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DOE OSTI2025

Novel Preprocessing Techniques for Enhancing Flowability of Miscanthus

Purpose-grown energy crops possess significant potential as promising feedstocks for biofuel and biochemical production. However, similar to other biomass feedstocks, their utilization has been hindered by handling and feeding challenges such as clogging and segregation, which prevent biorefineries from operating at full capacity. These challenges arise primarily due to particle attributes including irregular shape, high flexibility, and high compressibility, leading to interlocking, high compaction, and significant friction under stress consolidation. To enhance operational reliability, it is crucial to focus on preprocessing techniques to address these issues, alongside accurately characterizing the mechanical and physical properties and flow performance of these feedstocks. This study investigates novel preprocessing techniques, including pelletization and torrefaction, to fundamentally alter these particle attributes and improve flowability. Miscanthus, an herbaceous energy crop, was the primary focus of this study. Samples were processed using a Forest Concepts Crumbler rotary shear system and an oscillating multi-stack screen bed to achieve two nominal (baseline) particle sizes: 6mm and 2mm. The study evaluated the efficiency and energy consumption of size reduction, revealing that while 2mm particles required more energy, they exhibited better flowability and higher yield strength compared to 6mm particles. Shear and compression tests assessed the material's shear strength, internal friction, and elastic modulus, while wedge-shaped hopper tests measured the critical arching distance and mass flow rate. The results provide valuable insights into the mechanical properties and processing efficiency of Miscanthus, contributing to the development of a preprocessing framework that enhances energy efficiency and material flowability in bioenergy production. However, further preprocessing and development are required to optimize this framework fully.

09 - BIOMASS FUELS↗

NASA NTRS1991

Using semantic data modeling techniques to organize an object-oriented database for extending the mass storage model

A methodology for optimizing organization of data obtained by NASA earth and space missions is discussed. The methodology uses a concept based on semantic data modeling techniques implemented in a hierarchical storage model. The modeling is used to organize objects in mass storage devices, relational database systems, and object-oriented databases. The semantic data modeling at the metadata record level is examined, including the simulation of a knowledge base and semantic metadata storage issues. The semantic data model hierarchy and its application for efficient data storage is addressed, as is the mapping of the application structure to the mass storage.

Campbell, William J.↗

NASA NTRS1993

HL-20 subsystem design

The NASA Langley Research Center has been developing a lifting-body configuration called the HL-20 for potential application as a personnel launch system orbiter that will provide the crew changeout at the Space Station Freedom. The objectives have been to provide an alternate manned access to space with a more cost-effective, efficient, reliable, and safer system for the routine transportation of people to LEO. The detailed study of this concept includes the subsystem design, flight software sizing, and mass properties that are discussed in this paper. The goals were to develop a subsystem complement to maximize operational efficiency with minimum development costs while using current technology. Subsystem selection and trade studies showed that current technology components will provide the required performance and operational effectiveness. Many of the selected components have Shuttle flight histories or considerable development heritage from other programs that will help minimize development costs.

Stone, H. W.↗

DOE OSTI2024

Toward Mass-Production of Transition Metal Dichalcogenide Solar Cells: Scalable Growth of Photovoltaic-Grade Multilayer WSe2 by Tungsten Selenization

Semiconducting transition metal dichalcogenides (TMDs) are promising for high-specific-power photovoltaics due to their desirable band gaps, high absorption coefficients, and ideally dangling-bond-free surfaces. Despite their potential, the majority of TMD solar cells to date are fabricated in a nonscalable fashion, with exfoliated materials, due to the lack of high-quality, large-area, multilayer TMDs. Here, we present the scalable, thickness-tunable synthesis of multilayer WSe2 films by selenizing prepatterned tungsten with either solid-source selenium at 900 degrees C or H2Se precursors at 650 degrees C. Both methods yield photovoltaic-grade, wafer-scale WSe2 films with a layered van der Waals structure and superior characteristics, including charge carrier lifetimes up to 144 ns, over 14x higher than those of any other large-area TMD films previously demonstrated. Simulations show that such carrier lifetimes correspond to ~22% power conversion efficiency and ~64 W g-1 specific power in a packaged solar cell, or ~3 W g-1 in a fully packaged solar module. The results of this study could facilitate the mass production of high-efficiency multilayer WSe2 solar cells at low cost.

