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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,351 records · Page 75
All sourcesNASA NTRSDOE OSTI
DOE OSTI2016

Analytical results from routine DSSHT and SEHT monthly samples

Strip Effluent Hold Tank (SEHT) and Decontaminated Salt Solution Hold Tank (DSSHT) samples from several of the “microbatches” of Integrated Salt Disposition Project (ISDP) Salt Batch (“Macrobatch”) 8B have been analyzed for 238 Pu, 90 Sr, 137 Cs, cations (Inductively Coupled Plasma Emission Spectroscopy - ICPES), and anions (Ion Chromatography Anions - IC-A). The analytical results from the current microbatch samples are similar to those from previous macrobatch samples. The Cs removal continues to be excellent, with decontamination factors (DF) averaging 22,100 (114% RSD). The bulk chemistry of the DSSHT and SEHT samples does not show any signs of unusual behavior, other than lacking the anticipated degree of dilution that is calculated to occur during Modular Caustic-Side Solvent Extraction Unit (MCU) processing.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2019

Module Level Exposure and Evaluation Test (MLEET) for Real- world and Laboratory-based PV Modules: Common Data and Analytics for Quantitative Cross-correlation and Validation

Our objective is to develop a set of lifetime performance prediction models for PV modules. Models were developed based on common I-V, P mp datastreams from modules under outdoor (real-world) exposure and indoor (laboratory-based) accelerated exposures and temporal analytics. These common datastreams that span both indoor and outdoor exposures were supplemented with additional information such as meteorology data, climate and PV module make/model and module specifications. The predictive models were developed using a stressor/mechanism/response framework in which all data are categorized as stressor, mechanism or performance variables and are represented as time-series datastreams. We develop and validate these accelerated indoor exposures and evaluation tests and models and cross-correlate the temporal signatures of PV module degradation mechanisms in the I-V, P mp time-series between outdoor and accelerated indoor tests. The predictive test and model specify indoor and outdoor exposure and data acquisition criteria, variable selection, and temporal duration and variance.

14 SOLAR ENERGY↗
DOE OSTI2019

Determination of cis,cis- and cis,trans- Muconic Acid from Biological Conversion: Laboratory Analytical Procedure (LAP)

Muconic acid is an important platform molecule for production of bio-based polymers. To date, cis,cis-muconic acid (ccMA) has been produced from multiple types of carbon sources including carbohydrates and aromatic compounds via cultivation with genetically engineered microbes. Accurate analysis of muconic acid has previously been a challenge due to ccMA isomerization into cis,trans-muconic acid (ctMA). This Laboratory Analytical Procedure (LAP) is used to separately quantify ccMA and ctMA as the total sum of muconic acid present in the liquid fraction of pretreated biological samples.

09 BIOMASS FUELS↗
DOE OSTI2019

Soluble and Particulate Mercury Deployment of Analytical Method for the Savannah River Site Liquid Waste System

Savannah River National Laboratory (SRNL) developed, tested, and deployed in a radiological containment unit (CU) an analytical method for quantifying particulate total mercury and soluble total mercury in radioactive samples such as the those generated by the dilution of Savannah River Site (SRS) High-Level Waste. This method relies on direct mercury analysis and other associated capabilities for matrix independent quantification of total mercury in solids or liquids (i.e., any sample that can be introduced into the instrument oven for pyrolysis to release all mercury for measurement). The matrix independence allows for discreet measurements of the starting sample, the collected particulates and the filtrate liquid, thus enabling a mass balance quality check. For example, an analysis of a diluted sample from the SRS liquid waste system (LWS) resulted in a measured total mercury value of 55.0 mg Hg/L and a nearly matching calculated total mercury value of 55.1 mg Hg/L (± 20% 2σ) from the summation of measured soluble mercury (47.8 mg Hg/L ± 20% 2σ) and measured particulate mercury (7.26 mg Hg/L ± 20% 2σ). The advantages of the particulate-soluble mercury analysis method are: waste minimization using small radioactive liquid volumes, minimal radiological sample processing and reduced handling steps protective of workers (ALARA) and improved data quality, syringe filter technology which eliminates vacuum filtration and the potential loss of volatile species, small diameter filters (13 mm nominal to 25 mm if needed to avoid clogging) and small disposable poly filter holders (no need to clean) which minimize waste, flexibility provided for a range of starting concentrations, particulate-soluble ratios, and sample matrix conditions, soluble and particulate are measured results that, when summed, and are in good agreement with the total mercury measurement.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2020

