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At least 1,351 records · Page 75

Heat Flux Sensor Calibrator

The heat flux to space shuttle main engine (SSME) turbopump turbine blades may be as high as 10 to the 7th power. The heat flux causes thermal transients that are of the order of 1 sec as temperature varies from perhaps 1500 K to 100 K. It is suspected that these transients cause durability problems in the turbine blades. To quantitatively evaluate the effect of these transients, heat flux sensors or gauges were developed to obtain data to verify analytical models. The objective is to design and fabricate a system for steady state and transient calibration and durability testing of heat flux sensors for use in SSME turbine blades. The calibrator consists of: (1) the arc lamp, (2) a high speed positioning table for placing standard and special heat flux sensors in the incident beam of radiant heat flux, (3) provision for cooling the blade and special sensors inserted in the blade, (4) a computer for controlling the positioning table, storing electrical output values from sensors, and calculating heat flux from these values, and (5) a pyrometer for measuring sensor surface temperatures.

Liebert, C. H.↗

All-aerosol-jet-printed highly sensitive and selective polyaniline-based ammonia sensors: a route toward low-cost, low-power gas detection

In this work, we report the design and scalable fabrication of a low-cost and low-power polyaniline-based (PANI) ammonia (NH3) gas sensor on polyimide (PI) substrates using additive manufacturing techniques. The silver interdigitated electrode (IDE) arrays and conducting polymer films are printed onto PI using a direct-write technology of aerosol-jet printing. Morphological characteristics are examined by scanning electron microscopy and energy-dispersive X-ray analysis which reveal homogeneously printed PANI film on the IDE platform. The gas sensing performance is evaluated in the analytical early leak detection range of 5–1000 ppm NH3 in air as a function of both thermal (23 °C, 50 °C, 80 °C) and relative humidity (RH = 0%, 30%, 50%) exposures. The sensor exhibits sensitivity down to 5 ppm NH3 with a sub-ppm detection limit and good repeatability. We observe rapid NH3 detection at 0% RH with very extended times for equilibration and recovery. However, at both 30 and 50% RH, the room temperature response and recovery times are reduced to only about 1 min and 5 min, respectively. Experiments also reveal good sensitivity toward the analyte even at higher operating temperatures. Present results merit the practical application of aerosol-jet-printed, low-power sensors for industrial applications where low-level hazardous gas detection is essential.

36 MATERIALS SCIENCE↗

Europa Clipper Magnetometer Thermal Design Evolution, Validation, and Verification

Europa Clipper Spacecraft is exposed to a high radiation environment and is limited with power. This makes the thermal design of Europa Clipper magnetometer more challenging. The design is required to be highly insulated and at the same time magnetically clean. This paper describes the thermal design evolution of Europa Clipper Magnetometer. A thermal vacuum test is conducted in Europa Clipper orbit’s relevant environment to characterize the requirements and estimate the power consumption. A flight-like engineering model magnetometer from the University of California at Los Angeles (UCLA) is used for this test. Magnetically clean Cernox temperature measurement sensors with the accuracy of ±0.1ºC are used to measure the temperature value inside the sensor head and across the main frame interfaces. This level of accuracy in temperature measurement is required to capture the temperature gradient across the sensor head in a relevant environment which impacts the magnetometer measurement accuracy. Test data is used to correlate the thermal model and characterize the heat leak across the interfaces. Validated thermal model is used as a verification tool for power consumption and thermal requirements.

Caron, Ryan↗

Development of copper thiolate organometallic compound as thermal sensitive coating for energy storage system safety

