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At least 1,315 records · Page 73

Optical measurements on contaminated surfaces

A bidirectional reflectometer system was developed for in situ measurements of the changes in spectral reflectance of surfaces contaminated with films of organic materials. The system permits experiments with films of controlled thickness in an environment that simulates the thermal, radiation, and vacuum conditions of space. The mechanical and optical construction of the reflectometer are discussed in detail, and actual data curves are used to illustrate its operation and performance.

Bonham, T. E.↗

Contamination control in hybrid microelectronic modules. Part 2: Selection and evaluation of coating materials

The selection, test, and evaluation of organic coating materials for contamination control in hybrid circuits is reported. The coatings were evaluated to determine their suitability for use as a conformal coating over the hybrid microcircuit (including chips and wire bonds) inside a hermetically sealed package. Evaluations included ease of coating application and repair and effect on thin film and thick film resistors, beam leads, wire bonds, transistor chips, and capacitor chips. The coatings were also tested for such properties as insulation resistance, voltage breakdown strength, and capability of immobilizing loose particles inside the packages. The selected coatings were found to be electrically, mechanically, and chemically compatible with all components and materials normally used in hybrid microcircuits.

Himmel, R. P.↗

Study of volatile contaminants in reclaimed water

Different methods were evaluated for reducing the volatile contaminants found in water recovered from urine by distillation. The use of activated carbon, addition of potassium permanganate, and the use of oxidation catalyst are described along with laboratory tests. It is concluded that catalytic decomposition appears to be feasible, and further investigation is recommended.

Mckee, H. C.↗

Apollo experience report: Detection and minimization of ignition hazards from water/glycol contamination of silver-clad electrical circuitry

The potential flammability hazard when a water/glycol solution contacts defectively insulated silver-clad copper circuitry or electrical components carrying a direct current is described. The chemical reactions and means for detecting them are explained. Methods for detecting and cleaning contaminated areas and the use of inhibitors to arrest chemical reactivity are also explained. Preventive measures to minimize hazards are given. Photomicrographs of the chemical reactions occurring on silver clad wires are also included.

Downs, W. R.↗

Payload/orbiter contamination control requirement study: Computer interface

The MSFC computer facilities, and future plans for them are described relative to characteristics of the various computers as to availability and suitability for processing the contamination program. A listing of the CDC 6000 series and UNIVAC 1108 characteristics is presented so that programming requirements can be compared directly and differences noted.

Bareiss, L. E.↗

Integrated Real Time Contamination Monitor IRTCM

Engineering and design work was performed on a monitoring device for particulate and gas contamination to be used in the space shuttle cargo area during launch at altitudes up to 50 km and during return phases of the flight. The gas sampling device consists of ampules filled with specific absorber materials which are opened and/or sealed at preprogrammed intervals. The design eliminates the use of valves which, according to experiments, are never sealing properly at hard vacuum. Methods of analysis including in-flight measuring possibilities are discussed.

Luttges, W. E.↗

A single field of view method for retrieving tropospheric temperature profiles from cloud-contaminated radiance data

An iterative method is presented to retrieve single field of view (FOV) tropospheric temperature profiles directly from cloud-contaminated radiance data. A well-defined temperature profile may be calculated from the radiative transfer equation (RTE) for a partly cloudy atmosphere when the average fractional cloud amount and cloud-top height for the FOV are known. A cloud model is formulated to calculate the fractional cloud amount from an estimated cloud-top height. The method is then examined through use of simulated radiance data calculated through vertical integration of the RTE for a partly cloudy atmosphere using known values of cloud-top height(s) and fractional cloud amount(s). Temperature profiles are retrieved from the simulated data assuming various errors in the cloud parameters. Temperature profiles are retrieved from NOAA-4 satellite-measured radiance data obtained over an area dominated by an active cold front and with considerable cloud cover and compared with radiosonde data. The effects of using various guessed profiles and the number of iterations are considered.

Hodges, D. B.↗

Oxidation of contaminative methane traces with radio-frequency discharge

An 11.8 MHz glow discharge was used to oxidize trace levels of methane in oxygen. The concentration of methane can be reduced by three orders of magnitude. The effects of power (0-400 W), flow rate (10-1000 cc-STP/min) and concentration (70-8000 ppm) were investigated at pressures ranging from 50 torr to almost 1 atm. No organic reaction products were detected in the treated gas stream. The process may prove useful for the removal of atmospheric trace contaminants at ambient pressure.

