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At least 1,297 records · Page 72

Viewgraph preparation made easier

Rolls of color-reversal film permit exposure of over 200 viewgraphs on one film loading. Time is saved in film development as roll film lends itself readily to automatic processing.

Broskie, H. W.↗

Preparation and evaluation of thin-film sodium tungsten bronzes

Thin films of sodium tungsten bronze (NaxWO3) were investigated as reversible sodium ion electrodes for solid electrolytes. The films were made by electron beam evaporation of the three phases, W metal, Na2WO4, and WO3, followed by sintering. The substrates were sodium beta alumina disks and glass slides. X-ray diffraction analyses of the films showed that sintering in dry nitrogen with prior exposure to air lead to mixed phases. Sintering in vacuum with no air exposure produced tetragonal I bronze with a nominal composition of Na0.31WO3, single phase within the limits of X-ray diffraction detectability. The films were uniform and adherent on sodium beta alumina substrates. The ac and dc conductivities of the beta alumina were measured with the sodium tungsten bronze films as electrodes. These experiments indicated that the tetragonal I bronze electrodes were not completely reversible. This may have resulted from sodium ion blocking within the bronze film or at the bronze beta alumina interface. Methods for attempting to make more completely reversible electrodes are suggested.

Kautz, H. E.↗

First geosynchronous weather satellite prepared for launch

The Synchronous Meteorological Satellite (SMS), which is scheduled for launch 16 May 1974 is described along with the data transmission system. The Carrier Balloon System is discussed. The primary type of data to be obtained in conjunction with SMS and Nimbus F are meteorological, oceanographic, seismic, and tsunami information. The Space Environment Monitoring System is also described.

Source record↗

Study, selection, and preparation of solid cationic conductors

Crystal chemical principles and transport theory have been used to predict structures and specific compounds which might find application as solid electrolytes in rechargeable high energy and high power density batteries operating at temperatures less than 200 C. Structures with 1-, 2-, and 3-dimensional channels were synthesized and screened by nuclear magnetic resonance, dielectric loss, and conductivity. There is significant conductivity at room temperature in some of the materials but none attain a level that is comparable to beta-alumina. Microwave and fast pulse methods were developed to measure conductivity in powders and in small crystals.

Roth, W. L.↗

Role of gravity in preparative electrophoresis

Electrophoresis has contributed significantly to the methodology of biological sciences, and shows the potential for large scale fractionation of a wide range of medically important substances, including living cells. Gravity plays an important role in the electrophoretic process, and hence the importance of the NASA effort to develop a zero-gravity separation facility as part of its shuttle program. The current state of art in electrophoresis is reviewed with particular emphasis on the role of gravity and the possible use of istachophoresis. This technique utilizes a discontinuous buffer system, and appears to be the only high resolution electrophoretic technique currently available for separation of living cells.

Bier, M.↗

Preparing oxidizer coated metal fuel particles

A solid propellant composition of improved efficiency is described which includes an oxidizer containing ammonium perchlorate, and a powered metal fuel, preferably aluminum or beryllium, in the form of a composite. The metal fuel is contained in the crystalline lattice framework of the oxidizer, as well as within the oxidizer particles, and is disposed in the interstices between the oxidizer particles of the composition. The propellant composition is produced by a process comprising the crystallization of ammonium perchlorate in water, in the presence of finely divided aluminum or beryllium. A suitable binder is incorporated in the propellant composition to bind the individual particles of metal with the particles of oxidizer containing occluded metal.

Shafer, J. I.↗

Computer experiments in preparation of system identification from transient rotor model tests, part 2

System identification methods which can extract model rotor paramenters with reasonable accuracy from noise polluted blade flapping transient measurements were developed. Usually parameter identification requires data on the state variables, that is on deflections and on rate of deflections. The small size of rotor models makes it, however, difficult to measure more than the blade flapping deflections. For the computer experiments it was, therefore, assumed that only noisy deflection measurements are available. Parameter identifications were performed for one and two unknown parameters. Both rotating coordinates and multiblade coordinates were used. It was found that data processing with a digital filter allowed by numerical differentiation a sufficiently accurate determination of the rates of deflection and of the accelerations to obtain reasonable parameter estimates with a simple linear estimator.

Hohenemser, K. H.↗

Preparation and metallurgical properties of low gravity processed immiscible materials

Initial experiments conducted during the Apollo 14 mission demonstrated that unique dispersions of immiscible materials could be obtained by processing in a low gravity environment. Subsequently, seven metallic systems have been processed in three NASA facilities: the drop tower at MSFC, the M-512 facility on board a KC-135 aircraft and the M-518 furnace on board Skylab. All couples were solidified from the liquid while in a low gravity environment, with one gravity processed specimens as controls. Metallographic examination demonstrated that the specimens processed in a low gravity environment exhibited a more uniform dispersion and microstructure than the one gravity processed controls.

Reger, J. L.↗

Thermal preparation of foods in space-vehicle environments

Convection is the primary heat transfer mechanism for most foods heated in an earth-based environment. In contrast, in the low-gravity environment of space flight, the primary heat transfer mechanism is conduction (or radiation in the absence of a conducting medium). Conduction heating is significantly slower and less efficient than convection heating. This fact poses a problem for food heating during space flight. A numerical model has been developed to evaluate this problem. This model simulates the food-heating process for Skylab. The model includes the effect of a thermally controlled on/off heat flux. Parametric studies using this model establish how the required heating time is affected by: the thermal diffusivity of the nutrient materials, the power level of the heater, the initial food temperatures, and the food container dimensions.

Bannerot, R. B.↗

Transphoresis and isotachophoresis as preparative techniques with reference to zero-gravity

Transphoresis and isotachophoresis are high resolution electrophoretic separation methods for biological materials. They benefit substantially from a weightless environment. Low power consumption and apparatus payload per unit product yield reflect their high electrophoretic efficiency. Properties unique to these systems, including their imposition of self-stabilizing geometry, suggest novel apparatus automatically controllable by largely electrical means with few or no moving parts. Configurations allowing continuous and semicontinuous operation, and further improvement of efficiency, are discussed.

Hinckley, J. O. N.↗

Process for preparing polyimide adhesives

High bonding strengths are obtained for metals and fiber-reinforced organic resin composites with no significant loss in thermo-oxidative stability of the adhesive resin.

Progar, D. J.↗

Apollo experience report: The role of flight mission rules in mission preparation and conduct

The development of flight mission rules from the mission development phase through the detailed mission-planning phase and through the testing and training phase is analyzed. The procedure for review of the rules and the coordination requirements for mission-rule development are presented. The application of the rules to real-time decision making is outlined, and consideration is given to the benefit of training ground controllers and flightcrews in the methods of determining the best response to a nonnominal in-flight situation for which no action has been preplanned. The Flight Mission Rules document is discussed in terms of the purpose and objective thereof and in terms of the definition, the development, and the use of mission rules.

Keyser, L. W.↗