Safety and reliability are primary concerns for the deployment of lithium-ion batteries, especially in electric vehicles (EV) and larger-scale energy storage systems (ESS). Current technology in battery management systems (BMS) includes cell voltage monitoring and positioning temperature sensors in selected locations. For a system with hundreds to thousands of individual batteries, single-point temperature monitoring is inadequate to detect hot spots and cell overheating, which could lead to thermal runaway. Here, we have developed a temperature-sensitive copper-thiol compound that can be directly coated onto battery pouch foils to enable early detection of thermal runaway. Upon reaching specific temperatures, this compound releases a sulfur-containing detectable gas, which can be identified using chemically specific gas sensors to trigger an early warning signal. Such a signal propagate through air offers broad signal coverage and enables a more comprehensive approach to large-area temperature monitoring. The Cu-ethanethiol coating is designed to release volatile gases when the substrate surface temperature exceeds 70 °C, with continuous outgassing as the temperature increases. The compound is composed of Cu, S, Cl, hydrocarbons and trace amounts of oxygen. Upon heating, the oxidation state of Cu(I) transitions to Cu (II), accompanied by gas release. Thermogravimetric analysis coupled with mass spectrometry correlated well with the onset of gas release temperature and emission of sulfur-containing volatile gases. Additionally, an acrylic overcoat is applied to enhance the adhesion of the thermally sensitive compound film to the battery pouch foil. This coating is expected to offer an additional safety layer for ESS, alerting possible thermal runaway events before a failure occurs, thereby allowing sufficient time to implement a mitigation plan.

Early warning systems↗

Optimal experimental designs for the estimation of thermal properties of composite materials

Reliable estimation of thermal properties is extremely important in the utilization of new advanced materials, such as composite materials. The accuracy of these estimates can be increased if the experiments are designed carefully. The objectives of this study are to design optimal experiments to be used in the prediction of these thermal properties and to then utilize these designs in the development of an estimation procedure to determine the effective thermal properties (thermal conductivity and volumetric heat capacity). The experiments were optimized by choosing experimental parameters that maximize the temperature derivatives with respect to all of the unknown thermal properties. This procedure has the effect of minimizing the confidence intervals of the resulting thermal property estimates. Both one-dimensional and two-dimensional experimental designs were optimized. A heat flux boundary condition is required in both analyses for the simultaneous estimation of the thermal properties. For the one-dimensional experiment, the parameters optimized were the heating time of the applied heat flux, the temperature sensor location, and the experimental time. In addition to these parameters, the optimal location of the heat flux was also determined for the two-dimensional experiments. Utilizing the optimal one-dimensional experiment, the effective thermal conductivity perpendicular to the fibers and the effective volumetric heat capacity were then estimated for an IM7-Bismaleimide composite material. The estimation procedure used is based on the minimization of a least squares function which incorporates both calculated and measured temperatures and allows for the parameters to be estimated simultaneously.

Scott, Elaine P.↗

Landscape-scale Characterization of Arctic Tundra Vegetation Composition, Structure, and Function with a Multi-sensor Unoccupied Aerial System: Supporting Data.

Airborne remote sensing data collected using the Brookhaven National Laboratory's (BNL) heavy-lift unoccupied aerial system (UAS) octocopter platform, the Osprey, operated by the Terrestrial Ecosystem Science and Technology (TEST) group (https://www.bnl.gov/testgroup). This package includes data from three flights flown over the NGEE-Arctic Council, Kougarok and Teller sites in July, 2018. The Osprey is a multi-sensor UAS platform that simultaneously measures very high spatial resolution optical red/green/blue (RGB) and thermal infrared (TIR) surface 'skin' temperature imagery, as well as surface reflectance at 1 nm intervals in the visible to near-infrared spectral range 350 - 1000 nm measured at regular intervals along each flight path. Derived image products include ortho-mosaiced RGB and TIR images, an RGB-based digital surface model (DSM) using the structure from motion (SfM) technique, digital terrain model (DTM), and a canopy height model (CHM). In addition, a VNIR surface reflectance file is provided for the trigger locations collected during each flight campaign. Ancillary aircraft data, flight mission parameters, and general flight conditions provided by the onboard flight and data collection computers are also included. Unprocessed and processed data products are included in this package (processing levels 0-3). Data and metadata are provided as text (*.txt, *.json, *.kml, *hdr, *.enp), tabular (*.dat, *.csv, *.waypoint, ENVI format (no extension)), point cloud (*.laz) and image (*.jpg, *.tif, *png) formats. This metadata document contains flight campaign, instrument and file metadata, along with a description of data processing levels, data products and file naming scheme.The Next-Generation Ecosystem Experiments: Arctic (NGEE Arctic), a research effort to reduce uncertainty in Earth System Models by developing a predictive understanding of carbon-rich Arctic ecosystems and feedbacks to climate. NGEE Arctic was supported by the Department of Energy?s Office of Biological and Environmental Research.The NGEE Arctic project had two field research sites: 1) located within the Arctic polygonal tundra coastal region on the Barrow Environmental Observatory (BEO) and the North Slope near Utqiagvik (Barrow), Alaska and 2) multiple areas on the discontinuous permafrost region of the Seward Peninsula north of Nome, Alaska.Through observations, experiments, and synthesis with existing datasets, NGEE Arctic provided an enhanced knowledge base for multi-scale modeling and contributed to improved process representation at global pan-Arctic scales within the Department of Energy's Earth system Model (the Energy Exascale Earth System Model, or E3SM), and specifically within the E3SM Land Model component (ELM).