Analytical Functions for 200 West Pump-and-Treat SCADA Sensor Data

Historical operations at the U.S. Department of Energy’s Hanford Site included disposal of waste fluids to the subsurface in the 200 West Area on the Hanford Central Plateau. Subsequent infiltration of fluids has resulted in groundwater contamination with carbon tetrachloride, nitrate, uranium, technetium-99, and other contaminants. A pump-and-treat (P&T) system, with an extraction/injection well network and an aboveground treatment plant, was implemented as part of interim and final remedies in the 200 West area. The HYPATIA single-page web application (part of the SOCRATES suite) is being developed to provide access to and analysis of chemistry and treatment facility sensor data for this 200 West P&T system. For the web application, analytical algorithms were developed to perform summing, differencing, smoothing, outlier detection, change-point detection, mass flow rate, and injectivity calculations on the data. Candidate algorithms were identified and tested, with the best-performing algorithms then assembled for implementation in HYPATIA. Because HYPATIA is hosted on the Amazon Web Services (AWS) cloud computing platform, algorithms were implemented in a back-end AWS Lambda function that can be called by the HYPATIA front end. The Lambda function applies the requested data processing to specified data via functions written in R, Python, and JavaScript. Development, testing, and review of the data analysis algorithms was completed under an NQA-1 quality program. This new HYPATIA functionality will provide information to support site decisions regarding P&T system performance and optimization.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2020

An Analytical Model of Erosive Wear of BioMass Comminution Components

An analytical erosion model that relates critical process parameters (speed and impingement angle) to critical material attributes of inorganic mineral species in feedstock (density, size, aspect ratio) and substrate (hardness, toughness, and fatigue ductility) was applied to model wear in pretreatment milling operations. Results of the model were compared to experimental measurements of wear produced using the Accelerated Wear Test (AWT) rig at Idaho National Laboratory (INL). Results showed that there is good agreement between predicted and measured performance, and that a quality-by-design (QbD) tool can be developed to predict component reliability based on scientific engineering principles in lieu of trial-and-error approaches.

09 BIOMASS FUELS↗
DOE OSTI2022

MIS Shelf-Life Final Report for Plutonium Oxide Item CAN92 (SSR147) from Rocky Flats Analytical Laboratory Operations

A plutonium/uranium oxide material from the Material Identification and Surveillance (MIS) Program inventory has been studied to determine the gas generation and corrosion behavior in a storage environment. Sample CAN92 represents plutonium/uranium oxides stored in 3013 containers. The material originated in the analytical laboratory at Rocky Flats. This study followed over time the gas pressure and composition of a sample with nominally 0.5 wt% water in a sealed container with an internal volume scaled to 1/400th of the volume of a 3013 container. Gas compositions had been measured periodically over 5 ½ years. The maximum observed gas pressure from gas generation was 117 kPa. The increase over the initial pressure of 77.5 kPa was largely due to the generation of nitrogen and carbon dioxide with minor amounts of hydrogen and nitrous oxide. The internal components of SSR147 were inspected 6.5 years after it was removed from the array. The inside surfaces of the inner bucket exposed to the original sample for 1,937 days had an etched appearance and general corrosion. No pitting was observed on the inner bucket that held the sample.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗
DOE OSTI2021

Development of Analytical Method for Measuring U and Pu Particles by Laser Ablation MC-ICP-MS for the NWAL

This project will develop methodology to identify and analyze U and Pu containing particles using laser ablation MC-ICP-MS. The proposed work will involve: i) setup and optimization of the LA-MC-ICP-MS system, ii) testing and validation by analysis of QC standards, iii) designing analytical protocols for single particles, and iv) developing a data processing system. Ultimately, this project will output a detailed operating procedure documenting the experimental techniques and data processing routines required to perform particle identification and analysis by laser ablation MC-ICP-MS.

07 ISOTOPE AND RADIATION SOURCES↗
DOE OSTI2023

Determination of Total, Organic, and Inorganic Carbon and Total Nitrogen in Biological Cultures and Liquid Fraction Process Samples: Laboratory Analytical Procedure (LAP)

This Laboratory Analytical Procedure (LAP) describes the quantitative determination of total organic carbon, inorganic carbon in whole suspended biological samples and in the cell-free supernatant, by combustion and CO 2 detection with a non-dispersive infrared (NDIR) detector. This allows for distinct reporting of soluble and insoluble organic and inorganic carbon. In addition, this procedure covers the quantitative determination of soluble nitrogen in the cell-free supernatant.

