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At least 1,351 records · Page 75

The characterization of a crack-tip field

The stress intensity factor, K, has been successfully used as a measure of fracture toughness, and stress intensity factor range, Delta K, correlates well with the fatigue crack growth rate. This paper gives a deductive logic to demonstrate rigorously that, in the case of small-scale yielding, K and Delta K are capable of characterizing the elastic-plastic crack-tip field both under a monotonic loading and cyclic fatigue loading. This capability to characterize the entire crack-tip field is the underlying reason for the successful application of K and Delta K to linear fracture mechanics.

Liu, H. W.↗

Characterization and calibration of the EOIM-III flight mass spectrometer in a high velocity oxygen atom beam

Calibration and characterization of the quadrupole mass spectrometer component of the Evaluation of Oxygen Effects on Materials III (EOIM-III) space-flight experiment are reported in this paper. A high-velocity atom beam system was used to characterize the response of the flight mass spectrometer to high velocity oxygen atoms as well as the reaction/scattering products formed when the atom beam struck a surface. Carbon dioxide, carbon monoxide, and water were observed to form in the mass spectrometer whenever high velocity oxygen atoms were present. The major gaseous products formed from high-velocity atom-beam polymer reactions were easily detected and identified.

Koontz, S. L.↗

Theoretical characterization of the potential energy surface for H + N2 yields HN2. III - Calculations for the excited state surfaces

Additional calculations which characterize potential energy sources (PESs) for the excited 3A-double-prime state, for a bound 2(2A-prime) state, for HN2(+), and for the Rydberg states associated with HN2(+). It is anticipated that these excited state PESs will be important in interpreting and designing experiments to characterize the ground state HN2 species via neutralized ion beam techniques.

Walch, Stephen P.↗

Synthesis and characterization of polyamide-imides

The synthesis and characterization of polyamide-imides (PAI) derived from four different dianhydrides and three isomers of diaminobenzanilide are discussed with emphasis on the effect of combining an amide linkage in the diamine portion with other bridging groups in the dianhydride portion of the polymer backbone. It is noted that all of the amide-imide polymers exhibit high-glass transition temperatures, high thermooxidative stability, and a relatively good solvent resistance. These aromatic PAIs are characterized by high thermal stability due to chain stiffness, crystallinity, and intermolecular hydrogen bonding, and are considered to be good candidates as high-temperature films, coatings, and fibers for aerospace applications.

Dezern, James F.↗

Characterization of magneto-optical media

Amorphous rare earth-transition metal (RE-TM) alloys and compositionally modulated TM/TM films were characterized in terms of their magnetic, magneto-optic, and galvanomagnetic properties. The loop tracer, vibrating sample magnetometer (VSM), and Rutherford Backscattering (RBS) facility were used to characterize and analyze the various properties of these magneto-optical storage media. Kerr effect, ellipticity, coercivity, and anisotropy at various temperatures, magnetoresistance, and resistivity are among the properties measured in Co/Pt films, Co/Pd films, and TbFeCo films.

Hajjar, Roger A.↗

Fluorescence microscopy for the characterization of structural integrity

The absorption characteristics of light and the optical technique of fluorescence microscopy for enhancing metallographic interpretation are presented. Characterization of thermally sprayed coatings by optical microscopy suffers because of the tendency for misidentification of the microstructure produced by metallographic preparation. Gray scale, in bright field microscopy, is frequently the only means of differentiating the actual structural details of porosity, cracking, and debonding of coatings. Fluorescence microscopy is a technique that helps to distinguish the artifacts of metallographic preparation (pullout, cracking, debonding) from the microstructure of the specimen by color contrasting structural differences. Alternative instrumentation and the use of other dye systems are also discussed. The combination of epoxy vacuum infiltration with fluorescence microscopy to verify microstructural defects is an effective means to characterize advanced materials and to assess structural integrity.

Street, Kenneth W.↗

Nondestructive Structural Damage Detection in Flexible Space Structures Using Vibration Characterization

Spacecraft are susceptible to structural damage over their operating life from impact, environmental loads, and fatigue. Structural damage that is not detected and not corrected may potentially cause more damage and eventually catastrophic structural failure. NASA's current fleet of reusable spacecraft, namely the Space Shuttle, has been flown on several missions. In addition, configurations of future NASA space structures, e.g. Space Station Freedom, are larger and more complex than current structures, making them more susceptible to damage as well as being more difficult to inspect. Consequently, a reliable structural damage detection capability is essential to maintain the flight safety of these structures. Visual inspections alone can not locate impending material failure (fatigue cracks, yielding); it can only observe post-failure situations. An alternative approach is to develop an inspection and monitoring system based on vibration characterization that assesses the integrity of structural and mechanical components. A methodology for detecting structural damage is presented. This methodology is based on utilizing modal test data in conjunction with a correlated analytical model of the structure to: (1) identify the structural dynamic characteristics (resonant frequencies and mode shapes) from measurements of ambient motions and/or force excitation; (2) calculate modal residual force vectors to identify the location of structural damage; and (3) conduct a weighted sensitivity analysis in order to assess the extent of mass and stiffness variations, where structural damage is characterized by stiffness reductions. The approach is unique from other existing approaches in that varying system mass and stiffness, mass center locations, the perturbation of both the natural frequencies and mode shapes, and statistical confidence factors for structural parameters and experimental instrumentation are all accounted for directly.