54 ENVIRONMENTAL SCIENCES↗

Flow Components in a NaK Test Loop Designed to Simulate Conditions in a Nuclear Surface Power Reactor

A test loop using NaK as the working fluid is presently in use to study material compatibility effects on various components that comprise a possible nuclear reactor design for use on the lunar surface. A DC electromagnetic (EM) pump has been designed and implemented as a means of actively controlling the NaK flow rate through the system and an EM flow sensor is employed to monitor the developed flow rate. These components allow for the matching of the flow rate conditions in test loops with those that would be found in a full-scale surface-power reactor. The design and operating characteristics of the EM pump and flow sensor are presented. In the EM pump, current is applied to a set of electrodes to produce a Lorentz body force in the fluid. A measurement of the induced voltage (back-EMF) in the flow sensor provides the means of monitoring flow rate. Both components are compact, employing high magnetic field strength neodymium magnets thermally coupled to a water-cooled housing. A vacuum gap limits the heat transferred from the high temperature NaK tube to the magnets and a magnetically-permeable material completes the magnetic circuit. The pump is designed to produce a pressure rise of 5 psi, and the flow sensor's predicted output is roughly 20 mV at the loop's nominal flow rate of 0.5 GPM.

Polzin, Kurt A.↗

Multi-Channel Electronically Scanned Cryogenic Pressure Sensor And Method For Making Same

A miniature, multi-channel, electronically scanned pressure measuring device uses electrostatically bonded silicon dies in a multi-element array. These dies are bonded at specific sites on a glass, pre-patterned substrate. Thermal data is multiplexed and recorded on each individual pressure measuring diaphragm. The device functions in a cryogenic environment without the need of heaters to keep the sensor at constant temperatures.

Chapman, John J.↗

Overview of NASA Earth Observing Systems Terra and Aqua Moderate Resolution Imaging Spectroradiometer Instrument Calibration Algorithms and On-Orbit Performance

Since launch, the Terra and Aqua moderate resolution imaging spectroradiometer (MODIS) instruments have successfully operated on-orbit for more than 9 and 6.5 years, respectively. Iv1ODIS, a key instrument for the NASA's Earth Observing System (EOS) missions, was designed to make continuous observations for studies of Earth's land, ocean, and atmospheric properties and to extend existing data records from heritage earth-observing sensors. In addition to frequent global coverage, MODIS observations are made in 36 spectral bands, covering both solar reflective and thermal emissive spectral regions. Nearly 40 data products are routinely generated from MODIS' observations and publicly distributed for a broad range of applications. Both instruments have produced an unprecedented amount of data in support of the science community. As a general reference for understanding sensor operation and calibration, and thus science data quality, we ;provide an overview of the MODIS instruments and their pre-launch calibration and characterization, and describe their on-orbit calibration algorithms and performance. On-orbit results from both Terra and Aqua MODIS radiometric, spectral, and "spatial calibration are discussed. Currently, both instruments, including their on-board calibration devices, are healthy and are expected to continue operation for several }rears to come.

