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At least 1,333 records · Page 74
All sourcesNASA NTRSDOE OSTI
NASA NTRS1979

Effect of thermally induced porosity on an as-HIP powder metallurgy superalloy

The impact of thermally induced porosity on the mechanical properties of an as-hot-isostatically-pressed and heat treated pressing made from low carbon Astroloy was determined. Porosity in the disk-shape pressing studied ranged from 2.6 percent at the bore to 1.4 percent at the rim. Tensile, yield strength, ductility, and rupture life of the rim of the porous pressing was only slightly inferior to the rim of sound pressings. The strength, ductility, and rupture life of the bore of the porous pressing was severely degraded compared to sound pressings. At strain ranges typical of commercial jet engine designs, the rim of the porous pressing had slightly inferior fatigue life to sound pressings.

Dreshfield, R. L.↗
NASA NTRS1980

Effects of thermally induced porosity on an as-HIP powder metallurgy superalloy

The effect of thermally induced porosity on the mechanical properties of an as-hot-isostatically pressed and heat-treated pressing made from low carbon Astroloy is examined. Tensile, stress-rupture, creep, and low cycle fatigue tests were performed and the results were compared with industrial acceptance criteria. It is shown that the porous pressing has a porosity gradient from the rim to the bore with the bore having 1-1/2% greater porosity. Mechanical properties of the test ring below acceptance level are tensile reduction in area at room temperature and 538 C and time for 0.1% creep at 704 C. It is also found that the strength, ductility, and rupture life of the rim are slightly inferior to those of the rim of the sound pressings, while those of the bore are generally below the acceptable level. At strain ranges typical of commercial aircraft engines, the low cycle fatigue life of the rim of the porous pressings is slightly lower than that of the sound pressings.

Dreshfield, R. L.↗
NASA NTRS1982

Dual-Alloy Disks are Formed by Powder Metallurgy

High-performance disks have widely varying properties from hub to rim. Dual property disk is fabricated using two nickel-base alloys, AF-115 for rim and Rene 95 for hub. Dual-alloy fabrication may find applications in automobiles, earth-moving equipment, and energy conversion systems as well as aircraft powerplants. There is potential for such applications as shafts, gears, and blades.

Harf, F. H.↗
NASA NTRS1981

Powder metallurgy Rene 95 rotating turbine engine parts, volume 2

A Rene 95 alloy as-HIP high pressure turbine aft shaft in the CF6-50 engine and a HIP plus forged Rene 95 compressor disk in the CFM56 engine were tested. The CF6-50 engine test was conducted for 1000 C cycles and the CFM56 test for 2000 C cycles. Post test evaluation and analysis of the CF6-50 shaft and the CFM56 compressor disk included visual, fluorescent penetrant, and dimensional inspections. No defects or otherwise discrepant conditions were found. These parts were judged to have performed satisfactorily.

Wilbers, L. G.↗
NASA NTRS1982

Development of powder metallurgy Al alloys for high temperature aircraft structural applications, phase 2

In this continuing study, the development of mechanically alloyed heat resistant aluminum alloys for aircraft were studied to develop higher strength targets and higher service temperatures. The use of higher alloy additions to MA Al-Fe-Co alloys, employment of prealloyed starting materials, and higher extrusion temperatures were investigated. While the MA Al-Fe-Co alloys exhibited good retention of strength and ductility properties at elevated temperatures and excellent stability of properties after 1000 hour exposure at elevated temperatures, a sensitivity of this system to low extrusion strain rates adversely affected the level of strength achieved. MA alloys in the Al-Li family showed excellent notched toughness and property stability after long time exposures at elevated temperatures. A loss of Li during processing and the higher extrusion temperature 482 K (900 F) resulted in low mechanical strengths. Subsequent hot and cold working of the MA Al-Li had only a mild influence on properties.

Chellman, D. J.↗
NASA NTRS1983

Influence of deflocculant on the isoelectric point of refractory powders: Considerations on the action of deflocculant

Isoelectric point changes in suspensions of refractory materials vis-a-vis the role of deflocculants used in monolithic refractories were investigated by considering the mineral compositions and adsorbed ions in four kinds of clay. Three types of curves represented the relation between the isoelectric point and the deflocculant. The surface charge of clay particles in the suspensions became negative as a result of the deflocculant, since the isoelectric point of suspensions decreased as the deflocculant was added. The isoelectric point changes of calcined alumina were also compared with those of the clays, and a similar phenomenon was observed, except that the deflocculant dispersed the calcined alumina better than it did the clays. A simple model was used to analyze the results.