carrier lifetime↗

DOE OSTI2024

Volatility Basis Set Distributions and Viscosity of Organic Aerosol Mixtures: Insights from Chemical Characterization Using Temperature-Programmed Desorption–Direct Analysis in Real-Time High-Resolution Mass Spectrometry

Quantitative assessment of gas-particle partitioning of individual components within complex atmospheric organic aerosols (OA) mixtures is critical for predicting and comprehending the formation and evolution of OA particles in the atmosphere. This investigation leverages previously documented data obtained through a temperature programmed desorption - direct analysis in real time – high resolution mass spectrometry (TPD-DART-HRMS) platform. This methodology facilitates the bottom-up construction of volatility basis set (VBS) distributions for constituents found in three biogenic secondary organic aerosol (SOA) mixtures produced through the ozonolysis of a-pinene, limonene, and ocimene. The apparent enthalpies (ΔH*, kJ mol -1 ) and saturated vapor mass concentrations (C T *, µg∙m -3 ) of individual SOA components, determined as a function of temperature (T, K), facilitated an assessment of changes in VBS distributions and gas-particle partitioning with respect to T and atmospheric total organic mass loadings (tOM, µg∙m -3 ). Further, the VBS distributions reveal distinct differences in volatilities among monomers, dimers, and trimers, enabling their categorization into separate volatility bins. At the ambient temperature of T = 298 K, only monomers efficiently partition between gas and particle phases across a broad range of atmospherically relevant total organic mass loadings (tOM) values of 1–100 µg∙m -3 . Partitioning of dimers and trimers becomes notable only at T > 360 K and T > 420 K, respectively. The viscosity of SOA mixtures is assessed using a bottom-up calculation approach, incorporating the input of elemental formulas, ΔH*, C T *, and particle-phase mass fractions of the SOA components. Through this approach, we are able to accurately estimate the variations in SOA viscosity that result from the evaporation of its components. These variations are, in turn, influenced by atmospherically relevant changes in tOM and T. Comparison of the calculated SOA viscosity and diffusivity values with literature reported experimental results shows close agreement, thereby validating the employed calculation approach. These findings underscore the significant potential for TPD-DART-HRMS measurements in enabling the untargeted analysis of organic molecules within OA mixtures. This approach facilitates quantitative assessment of their gas-particle partitioning and allows for the estimation of their viscosity and condensed-phase diffusion, thereby contributing valuable insights to atmospheric models.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2021

Inertially enhanced mass transport using 3D-printed porous flow-through electrodes with periodic lattice structures

Significance The efficient utilization of electrical energy is an increasingly important challenge, especially as renewable energy sources become cheaper and demand increases. Electrochemical reactors utilizing flow-through electrodes (FTEs) provide an attractive path toward the efficient utilization of electrical energy. Their commercial viability and ultimate adoption hinge on attaining high current densities to drive cost competitiveness. There are limited opportunities for engineering FTE materials, as these are often random, disordered media. Alternatively, three-dimensional (3D)–printed FTEs provide the opportunity to quickly explore the impact of engineered electrode architectures on device performance. We demonstrate that 3D-printed FTEs have the potential to exceed the performance of conventional materials by using the expanded design freedom to engineer the internal flow.