Ricles, James M.↗

Characterization of selected LDEF polymer matrix resin composite materials

The characterization of selected graphite fiber reinforced epoxy (934 and 5208) and polysulfone (P1700) matrix resin composite materials which received 5 years and 10 months of exposure to the LEO environment on the Long Duration Exposure Facility is reported. Resin loss and a decrease in mechanical performance as well as dramatic visual effects were observed. However, chemical characterization including infrared, thermal, and selected solution property measurements showed that the molecular structure of the polymeric matrix had not changed significantly in response to this exposure. The potential effect of a silicon-containing molecular contamination of these specimens is addressed.

Young, Philip R.↗

Automated site characterization for robotic sample acquisition systems

A mobile, semi-autonomous vehicle with multiple sensors and on-board intelligence is proposed for performing preliminary scientific investigations on extraterrestrial bodies prior to human exploration. Two technologies, a hybrid optical-digital computer system based on optical correlator technology and an image and instrument data analysis system, provide complementary capabilities which might be part of an instrument package for an intelligent robotic vehicle. The hybrid digital-optical vision system could perform real-time image classification tasks using an optical correlator with programmable matched filters under control of a digital microcomputer. The data analysis system would analyze visible and multiband imagery to extract mineral composition and textural information for geologic characterization. Together these technologies would support the site characterization needs of a robotic vehicle for both navigational and scientific purposes.

Scholl, Marija S.↗

Characterization of elastic-viscoplastic properties of an AS4/PEEK thermoplastic composite

The elastic-viscoplastic properties of an AS4/PEEK (APC-2) thermoplastic composite were characterized at 24 C (75 F) and 121 C (250 F) by using a one-parameter viscoplasticity model. To determine the strain-rate effects, uniaxial tension tests were performed on unidirectional off-axis coupon specimens with different monotonic strain rates. A modified Bodner and Partom's model was also used to describe the viscoplasticity of the thermoplastic composite. The experimental results showed that viscoplastic behavior can be characterized quite well using the one-parameter overstress viscoplasticity model.

Yoon, K. J.↗

Characterization of elastic-plastic behavior of AS4/PEEK thermoplastic composite for temperature variation

Inelastic and strength properties of AS4/PEEK composites were characterized with respect to temperature variation by using a one-parameter orthotropic plasticity model and a one-parameter failure criterion. Simple uniaxial off-axis tension tests were performed on coupon specimens of unidirectional AS4/PEEK thermoplastic composite at various temperatures. To avoid the complication caused by the extension-shear coupling effect in off-axis testing, new tabs were designed and used on the test specimens. Experimental results showed that the nonlinear behavior of constitutive relations and the strength can be characterized quite well using the one-parameter plasticity model and the failure criterion, respectively.

Sun, C. T.↗

Characterization and classification of sea ice in polarimetric SAR data

A more detailed characterization of the apparent thin ice types in the multifrequency, multipolarization synthetic aperture radar (SAR) dataset acquired during a campaign for validation of the DMSP SSM/I radiometer ice products is given. The emphasis is on providing a more detailed characterization of the signatures of apparent thin ice types observed in this data and the utility of these signatures for ice type classification purposes. The statistical characteristics of these signatures and their dependence on system calibration are summarized. Implications of these observations for sea ice scattering models are briefly discussed.

Kwok, R.↗

Characterizing mode I fatigue delamination of composite materials

Two techniques for characterizing fatigue delamination in double cantilever beams, the delamination growth onset method and the delamination growth and arrest method, are evaluated. Two glass/epoxy systems, S2/SP250 and S2/CE9000, were tested at R = 0.1 and R = 0.5. The values of the strain energy release rate threshold Delta G(Ith) for no onset of delamination growth until one million cycles were compared with the values of Delta G(I) at delamination arrest. The values at arrest were consistently higher because fiber bridging occurred in the tests. Normalizing Delta G(I) by the mode I value of interlaminar fracture toughness G(Ir) at the corresponding delta A gave values of Delta G(I)/G(Ir) at delamination arrest which were closer to the threshold values obtained from the Delta G-N technique. However, this normalization did not represent a generic materials characterization technique and did not allow for delamination onset predictions.