Xiong, Xiaoxiong↗

Enhanced micro-pocket fission detector for high temperature reactor evaluations - 259

A collaboration between the Idaho National Laboratory (INL), the Kansas State University (KSU), and the French Atomic Energy Agency, Commissariat a l'energie Atomique et aux Energies Alternatives, (CEA), has been initiated by the Nuclear Energy Enabling Technologies (NEET) Advanced Sensors and Instrumentation (ASI) program for developing and testing High Temperature Micro-Pocket Fission Detectors (HT MPFD), which are compact fission chambers capable of simultaneously measuring thermal neutron flux, fast neutron flux and temperature within a single package for temperatures up to 800 deg. C. The MPFD technology utilizes small, multi-purpose, robust, in-core fission chambers and can be configured with a thermocouple. The small size, variable sensitivity, and increased accuracy of the MPFD technology represent a revolutionary improvement over current methods used to support irradiations in US Material Test Reactors (MTRs). Previous research conducted through NEET ASI has shown that the MPFD technology could be made robust and was successfully tested in a reactor core. In addition, the accomplishments of this project have attracted independent funding from other Department of Energy Office of Nuclear Energy (DOE-NE) programs for MTR irradiations of the MPFD technology. (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

STS-103 Flight Day 5 Highlights and Crew Activities Report

Highlights of the fifth day of the STS-103 mission on board the space shuttle Discovery are shown in this videotape. The mission was led by Commander Curtis L. Brown, with Pilot Scott J Kelly, and Mission Specialists Steven L. Smith, Jean-Francois Clervoy, John M. Grunsfeld, Michael Foale, and Claude Nicollier. The main purpose of the mission was to service the Hubble Space Telescope (HST). The primary objective of the mission was to replace all six of the gyroscopes that make up the three Rate Sensor Units. In addition the Astronauts installed a new computer. During the 5th day Michael Foale and Claude Nicollier performed the servicing of the HST in an 8 hour 10 minute Extravehicular Activity (EVA). The servicing included the removal of the old computer and the installation of a new, faster computer with more memory. They also installed a new outer thermal layer to protect the computer. After this was finished the astronauts replaced one of the Fine Guidance Sensors (FGS), an optical sensor which allows NASA to point the telescope in the desired direction. The video includes actual live views of the HST in the shuttle's service bay, and footage of the repair and servicing EVA.

Source record↗

Results of Use of Heat Flux Sensors on Liquid Hydrogen Tanks

Heat flux sensors were used to characterize the performance of insulation on the Structural Heat Intercept, Insulation, and Vibration Evaluation Rig (SHIIVER), a large-scale test article designed to simulate upper stage cryogenic propellant tank thermal performance in simulated space environments. Usually, the insulation heat loads are derived from calculations removing all other heat sources and attributing the residual heat load to the insulation system. Testing for SHIIVER included the tank being just insulated with spray-on-foam insulation as well as covering the domes with multilayer insulation while leaving the barrel section insulated with spray-on-foam. Heat flux sensors were located at multiple locations on both domes as well as on the barrel section of the tank. Results from the SHIIVER testing using the heat flux sensors are compared to other calculated heat inputs for both liquid nitrogen and liquid hydrogen testing as a function of tank fill level. Further investigation into the transient nature of the SHIIVER testing including the heat flux sensors provided insight into heat flow patterns that may not have been otherwise seen using temperature sensors and calculated insulation heat loads. While the demonstrated uncertainties in the absolute values in the heat flux sensors are high, the values and the trends match well with other calculation methods. The results of SHIIVER allow for the use of heat flux sensors for measurements of insulation performance and dynamic system thermal response for future applications.

Cryogenic Fluid Management↗

Results of Use of Heat Flux Sensors on Liquid Hydrogen Tanks

ABSTRACT: Heat flux sensors were used to characterize the performance of insulation on the Structural Heat Intercept, Insulation, and Vibration Evaluation Rig (SHIIVER), a large-scale test article designed to simulate upper stage cryogenic propellant tank thermal performance in simulated space environments. Usually, the insulation heat loads are derived from calculations removing all other heat sources and attributing the residual heat load to the insulation system. Testing for SHIIVER included the tank being just insulated with spray-on-foam insulation as well as covering the domes with multilayer insulation while leaving the barrel section insulated with spray-on-foam. Heat flux sensors were located at multiple locations on both domes as well as on the barrel section of the tank. Results from the SHIIVER testing using the heat flux sensors are compared to other calculated heat inputs for both liquid nitrogen and liquid hydrogen testing as a function of tank fill level. Further investigation into the transient nature of the SHIIVER testing including the heat flux sensors provided insight into heat flow patterns that may not have been otherwise seen using temperature sensors and calculated insulation heat loads. While the demonstrated uncertainties in the absolute values in the heat flux sensors are high, the values and the trends match well with other calculation methods. The results of SHIIVER allow for the use of heat flux sensors for measurements of insulation performance and dynamic system thermal response for future applications.