30 DIRECT ENERGY CONVERSION↗

DOE OSTI2023

Comparison of sleep parameters from wrist-worn ActiGraph and Actiwatch devices

Abstract Sleep and physical activity, two important health behaviors, are often studied independently using different accelerometer types and body locations. Understanding whether accelerometers designed for monitoring each behavior can provide similar sleep parameter estimates may help determine whether one device can be used to measure both behaviors. Three hundred and thirty one adults (70.7 ± 13.7 years) from the Baltimore Longitudinal Study of Aging wore the ActiGraph GT9X Link and the Actiwatch 2 simultaneously on the non-dominant wrist for 7.0 ± 1.6 nights. Total sleep time (TST), wake after sleep onset (WASO), sleep efficiency, number of wake bouts, mean wake bout length, and sleep fragmentation index (SFI) were extracted from ActiGraph using the Cole–Kripke algorithm and from Actiwatch using the software default algorithm. These parameters were compared using paired t-tests, Bland–Altman plots, and Deming regression models. Stratified analyses were performed by age, sex, and body mass index (BMI). Compared to the Actiwatch, the ActiGraph estimated comparable TST and sleep efficiency, but fewer wake bouts, longer WASO, longer wake bout length, and higher SFI (all p < .001). Both devices estimated similar 1-min and 1% differences between participants for TST and SFI (β = 0.99, 95% CI: 0.95, 1.03, and 0.91, 1.13, respectively), but not for other parameters. These differences varied by age, sex, and/or BMI. The ActiGraph and the Actiwatch provide comparable absolute and relative estimates of TST, but not other parameters. The discrepancies could result from device differences in movement collection and/or sleep scoring algorithms. Further comparison and calibration is required before these devices can be used interchangeably.

Liu, Fangyu (ORCID:0000000315541478)↗

DOE OSTI2022

Understanding Mass Transport in Copper Electrolyte-Based Dye-Sensitized Solar Cells

Copper redox shuttles, particularly [Cu(tmby) 2 ] 2+/1+ (tmby = bis(4,4',6,6'-tetramethyl-2,2'-bipyridine)), proved to be among the best electrolytes for dye-sensitized solar cells (DSCs), realizing higher power conversion efficiencies both under full sun and indoor illumination than conventional iodide/triiodide and cobalt electrolytes. Even though [Cu(tmby) 2 ] 2+/1+ renders a relatively higher performance, this metal complex is bulky and is limited by mass transport. Since the regeneration of the dye ground state by Cu I and the reaction of Cu II at the counter electrode are comparatively faster processes, the efficiency of DSC involving Cu I /Cu II electrolytes under relatively high light intensities is largely governed by the diffusion of Cu I /Cu II species. Understanding mass transport in these solar cells will enable further improvements in the performance of such copper-based DSCs. Here in the present study, the role of illumination intensity on the photogenerated current and its relationship to mass transport is evaluated using the best cosensitized dye (D35:XY1) and copper electrolyte ([Cu(tmby) 2 ] 2+/1+ ) combination.

14 SOLAR ENERGY↗

NASA NTRS2002

Synthetic Jet Interaction With A Turbulent Boundary Layer Flow

Perhaps one of the more notable advances to have occurred in flow control technology in the last fifteen years is the application of surface-issuing jets for separation control on aerodynamic surfaces. The concept was introduced by Johnston and Night (1990) who proposed using circular jets, skewed and inclined to the wall, to generate streamwise vortices for the purpose of mitigating boundary layer separation. The skew and inclination angles have subsequently been shown to affect the strength and sign of the ensuing vortices. With a non-circular orifice, in addition to skew and inclination, the yaw angle of the major axis of the orifice can influence the flow control effectiveness of the jet. In particular, a study by Chang arid Collins (1997) revealed that a non-circular orifice, yawed relative to the freestream, can be used to control the size and strength of the vortices produced by the control jet. This early work used jets with only a steady injection of mass. Seifert et al. revealed that an unsteady blowing jet, could be as effective at separation control as a steady jet but with less mass flow. Seifert et al. showed that small amplitude blowing oscillations superimposed on a low momentum steady jet Was the most effective approach to delaying separation on a NACA 0015 airfoil at post-stall angles of attack. More recent work suggests that perhaps the most efficient jet control effect comes from a synthetic (oscillatory) jet where the time-averaged mass flux through the orifice is zero, but the net wall normal momentum is non-zero. The control effectiveness of synthetic jets has been demonstrated for several internal and external flow fields used synthetic jet control on a thick, blunt-nosed airfoil to delay stall well beyond the stall angles for the uncontrolled airfoil and with a dramatic increase in the lift-to-drag performance. Amitay et al. used an array of synthetic jets to mitigate flow separation in curved and diffusing ducts. While the control effectiveness of synthetic jet actuators in an application setting has been confirmed through a number of studies, the fluid dynamic mechanism by which control is effected is not well understood. Issues like yaw angle arid velocity ratio that have been studied for steady control jets have not been investigated for synthetic jets. Moreover, the role played by the inherently unsteady nature of a synthetic jet in the interaction with the controlled flow is not known. Some recent work by Rinehart and Glazer and Smith suggests that away from tile immediate vicinity of the jet orifice the flow field is steady in the mean, and that the interaction of a synthetic jet and a boundary layer creates a secondary flow in the boundary layer consisting primarily of streamwise vortices.