Martin, Roderick H.↗

Laboratory calibration and characterization of video cameras

Some techniques for laboratory calibration and characterization of video cameras used with frame grabber boards are presented. A laser-illuminated displaced reticle technique (with camera lens removed) is used to determine the camera/grabber effective horizontal and vertical pixel spacing as well as the angle of nonperpendicularity of the axes. The principal point of autocollimation and point of symmetry are found by illuminating the camera with an unexpanded laser beam, either aligned with the sensor or lens. Lens distortion and the principal distance are determined from images of a calibration plate suitably aligned with the camera. Calibration and characterization results for several video cameras are presented. Differences between these laboratory techniques and test range and plumb line calibration are noted.

Burner, A. W.↗

Preliminary characterization of a water vaporizer for resistojet applications

A series of tests was conducted to explore the characteristics of a water vaporizer intended for application to resistojet propulsion systems. The objectives of these tests were to (1) observe the effect of orientation with respect to gravity on vaporizer stability, (2) characterize vaporizer efficiency and outlet conditions over a range of flow rates, and (3) measure the thrust performance of a vaporizer/resistojet thruster assembly. A laboratory model of a forced-flow, once-through water vaporizer employing a porous heat exchange medium was built and characterized over a range of flow rates and power levels of interest for application to water resistojets. In a test during which the vaporizer was rotated about a horizontal axis normal to its own axis, the outlet temperature and mass flow rate through the vaporizer remained steady. Throttlability to 30 percent of the maximum flow rate tested was demonstrated. The measured thermal efficiency of the vaporizer was near 0.9 for all tests. The water vaporizer was integrated with an engineering model multipropellant resistojet. Performance of the vaporizer/thruster assembly was measured over a narrow range of operating conditions. The maximum specific impulse measured was 234 s at a mass flow rate and specific power level (vaporizer and thruster combined) of 154 x 10(exp-6)kg/s and 6.8 MJ/kg, respectively.

Morren, W. Earl↗

Physical interpretation and development of ultrasonic nondestructive evaluation techniques applied to the quantitative characterization of textile composite materials

The development and implementation of advanced ultrasonic nondestructive evaluation methods applied to the characterization of composite materials requires a better understanding of the physics underlying the interaction of ultrasound with the material. The purpose of this investigation is to identify and characterize the features of complex, three dimensional materials that limit the ability of ultrasound to detect flaws in this broad class of emerging materials. In order to explore the interaction of ultrasound with such complex media, we investigate the characteristics of ultrasonic fields which have propagated through samples with complex geometries and/or internal architecture. We focus on the physics that underlies the detection of flaws in such materials.

Miller, James G.↗

Capacitive skin characterization

NASA is currently involved in research that utilizes a capacitive sensor that is used for proximity detection of objects. This sensor is sensitive to conductive and dielectric materials including metal objects and humans. The range of the sensor has been found to be about twelve inches. It is the goal of this research project to further characterize the sensor so that it can be tailored to specific requirements. The characterization of the sensor should be with respect to shield size, sensor size, object size, and object distance. The method of finite elements to calculate the capacitance of the sensor while varying different parameters was used. Each of the parameters was varied in turn, often by selecting data points from different runs. The plotted results are shown and an apparent functionality developed for each.

Mcconnell, Robert↗

Characterization of radiation-induced damage in high performance polymers by electron paramagnetic resonance imaging spectroscopy

The potential for long-term human activity beyond the Earth's protective magnetosphere is limited in part by the lack of detailed information on the effectiveness and performance of existing structural materials to shield the crew and spacecraft from highly penetrating space radiations. The two radiations of greatest concern are high energy protons emitted during solar flares and galactic cosmic rays which are energetic ions ranging from protons to highly oxidized iron. Although the interactions of such high-energy radiations with matter are not completely understood at this time, the effects of the incident radiation are clearly expected to include the formation of paramagnetic spin centers via ionization and bond-scission reactions in the molecular matrices of structural materials. Since this type of radiation damage is readily characterized by Electron Paramagnetic Resonance (EPR) spectroscopy, the NASA Langley Research Center EPR system was repaired and brought on-line during the 1991 ASEE term. A major goal of the 1992 ASEE term was to adapt the existing core of the LaRC EPR system to meet the requirements for EPR Imaging--a powerful new technique which provides detailed information on the internal structure of materials by mapping the spatial distribution of unpaired spin density in bulk media. Major impetus for this adaptation arises from the fact that information derived from EPRI complements other methods such as scanning electron microscopy which primarily characterize surface phenomena. The modification of the EPR system has been initiated by the construction of specially designed, counterwound Helmholtz coils which will be mounted on the main EPR electromagnet. The specifications of the coils have been set to achieve a static linear magnetic field gradient of 10 gauss/mm/amp along the principal (Z) axis of the Zeeman field. Construction is also in progress of a paramagnetic standard in which the spin distribution is known in all three dimensions. This sample will be used to assess the linearity of the magnetic field gradient and to ensure authentic image reconstruction. A second major task was to secure the computer capability to enable image reconstruction from projection data generated by the magnetic field gradients. To this end, commercially available and public domain software packages which perform inverse Fourier Transform and convoluted (filtered) back projection functions are being integrated into the existing EPR data processing system.

Suleman, Naushadalli K.↗