Cryogenic Fluid Management↗

Commercial Non-Dispersive Infrared Spectroscopy Sensors for Sub-Ambient Carbon Dioxide Detection

Carbon dioxide produced through respiration can accumulate rapidly within closed spaces. If not managed, a crew's respiratory rate increases, headaches and hyperventilation occur, vision and hearing are affected, and cognitive abilities decrease. Consequently, development continues on a number of CO2 removal technologies for human spacecraft and spacesuits. Terrestrially, technology development requires precise performance characterization to qualify promising air revitalization equipment. On-orbit, instrumentation is required to identify and eliminate unsafe conditions. This necessitates accurate in situ CO2 detection. Recursive compensation algorithms were developed for sub-ambient detection of CO2 with commercial off-the-shelf (COTS) non-dispersive infrared (NDIR) sensors. In addition, the source of the exponential loss in accuracy is developed theoretically. The basis of the loss can be explained through thermal, Doppler, and Lorentz broadening effects that arise as a result of the temperature, pressure, and composition of the gas mixture under analysis. The objective was to develop a mathematical routine to compensate COTS CO2 sensors relying on NDIR over pressures, temperatures, and compositions far from calibration conditions. The routine relies on a power-law relationship for the pressure dependency of the sensors along with an equivalent pressure to account for the composition dependency. A Newton-Raphson iterative technique solves for actual carbon dioxide concentration based on the reported concentration. Moreover, first principles routines were established to predict mixed-gas spectra based on sensor specifications (e.g., optical path length). The first principles model can be used to parametrically optimize sensors or sensor arrays across a wide variety of pressures/temperatures/ compositions. In this work, heuristic scaling arguments were utilized to develop reasonable compensation techniques. Experimental results confirmed this approach and provided evidence that composition broadening significantly alters spectra when pressure is reduced. Consequently, a recursive compensation technique was developed with the Newton-Raphson method, which was subsequently verified through experimentation.

Swickrath, Michael J.↗

Advanced instrumentation and analysis methods for in-pile thermal and nuclear measurements: from out-of-pile studies to irradiation campaigns

Research and development on nuclear fuel behavior under irradiations and accelerated ageing of structure materials is a key issue for sustainable nuclear energy in order to meet specific needs by keeping the best level of safety. A new Material Testing Reactor (MTR), the Jules Horowitz Reactor (JHR) currently under construction in the South of France in the CEA Cadarache research centre will offer a real opportunity to perform R and D programs and hence will crucially contribute to the selection, optimization and qualification of innovative materials and fuels. To perform such programs advanced accurate and innovative experiments, irradiation devices that contain material and fuel samples are required to be set up inside or beside the reactor core. These experiments needs beforehand in situ and on line sophisticated measurements to accurately reach specific and determining parameters such as thermal and fast neutron fluxes, nuclear heating and temperature conditions to precisely monitor and control the conducted assays. Consequently, since 2009 CEA and Aix-Marseille University collaborate in order to design and develop a new multi-sensor device which will be dedicated to measuring profiles of such conditions inside the experimental channels of the JHR. These works are performed in the framework of two complementary joint research programs called MAHRI-BETHY and INCORE. These programs couple experimental studies carried out both out-of nuclear fluxes (in laboratory) and under irradiation conditions (in OSIRIS MTR reactor in France and MARIA MTR reactor in Poland) with numerical works realized by thermal simulations (CAST3M code) and Monte Carlo simulations (MCNP code). These programs deal with three main aims. The first one corresponds to the design and/or the test of new in-pile instrumentation. The second one concerns the development of advanced calibration procedures in particular in the case of one specific sensor: a differential calorimeter used to quantify nuclear heating. The last one consists in the development of accurate measurement and analysis methods. The paper will be dedicated to a complete review of the experimental and numerical works performed since 2009 thanks to two parts. The first part will detail a new thermal approach implemented to improve nuclear heating measurements by radiometric calorimeters. New experimental tools (calorimeter prototypes and set-ups such BETHY Bench) developed to perform preliminary out-of-pile studies under suitable conditions will be presented (temperature and velocity of the external cooling fluid, heat source localization and intensity inside the calorimetric cells). Then the response of two kinds of sensors, their calibrations curves and their thermal behaviors will be compared for various parameters. Finally validated numerical thermal and Monte Carlo works will be discussed to propose new improvements. The second parts of the paper will focus on works realized in order to design, develop and test the first prototype of the multi-sensor device called CARMEN [7-9]. The two mock-ups dedicated respectively to neutron measurements and photon measurements will be detailed. The results obtained during two irradiation campaigns inside the periphery of OSIRIS reactor will be shown. The new analysis method will be discussed. (authors)