Smith, Douglas R.↗

NASA NTRS2002

Conceptual Design of an MTF Space Propulsion System

Most fusion propulsion concepts that have been investigated in the past employ some form of inertial or magnetic confinement separately, and are encumbered by the need for advanced drivers (e.g. laser) or steady-state magnetic confinement systems (e.g. superconductors) that have historically resulted in large, massive spacecraft designs. Here we present a comparatively new approach, Magnetized Target Fusion (MTF), which offers a nearer-term avenue for realizing the tremendous performance benefits of fusion propulsion. MTF attempts to combine the favorable attributes of both inertially and magnetically confined fusion to achieve both efficient and low-cost compressional plasma heating and energy confinement. The key advantage of MTF is its less demanding requirements for driver energy and power processing. Additional features include: 1) very low system masses and volumes, 2) relatively low waste heat, 3) substantial utilization of energy from product neutrons, 4) efficient, low peak-power drivers based on existing pulsed power technology, 5) very high Isp , specific power and thrust, and 6) relatively affordable R&D pathways. MTF overcomes many of the problems associated with traditional fusion techniques, thus making it particularly attractive for space applications. Isp greater than 50,000 seconds and specific powers greater than 20 kilowatts/kilogram appear feasible using relatively near-term pulse power and plasma gun technology.

Thio, Y. C. F.↗

NASA NTRS2021

Simultaneous Ice Water Content Measurements at Multiple Locations on the NASA DC-8 Aircraft during the 2018 HIWC RADAR Flight Campaign

Ice water content measurements were made simultaneously at three locations on the NASA DC-8 in natural, glaciated conditions during the 2018 High Ice Water Content RADAR flight campaign. The purpose of these measurements was to further evaluate efficiency factors of hot-wire total water content probes in glaciated conditions and investigate the enhancement of ice crystal concentrations near fuselage surfaces due to flow field inertial effects, and ice crystals impacting the nose, breaking up, and flowing downstream. The total water content measurements were made using either Science Engineering Associates Ice Crystal Detectors or Robust Probes. Three common sensors were mounted on an underwing canister considered to be in near free-flow conditions, a standoff from a fuselage window, and the nose of the fuselage near the pitot probes. The Ice Crystal Detector concave total water content sensor and Robust Probe sensor collection and retention efficiencies were evaluated through comparisons with the underwing Ice Crystal Detector and Robust Probe measurements to the Isokinetic Probe version 2 (IKP2), which provided the reference ice water content measurement. Local ice water content at the nose position was evaluated by comparing ratios of the nose and underwing ice crystal detectors to the IKP2. Local ice water content at the window-standoff location was also evaluated by comparing total water content sensor measurements from the window probes to the measurements made with the underwing and nose probes. The key findings were: (1) the Ice Crystal Detector concave water content sensor efficiency factor to glaciated conditions was similar to previous estimates, but reduced with increased ice crystal median mass diameter; (2) the ice water content at the fuselage nose location near the DC-8 pitot probes was approximately 2.5 times the freestream values—although this estimate is affected by a higher probe efficiency factor due to smaller particles in the debris cloud from impacts upstream of the probe; and (3) the ice water content at the 17 in. standoff from the port window varied from about 50 percent to nearly three times freestream values in a complicated manner. Similar measurement locations are not uncommon on cloud research aircraft, where ice particle measurements may be subject to similar uncertainties.