Naruse, Y.↗
NASA NTRS1984

Powder fed sheared dispersal particle generator

A particle generating system is described which is capable of breaking up agglomerations of particles and producing a cloud of uniform, submicron-sized particles at high pressure and high flow rates. This is achieved by utilizing a tubular structure which has injection microslits on is periphery to accept and disperse the desired particle feed. By suppling a carrying fluid at a pressure, of approximately twice the ambient pressure of the velocimeter's settling chamber, the microslits operate at choked flow conditions. The shearing action of this choked flow is sufficient to overcome interparticle bonding forces, thereby breaking up the agglomerates of the particles feed into individual particles.

Morrisette, E. L.↗
NASA NTRS1984

Photometric properties of powdered sulfur

Particle size, temperature, thermal history, and scattering geometry are shown by the present laboratory investigation of the spectrophotometric properties of three particle-size fractions of sulfur to influence the spectral reflectance of both normal and quenched molten samples of sulfur. A scattering law that consists of a linear combination of lunar-like and Lambertian terms adequately describes the data for all particle sizes. Near opposition, sulfur particles closely follow a Minnaert limb darkening law except where the reflectance is low, as in the strong UV absorption band of the larger particle size fractions. The present data indicate that quantitative comparisons between disk-integrated observations of Io and laboratory measurements of flat sulfur samples are inadequate unless temperature effects and scattering geometry changes are included.

Gradie, J.↗
NASA NTRS1984

Silicon nitride powder

The characteristics and preparation methods of Si3N4 are reviewed. Special emphasis is placed on the correlation between impurities and strength of sintered Si3N4.

Mori, M.↗
NASA NTRS1984

Development of powder metallurgy 2XXX series Al alloys for high temperature aircraft structural applications

The objective of the present investigation was to improve the strength and fracture toughness combination of P/M 2124 Al alloys in accordance with NASA program goals for damage tolerance and fatigue resistance. Two (2) P/M compositions based on Al-3.70 Cu-1.85 Mg-0.20 Mn with 0.12 and 0.60 wt. pct. Zr were selected for investigation. The rapid solidification rates produced by atomization were observed to prohibit the precipitation of coarse, primary Al3Zr in both alloys. A major portion of the Zr precipitated as finely distributed, coherent Al3Zr phases during vacuum preheating and solution heat treatment. The proper balance between Cu and Mg contents eliminated undissolved, soluble constituents such as Al2CuMg and Al2Cu during atomization. The resultant extruded microstructures produced a unique combination of strength and fracture toughness. An increase in the volume fraction of coherent Al3Zr, unlike incoherent Al20Cu2Mn3 dispersoids, strengthened the P/M Al base alloy either directly by dislocation-precipitate interactions, indirectly by a retardation of recrystallization, or a combination of both mechanisms. Furthermore, coherent Al3Zr does not appear to degrade toughness to the extent that incoherent Al20Cu2Mn3 does. Consequently, the addition of 0.60 wt. pct. Zr to the base alloy, incorporated with a 774K (935 F) solution heat treatment temperature, produces an alloy which exceeds all tensile property and fracture toughness goals for damage tolerant and fatigue resistant applications in the naturally aged condition.

Chellman, D. J.↗
NASA NTRS1985

Metallurgical and mechanical phenomena due to rubbing of titanium against sintered powder Nichrome

Metallurgical and mechanical changes occurring during high-speed rubbing of Ti-6Al-4V blade specimens against an abradable Nichrome aircraft engine seal material were studied using optical microscopy, electron microscopy, and microhardness techniques. Evidence of temperatures above the beta transus of Ti-6Al-4V (1000 C) and of thermal hardening was found on blade tips that exhibited undesirable abrading characteristics resulting in high forces of interaction, high temperatures, and smearing. The material within the layer of the corresponding seals was found to be work-hardened to a depth of about 0.1 mm and showed evidence of densification extending to a depth of about 0.5 mm below the rubbed surface. Wear particles produced by rub interactions that generated cleanly abraded seal surfaces were found to be several times larger than those produced during interactions which showed evidence of surface smearing and seal densification.

