavily electron-doped iron-selenide high-transition-temperature (high-T c ) superconductors, which have no hole Fermi pockets, but have a notably high T c , have challenged the prevailing s± pairing scenario originally proposed for iron pnictides containing both electron and hole pockets. The microscopic mechanism underlying the enhanced superconductivity in heavily electron-doped iron-selenide remains unclear. Here, we used neutron scattering to study the spin excitations of the heavily electron-doped iron-selenide material Li 0.8 Fe 0.2 ODFeSe (T c = 41 K). Our data revealed nearly ring-shaped magnetic resonant excitations surrounding (π, π) at ~21 meV. As the energy increased, the spin excitations assumed a diamond shape, and they dispersed outward until the energy reached ~60 meV and then inward at higher energies. The observed energy-dependent momentum structure and twisted dispersion of spin excitations near (π, π) are analogous to those of hole-doped cuprates in several aspects, thus implying that such spin excitations are essential for the remarkably high T c in these materials.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2019

Electromagnetic effect on geodesic acoustic mode with adiabatic electrons

The geodesic acoustic mode (GAM) is analytically investigated by taking into account the finite-orbit-width (FOW) resonance effect to the second order and the finite β effect. The general dispersion relation is derived from the gyro-kinetic equations in the presence of nonzero δA ∥ , the parallel component of the perturbed magnetic vector potential. Transparent and concise expressions for the GAM frequency and Landau damping rate in the presence of the second order FOW effect and finite β effect are first presented. It is clearly shown that the m = ±2 harmonics dominant δA ∥ and the kinetic expression of δA ∥ have the same form as the fluid one. For the real frequency, the electromagnetic effect introduces a term on the order of q 2 β, which is comparable to the second order electrostatic terms, namely, the terms introduced by the second order FOW resonance effect. While for the collisionless damping rate, δA ∥ does not directly introduce β–dependent terms, but affects the damping rate via modifying the real frequency. Besides, our analytical result shows good agreement with the numerical examinations.

58 GEOSCIENCES↗
DOE OSTI2020

Local probes for quantum Hall ferroelectrics and nematics

Two-dimensional multivalley electronic systems in which the dispersion of individual pockets has low symmetry give rise to quantum Hall ferroelectric and nematic states in the presence of strong quantizing magnetic fields. In this work, we investigate the local signatures of these states arising near impurities that can be probed via scanning tunneling microscopy (STM) spectroscopy. For quantum Hall ferroelectrics, we demonstrate a direct relation between the dipole moment measured at impurity bound states and the ideal bulk dipole moment obtained from the modern theory of polarization. We also study the many-body problem with a single impurity via exact diagonalization and find that near strong impurities a nontrivial excitonic state can form with specific features that can be easily identified via STM spectroscopy.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗
DOE OSTI2011

Dynamics of the two-dimensional S=1/2 dimer system (C5H6N2F)2CuCl4

Inelastic neutron scattering was used to study a quantum S=1/2 antiferromagnetic Heisenberg system Bis(2-amino-5-fluoropyridinium) Tetrachlorocuprate(II). The magnetic excitation spectrum was shown to be dominated by long-lived excitations with an energy gap 1.07(3) meV. The measured dispersion relation is consistent with a simple two-dimensional square lattice of weakly-coupled spin dimers. Comparing the data to a random phase approximation treatment of this model gives the intra-dimer and inter-dimer exchange constants J=1.45(2) meV and J =0.31(3) meV, respectively.

72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS↗
DOE OSTI2019

On the Background-gyroresonant Character of Bell’s Instability in the Large-current Regime

We demonstrate that the Bell instability, which is widely considered potentially significant for cosmic-ray (CR) acceleration, is the low-frequency limit of a gyroresonant interaction between the protons of the interstellar medium and shear-Alfvén waves. At large CR current densities, its growth rate is therefore limited by the proton gyrofrequency, and two modes emerge from the cold-beam dispersion relation. A third mode driven by electron gyroresonance is only weakly unstable at low current densities. We report on implications for magnetic field amplification and its saturation in the vicinity of supernova remnants.

79 ASTRONOMY AND ASTROPHYSICS↗
NASA NTRS1977

Common approach to solving SGEMP, DEMP, and ESD survivability

System Generated Electromagnetic Pulse (SGEMP) and Dispersed Electromagnetic Pulse DEMP) are nuclear generated spacecraft environments. Electrostatic discharge (ESD) is a natural spacecraft environment resulting from differential charging in magnetic substorms. All three phenomena, though differing in origin, result in the same problem to the spacecraft and that is Electromagnetic Interference (EMI). A common design approach utilizing a spacecraft structural Faraday Cage is presented which helps solve the EMI problem. Also, other system design techniques are discussed which minimize the magnitude of these environments through control of materials and electrical grounding configuration.

Ling, D.↗
NASA NTRS1979

A spectroscopic flare of YZ Canis Minoris

Observations of a spectroscopic flare in YZ Canis Minoris are reported. Emission lines of Mg I, Fe I, and Fe II were found in the spectral region 5090-5350 A. The intensity of the emission lines declined only slightly over a span of 2 hours. No significant radial-velocity difference was found between the emission and absorption lines. The turbulent velocity dispersion was less than 20 km/s. Upper limits of 7500 and 15,000 gauss can be placed on the longitudinal and transverse magnetic fields. The equal intensities of the Mg I b lines imply that the emitting region was optically thick. The intensity ratios did not change with time.

Mochnacki, S. W.↗
NASA NTRS1980

Cusp proton signatures and the interplanetary magnetic field

The variation of proton average energy with latitude in the cusp has been suggested as an indicator of the means of particle entry. If magnetic merging is the principal means of particle entry, the proton average energy should fall with increasing latitude; if diffusion is the principal means, the average energy should first fall and then briefly rise as a function of latitude, showing a 'V' signature. In the present work, 60 selected cusp passes of the AE-D satellite for which IMP-J interplanetary or magnetosheath magnetic-field data were available were examined. About one-third of these passes showed clear or likely merging-type energy dispersions; a third showed clear or likely V-type energy dispersions, and a third showed unclear or no energy dispersions. The results are strongly correlated with the IMF - the merging signatures are associated with southward IMF and the V signatures with northward IMF. Unclear cases are associated with unsteady or weakly northward IMF.

Reiff, P. H.↗
NASA NTRS1982

Wave excitation by inhomogeneous suprathermal electron beams

Wave excitation by an inhomogeneous suprathermal electron beam in a homogeneous magnetized plasma is studied. Not only is the beam density nonuniform, but the beam electrons possess a sheared bulk velocity. The general dispersion equation encompassing both electrostatic and electromagnetic effects is derived. Particular attention is given to the whistler mode. It is established that the density-gradient and velocity-shear effects are important for waves with frequencies close to the lower-hybrid resonance frequency.

Freund, H. P.↗
NASA NTRS1983

Density drift instabilities and weak collisions

A model is developed which describes the effects of weak collisions on the linear kinetic theory of electrostatic density drift instabilities. A dispersion equation valid at all frequencies and wave numbers is derived using the assumptions of a weak, uniform density gradient; a uniform magnetic field; and the BGK collision operator with a modification of the local approximation. The properties of the universal and collisional density drift instabilities at maximum growth rates are examined in detail. The thresholds of the instabilities are examined for an ionospheric model which includes ion-neutral, electron-neutral, and electron-ion collisions, and are compared with the threshold of the lower hybrid density drift instability. It is concluded that the k to the -5th short wavelength density power spectra observed above 280 km in the PLUMEX experiment are due to the effects of the universal density drift instability.

Gary, S. P.↗