Aircraft Icing↗

DOE OSTI2023

Operation Optimization using Reinforcement Learning with Integrated Artificial Reasoning Framework

In large and complex systems, operational decision-making requires a systematic analysis with a vast amount of data from both process parameters and component status monitoring. In this paper, we present an integrated artificial reasoning approach for system state transition models that can help operational decision-making with explainable and traceable reasoning. The integrated artificial reasoning framework is a physics-based approach of defining the system structure in a Bayesian network, so we leveraged it in a Markov decision process (MDP) for finding optimal operational solutions. In our proposed framework, the MDP is implemented on a dynamic Bayesian network (DBN), which represents causalities in a system. The multilevel flow modeling was utilized in order to extract these causalities in a more efficient and objective manner. Since multilevel flow modeling is based on the fundamental energy and mass conservation laws, the target system is decomposed into several mass, energy, and information structures, which serve as the basis for a DBN. The MDP consists of the processes of finding a solution for the Bellman equation, which can be derived from the conditional probability equations of the constructed DBN. System operators can capture stochastic system dynamics as multiple subsystem state transitions based on their physical relations and uncertainties coming from the component degradation process or random failures. We analyzed a simplified example system to illustrate finding an optimal operational policy with this approach.

99 GENERAL AND MISCELLANEOUS↗

NASA NTRS1976

A study of efficiency in low resistivity silicon solar cells

A general device-analysis program has been utilized to study the efficiency of silicon solar cells. The analysis is applied to specific geometries of both n(+)-p and n(+)-p-p(+) solar cells, and involves a numerical solution of the basic transport and continuity equations. This approach allows solutions that are free of typical limiting assumptions involved in solving the device equations as well as solutions relating to lifetime, mobility variations, and diffused-region profiles. The analysis includes available empirical information on diffusion length, mobility, and lifetime as a function of doping, as well as a Gaussian profile for the diffused region. Results are presented which illustrate the limitations of efficiency as a function of doping. It is found that the maximum efficiencies for both types of cell converge at lower resistivities to around 16% with air-mass-zero radiation and a single-layer absorbing-SiO antireflecting film. It is also found that the minority-carrier lifetime, both in the n(+) surface and p-type bulk regions, presents serious limitations to conversion efficiency, particularly in the low-resistivity cells.

Dunbar, P. M.↗

NASA NTRS1999

Bandwidth Efficient Wireless Digital Modem Developed

NASA Lewis Research Center has developed a digital approach for broadcasting highfidelity audio (nearly compact disk (CD) quality sound) in the commercial frequencymodulated (FM) broadcast band. This digital approach provides a means of achieving high data transmission rates with low hardware complexity--including low mass, size, and power consumption. Lewis has completed the design and prototype development of a bandwidth-efficient digital modem (modulator and demodulator) that uses a spectrally efficient modulation scheme: 16-ary rectangular quadrature amplitude modulation, or 16- ary QAM. The digital implementation is based strictly on inexpensive, commercial off-theshelf digital signal processing (DSP) hardware to perform up and down conversions and pulse shaping. The digital modem transmits data at rates up to 76 kilobits per second (kbps), which is almost 3 times faster than standard 28.8-kbps telephone modems. In addition, the modem offers improved power and spectral performance, flexible operation, and low-cost implementation.

Kifle, Muli↗

NASA NTRS1977

Evaporative winds in X-ray binaries

Evaporation of gas from the surface of HZ Her by Her X-1 and its implications regarding the mass transfer process are examined further. The powerful soft X-ray flux results in an evaporation rate greater than previous estimates. The evaporative flow is shown to be subsonic at first, with the result that the capture of evaporated gas by Her X-1 may be efficient, and the self-excited wind mechanism is possible. A criterion for stabilization of mass transfer by stellar wind mass loss is derived. Possible mechanisms for the long-period variability of HZ Her are discussed. Evaporative winds are also estimated for Sco X-1 and Cyg X-2 spectra.