Zenas, R.↗
NASA NTRS1984

Rapid solidification and dynamic compaction of Ni-base superalloy powders

A Ni-base superalloy containing 13Al-9Mo-2Ta (in at. percent) has been characterized in both the rapidly solidified condition and after dynamic compaction. Dynamically compacted specimens were examined in the as-compacted condition and observations related to current theories of interparticle bonding. In addition, the recrystallization behavior of the compacted material at relatively low temperature (about 0.5-0.75 Tm) was investigated.

Field, R. D.↗
NASA NTRS1985

Designing high frequency ac inductors using ferrite and Molypermalloy Powder Cores (MPP)

The major considerations in the design of high frequency ac inductors are reviewed. Two methods for designing the inductor: the area product method and the core geometry method, are presented. The two major effects of the inductor air gap, fringing flux power loss and increase of inductance, are discussed. Equations for the inductor design and a step-by-step design procedure are given. The use of a lumped air gap or a distributed air gap are discussed and a comparison of the losses resulting from these gaps, together with experimental results are presented.

Mclyman, W. T.↗
NASA NTRS1985

Utilization of Space Shuttle External Tank materials by melting and powder metallurgy

The Crucible Melt Extraction Process was demonstrated to convert scraps of aluminum alloy 2219, used in the Space Shuttle External Tank, into fibers. The cast fibers were then consolidated by cold welding. The X-ray diffraction test of the cast fibers was done to examine the crystallinity and oxide content of the fibers. The compressive stress-strain behavior of the consolidated materials was also examined. Two conceptual schemes which would adapt the as-developed Crucible Melt Extraction Process to the microgravity condition in space were finally proposed.

Chern, T. S.↗
NASA NTRS1985

Development of powder metallurgy 2XXX series Al alloy plate and sheet materials for high temperature aircraft structural applications, FY 1983/1984

The objective of this investigation is to fabricate and evaluate PM 2124 Al alloy plate and sheet materials according to NASA program goals for damage tolerance and fatigue resistance. Previous research has indicated the outstanding strength-toughness relationship available with PM 2124 Al-Zr modified alloy compositions in extruded product forms. The range of processing conditions was explored in the fabrication of plate and sheet gage materials, as well as the resultant mechanical and metallurgical properties. The PM composition based on Al-3.70 Cu-1.85 Mg-0.20 Mn with 0.60 wt. pct. Zr was selected. Flat rolled material consisting of 0.250 in. thick plate was fabricated using selected thermal mechanical treatments (TMT). The schedule of TMT operations was designed to yield the extreme conditions of grain structure normally encountered in the fabrication of flat rolled products, specifically recrystallized and unrecrystallized. The PM Al alloy plate and sheet materials exhibited improved strength properties at thin gages compared to IM Al alloys, as a consequence of their enhanced ability to inhibit recrystallization and grain growth. In addition, the PM 2124 Al alloys offer much better combinations of strength and toughnessover equivalent IM Al. The alloy microstructures were examined by optical metallographic texture techniques in order to establish the metallurgical basis for these significant property improvements.

Chellman, D. J.↗
NASA NTRS1987

Advanced powder metallurgy aluminum alloys via rapid solidification technology, phase 2

Marko's rapid solidification technology was applied to processing high strength aluminum alloys. Four classes of alloys, namely, Al-Li based (class 1), 2124 type (class 2), high temperature Al-Fe-Mo (class 3), and PM X7091 type (class 4) alloy, were produced as melt-spun ribbons. The ribbons were pulverized, cold compacted, hot-degassed, and consolidated through single or double stage extrusion. The mechanical properties of all four classes of alloys were measured at room and elevated temperatures and their microstructures were investigated optically and through electron microscopy. The microstructure of class 1 Al-Li-Mg alloy was predominantly unrecrystallized due to Zr addition. Yield strengths to the order of 50 Ksi were obtained, but tensile elongation in most cases remained below 2 percent. The class 2 alloys were modified composition of 2124 aluminum alloy, through addition of 0.6 weight percent Zr and 1 weight percent Ni. Nickel addition gave rise to a fine dispersion of intermetallic particles resisting coarsening during elevated temperature exposure. The class 2 alloy showed good combination of tensile strength and ductility and retained high strength after 1000 hour exposure at 177 C. The class 3 Al-Fe-Mo alloy showed high strength and good ductility both at room and high temperatures. The yield and tensile strength of class 4 alloy exceeded those of the commercial 7075 aluminum alloy.

Ray, Ranjan↗