Flamm, D. L.↗

Contamination control coatings for hybrids

Conductive particles unexpectedly present in hermetically sealed hybrid microcircuit packages pose a high risk of shorting the closely spaced planar conductors within the package, causing failure of the device. The present work evaluates commercially available organic coating materials and determines the most promising ones for protection of complex microcircuits against entrapped particulate contaminants. The candidate materials were exposed to a series of physical and electrical screening tests, the results of which were used as a basis for the final coating selection. Silicones and high-purity epoxies are found to not only display excellent compatibility with microcircuits but to improve the performance of microcircuits as to voltage breakdown between adjacent conductors.

Mastro, A. R.↗

Quantitative measurement of surface contamination

Portable and highly sensitive system permits quantitative determinations on test surfaces. Device is used in normal room light and permits detection of significantly smaller samples. Digitation of output permits easy evaluation of contamination cleanup techniques.

Richmond, R. G.↗

Space shuttle contamination due to backflow from control motor exhaust

Spacecraft contamination of the space shuttle orbiter and accompanying Spacelab payloads is studied. The scattering of molecules from the vernier engines and flash evaporator nozzle after impingement on the orbiter wing surfaces, and the backflow of molecules out of the flash evaporator nozzle plume flow field due to intermolecular collisions in the plume are the problems discussed. A method was formulated for dealing with these problems, and detailed results are given.

Robertson, S. J.↗

A survey of particle contamination in electronic devices

The experiences are given of a number of National Aeronautics and Space Administration (NASA) and Space and Missile System Organization (SAMSO) contractors with particle contamination, and the methods used for its prevention and detection, evaluates the bases for the different schemes, assesses their effectiveness, and identifies the problems associated with each. It recommends specific short-range tests or approaches appropriate to individual part-type categories and recommends that specific tasks be initiated to refine techniques and to resolve technical and application facets of promising solutions.

Adolphsen, J. W.↗

Correlation of self-contamination experiments in orbit and scattering return flux calculations

Gaseous emissions from a spacecraft modify the orbital environment degrade the observations of distant radiation sources, and provide contamination fluxes induced by self-scattering and scattering with ambient particles. Experiments were carried out on the orbiting Atmospheric Explorer-D satellite (AE-D) to verify the calculated return fluxes of a neon source. Known rates of neon were emitted in the direction of the velocity on command to the Molecular Return Measurement Unit (MRMU). At 250 km, the neutral mass spectrometer indicated a total neon return flux of .0246 times the emitted flux. The calculated fraction was .0123, including .00354 for the ambient scatter and .00354 for the altitude independent self-scatter. The pressure gages indicated return pressure less than .000933Pa .000007 at altitudes from 161 to 210 km. The maximum return pressure for 161-km orbit was calculated as 7.3 x 10-7 including a self scattering contribution of .000024 Pa .000000018.

Scialdone, J. J.↗

A dispersion model approach to the preliminary design of adsorber beds for trace contaminants

It is shown that a dispersion model for the transport of a gas through a porous medium can be useful in the preliminary design of adsorber beds for the control of trace contaminants. The transmission function is considered, taking into account the transmission of 102-ppm acetaldehyde in helium flowing at various flow rates through an absorber bed. The experiments were conducted at a temperature of 25.0 C. Attention is given to a representation of the experimental breakthrough curve, the volume adsorption capacity, temperature studies, and correlations.

Madey, R.↗

Infrared characterized spacecraft contaminants and related compounds

Infrared spectra (% transmittance plotted vs wavelength/wavenumber) of a large number of lubricant and sealant oils and greases, insulating tapes, and solvents likely to contaminate the internal or external environment of spacecraft are reproduced. Accompanying introductory remarks characterize the nomenclature and properties or uses of the materials whose spectra are reproduced, and offer information on the techniques and equipment used in taking the spectra.

Gross, F. C.↗

CO2 and humidity removal system for extended Shuttle missions - CO2, H2O, and trace contaminant equilibrium testing

The equilibrium relationships for the co-adsorption of CO2 and H2O on an amine coated acrylic ester are presented. The equilibrium data collection and reduction techniques are discussed. Based on the equilibrium relationship, other modes of operation of systems containing HS-C are discussed and specific space applications for HS-C are presented. Equilibrium data for 10 compounds which are found as trace contaminants in closed environments are also presented.

Davis, S. H.↗

Skylab contamination results: S052 particle analysis and T025 analysis

The size and velocity distributions of 500 contaminant particles in the near environs of Skylab were determined from video tape data obtained by the high altitude observatory's white light coronagraph. A complete listing of derived particle parameters, their frequency distributions, and their behavior as a function of time are presented. A correlation between particle size and velocity is noted, and at least two prominent directions of the particle spacecraft origins are identified.

Schuerman, D. W.↗