Basko, M. M.↗

NASA NTRS2004

The Space Technology 5 Avionics System

The Space Technology 5 (ST5) mission is a NASA New Millennium Program project that will validate new technologies for future space science missions and demonstrate the feasibility of building launching and operating multiple, miniature spacecraft that can collect research-quality in-situ science measurements. The three satellites in the ST5 constellation will be launched into a sun-synchronous Earth orbit in early 2006. ST5 fits into the 25-kilogram and 24-watt class of very small but fully capable spacecraft. The new technologies and design concepts for a compact power and command and data handling (C&DH) avionics system are presented. The 2-card ST5 avionics design incorporates new technology components while being tightly constrained in mass, power and volume. In order to hold down the mass and volume, and quali& new technologies for fUture use in space, high efficiency triple-junction solar cells and a lithium-ion battery were baselined into the power system design. The flight computer is co-located with the power system electronics in an integral spacecraft structural enclosure called the card cage assembly. The flight computer has a full set of uplink, downlink and solid-state recording capabilities, and it implements a new CMOS Ultra-Low Power Radiation Tolerant logic technology. There were a number of challenges imposed by the ST5 mission. Specifically, designing a micro-sat class spacecraft demanded that minimizing mass, volume and power dissipation would drive the overall design. The result is a very streamlined approach, while striving to maintain a high level of capability, The mission's radiation requirements, along with the low voltage DC power distribution, limited the selection of analog parts that can operate within these constraints. The challenge of qualifying new technology components for the space environment within a short development schedule was another hurdle. The mission requirements also demanded magnetic cleanliness in order to reduce the effect of stray (spacecraft-generated) magnetic fields on the science-grade magnetometer.

Speer, Dave↗

NASA NTRS2009

Instrumentation and Performance Analysis Plans for the HIFiRE Flight 2 Experiment

Supersonic combustion performance of a bi-component gaseous hydrocarbon fuel mixture is one of the primary aspects under investigation in the HIFiRE Flight 2 experiment. In-flight instrumentation and post-test analyses will be two key elements used to determine the combustion performance. Pre-flight computational fluid dynamics (CFD) analyses provide valuable information that can be used to optimize the placement of a constrained set of wall pressure instrumentation in the experiment. The simulations also allow pre-flight assessments of performance sensitivities leading to estimates of overall uncertainty in the determination of combustion efficiency. Based on the pre-flight CFD results, 128 wall pressure sensors have been located throughout the isolator/combustor flowpath to minimize the error in determining the wall pressure force at Mach 8 flight conditions. Also, sensitivity analyses show that mass capture and combustor exit stream thrust are the two primary contributors to uncertainty in combustion efficiency.

Gruber, Mark↗

NASA NTRS2001

Prospects for Nuclear Electric Propulsion Using Closed-Cycle Magnetohydrodynamic Energy Conversion

Nuclear electric propulsion (NEP) has long been recognized as a major enabling technology for scientific and human exploration of the solar system, and it may conceivably form the basis of a cost-effective space transportation system suitable for space commerce. The chief technical obstacles to realizing this vision are the development of efficient, high-power (megawatt-class) electric thrusters and the development of low specific mass (less than 1 kg/kWe) power plants. Furthermore, comprehensive system analyses of multimegawatt class NEP systems are needed in order to critically assess mission capability and cost attributes. This Technical Publication addresses some of these concerns through a systematic examination of multimegawatt space power installations in which a gas-cooled nuclear reactor is used to drive a magnetohydrodynamic (MHD) generator in a closed-loop Brayton cycle. The primary motivation for considering MHD energy conversion is the ability to transfer energy out of a gas that is simply too hot for contact with any solid material. This has several intrinsic advantages including the ability to achieve high thermal efficiency and power density and the ability to reject heat at elevated temperatures. These attributes lead to a reduction in system specific mass below that obtainable with turbine-based systems, which have definite solid temperature limits for reliable operation. Here, the results of a thermodynamic cycle analysis are placed in context with a preliminary system analysis in order to converge on a design space that optimizes performance while remaining clearly within established bounds of engineering feasibility. MHD technology issues are discussed including the conceptual design of a nonequilibrium disk generator and opportunities for exploiting neutron-induced ionization mechanisms as a means of increasing electrical conductivity and enhancing performance and reliability. The results are then used to make a cursory examination of piloted Mars missions during the 2018 opportunity.

Litchford, R. J.↗