21 SPECIFIC NUCLEAR REACTORS AND ASSOCIATED PLANTS↗

A New Insight into Cross-Sensitivity to Humidity of SnO 2 Sensor

Here, the efficiency of gas sensors varies enormously from fundamental study to practical application. This big gap comes mainly from the complex and unpredictable effect of atmospheric environment, especially in humidity. Here, the cross-sensitivity to humidity of a SnO 2 sensor from local structural and lattice evolutions is studied. The sensing response of ethanol is found to be efficiently activated by adsorbing trace of water but inhibited as humidity increases. By X-ray diffraction, pair distribution function of synchrotron and ab initio calculations, the independent effect of water and ethanol on lattice and local structure are clearly revealed, which elucidate the intricate sensing reactions. The formation of hydrogen bonds and repulsion of ethoxides play key roles in the structural distortions, and also in adsorption energies that are critical to the sensitive behavior. The results show the sensor performance coupled with local structural evolution, which provides a new insight into the controversial effects of humidity on SnO 2 sensors.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

Clustering and statistical analyses of air-conditioning intensity and use patterns in residential buildings

Energy conservation in residential buildings has gained increased attention due to its large portion of global energy use and potential of energy savings. Occupant behavior has been recognized as a key factor influencing the energy use and load diversity in buildings, therefore more realistic and accurate air-conditioning (AC) operating schedules are imperative for load estimation in equipment design and operation optimization. With the development of sensor technology, it became easier to access an increasing amount of heating/cooling data from thermal energy metering systems in residential buildings, which provides another possible way to understand building energy usage and occupant behaviors. However, except for cooling energy consumption benchmarking, there currently lacks effective and easy approaches to analyze AC usage and provide actionable insights for occupants. To fill this gap, this study proposes clustering analysis to identify AC use patterns of residential buildings, and develops new key performance indicators (KPIs) and data analytics to explore the AC operation characteristics using the long-term metered cooling energy use data, which is of great importance for inhabitants to understand their thermal energy use and save energy cost through adjustment of their AC use behavior. We demonstrate the proposed approaches in a residential district comprising 300 apartments, located in Zhengzhou, China. Main outcomes include: Representative AC use patterns are developed for three room types of residential buildings in the cold climate zone of China, which can be used as more realistic AC schedules to improve accuracy of energy simulation; Distributions of KPIs on household cooling energy usage are established, which can be used for household AC use intensity benchmarking and performance diagnoses.

32 ENERGY CONSERVATION, CONSUMPTION, AND UTILIZATI↗

A surface acoustic wave hydrogen sensor with tin doped indium oxide layers for intermediate temperatures

We report high temperature surface acoustic wave (SAW) gas sensors with conducting sensing layers require tuning of the sheet conductivity for optimal response. Conducting metal oxides are attractive sensing materials for their tunable electronic properties and high thermal stability, amongst others. Here, we have investigated the application of indium oxide (IO) and indium tin oxide (ITO) films on langasite (LGS)-based SAW reflective delay line sensor devices for monitoring hydrogen at 350 °C. Specifically, we modeled the effect of the IO and ITO sensing layer thickness on the wave velocity, attenuation, and effective electromechanical coefficient. This was followed by an experimental demonstration of tuning of the ITO film sheet conductivity by controlling the dopant concentration and yielding an improvement in the sensor sensitivity. The current study provides a pathway towards the development of conductivity-based sensing layers for high temperature SAW gas sensors with improved sensitivity.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