09 BIOMASS FUELS↗
DOE OSTI2013

Determination of Total Lipids as Fatty Acid Methyl Esters: Laboratory Analytical Procedure (LAP)

This Laboratory Analytical Procedure (LAP) covers the determination of total lipids expressed as fatty acid methyl esters (FAME). Results are reported as the percent FAME content based on the dry weight of the sample. The procedure is based on a whole biomass transesterification procedure of lipids to FAME, which eliminates the need for extraction and therefore is able to access all fatty acids in the biomass and represent an accurate reflection of the biofuels potential.

09 BIOMASS FUELS↗
DOE OSTI2024

Enabling Efficient Surveillance, Control, and Automation of Geothermal Operations with Advanced Predictive Analytics

Automation and control of geothermal energy production and operations require reliable and efficient predictive tools. While physics-based simulation offers a comprehensive tool for predicting energy production performance in geothermal systems, predicting the behavior of geothermal reservoirs involves complex multi-physics processes with coupling effects, highly uncertain input parameters and subsurface descriptions. Moreover, building, running, and integrating simulation models into standard model calibration and optimization workflows entail significant technical and computational efforts. An emerging alternative to physics-based simulation is data-driven predictive analytics models that have gained popularity in energy industry. In this report, we develop novel predictive models for integration into real-time fault diagnosis and model predictive control algorithms to improve the efficiency of energy production operations in geothermal reservoirs. The report includes two major research Thrust Areas, that is, the surface power plant and the subsurface reservoir.

15 GEOTHERMAL ENERGY↗
DOE OSTI2025

Real Time Phasor Analytics (RTPA) and RTPA-SCR System Strength Online Tool

This presentation showcases the Real-Time Phasor Analytics (RTPA) framework for monitoring inertia and assessing system strength in power grids. RTPA is an open-source tool designed to standardize access to data from Power Management Units (PMUs) and Phasor Data Concentrators (PDCs). It facilitates real-time connectivity to multiple PDCs in accordance with the IEEE C37.118-2 standard and supports asynchronous data stream integration. Additionally, RTPA can simulate a PDC server streaming C37.118-2 data and provides Python bindings for seamless interaction with the framework, eliminating the need for direct Rust programming.

24 POWER TRANSMISSION AND DISTRIBUTION↗
DOE OSTI2026

Probing Dynamic Phase Changes in Electrochemical Systems with Cryogenic and in Situ Analytical Electron Microscopy (Final Technical Report)

In this project, we focus on the advancement of our newly developed, unique in situ and cryogenic analytical electron microscopy (AEM) techniques and the development of additional high-end capabilities to quantitatively elucidate the mechanisms of resistive state changes in solid-state electrochemical materials for non-volatile, neuromorphic memory. The objectives of the proposed research are (1) to characterize and elucidate the mechanisms by which electronic state changes occur in various solid-state devices to build guiding principles for electrochemically activated smart materials; (2) to advance our understanding of such mechanisms by coupling cryogenic and in situ techniques to control kinetics of the observed mechanisms while mitigating probe-induced damage; and (3) to utilize additional advanced techniques including electron-beam induced current and quantum mechanical simulations in order to identify the underlying fundamental science of such processes, including roles of defect formation and its effect on phase nucleation, as well as dynamics of these processes in the electrochemical systems at the nanometer scale.

25 ENERGY STORAGE↗
DOE OSTI2021

Online Interactive Platform for COVID-19 Literature Visual Analytics: Platform Development Study

Background Papers on COVID-19 are being published at a high rate and concern many different topics. Innovative tools are needed to aid researchers to find patterns in this vast amount of literature to identify subsets of interest in an automated fashion. Objective We present a new online software resource with a friendly user interface that allows users to query and interact with visual representations of relationships between publications. Methods We publicly released an application called PLATIPUS (Publication Literature Analysis and Text Interaction Platform for User Studies) that allows researchers to interact with literature supplied by COVIDScholar via a visual analytics platform. This tool contains standard filtering capabilities based on authors, journals, high-level categories, and various research-specific details via natural language processing and dozens of customizable visualizations that dynamically update from a researcher’s query. Results PLATIPUS is available online and currently links to over 100,000 publications and is still growing. This application has the potential to transform how COVID-19 researchers use public literature to enable their research. Conclusions The PLATIPUS application provides the end user with a variety of ways to search, filter, and visualize over 100,00 COVID-19 publications.</:p>

96 KNOWLEDGE MANAGEMENT AND PRESERVATION↗