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DOE OSTI2022

Enhanced terrestrial Fe(II) mobilization identified through a novel mechanism of microbially driven cave formation in Fe(III)-rich rocks

Most cave formation requires mass separation from a host rock in a process that operates outward from permeable pathways to create the cave void. Given the poor solubility of Fe(III) phases, such processes are insufficient to account for the significant iron formation caves (IFCs) seen in Brazilian banded iron formations (BIF) and associated rock. Here in this study we demonstrate that microbially-mediated reductive Fe(III) dissolution is solubilizing the poorly soluble Fe(III) phases to soluble Fe(II) in the anoxic zone behind cave walls. The resultant Fe(III)-depleted material (termed sub muros) is unable to maintain the structural integrity of the walls and repeated rounds of wall collapse lead to formation of the cave void in an active, measurable process. This mechanism may move significant quantities of Fe(II) into ground water and may help to explain the mechanism of BIF dissolution and REE enrichment in the generation of canga. The role of Fe(III) reducing microorganism and mass separation behind the walls (outward-in, rather than inward-out) is not only a novel mechanism of speleogenesis, but it also may identify a previously overlooked source of continental Fe that may have contributed to Archaean BIF formation.

54 ENVIRONMENTAL SCIENCES↗

NASA NTRS2011

Exploring the Use of Radar for a Physically Based Lightning Cessation Nowcasting Tool

NASA s Marshall Space Flight Center (MSFC) and the University of Alabama in Huntsville (UAHuntsville) are collaborating with the 45th Weather Squadron (45WS) at Cape Canaveral Air Force Station (CCAFS) to enable improved nowcasting of lightning cessation. This project centers on use of dual-polarimetric radar capabilities, and in particular, the new C-band dual-polarimetric weather radar acquired by the 45WS. Special emphasis is placed on the development of a physically based operational algorithm to predict lightning cessation. While previous studies have developed statistically based lightning cessation algorithms, we believe that dual-polarimetric radar variables offer the possibility to improve existing algorithms through the inclusion of physically meaningful trends reflecting interactions between in-cloud electric fields and hydrometeors. Specifically, decades of polarimetric radar research using propagation differential phase has demonstrated the presence of distinct phase and ice crystal alignment signatures in the presence of strong electric fields associated with lightning. One question yet to be addressed is: To what extent can these ice-crystal alignment signatures be used to nowcast the cessation of lightning activity in a given storm? Accordingly, data from the UAHuntsville Advanced Radar for Meteorological and Operational Research (ARMOR) along with the NASA-MSFC North Alabama Lightning Mapping Array are used in this study to investigate the radar signatures present before and after lightning cessation. Thus far, our case study results suggest that the negative differential phase shift signature weakens and disappears after the analyzed storms ceased lightning production (i.e., after the last lightning flash occurred). This is a key observation because it suggests that while strong electric fields may still have been present, the lightning cessation signature encompassed the period of the polarimetric negative phase shift signature. To the extent this behavior is repeatable in other cases, even if only in a substantial fraction of those cases, the case analyses suggests that differential propagation phase may prove to be a useful parameter for future lightning cessation algorithms. Indeed, analysis of 15+ cases has shown additional indications of the weakening and disappearance of this ice alignment signature with lightning cessation. A summary of results will be presented.

Schultz, Elise V.↗

DOE OSTI2021

Insights into the Rich Polymorphism of the Na + Ion Conductor Na 3 PS 4 from the Perspective of Variable-Temperature Diffraction and Spectroscopy

Solid electrolytes are crucial for next-generation solid-state batteries, and Na 3 PS 4 is one of the most promising Na + conductors for such applications, despite outstanding questions regarding its structural polymorphs. In this contribution, we present a detailed investigation of the evolution in structure and dynamics of Na 3 PS 4 over a wide temperature range 30 < T T < 500 °C, which we attribute to dynamic local tetragonal distortions. The first-order phase transition to the mesophasic high-temperature polymorph (γ, Fddd ) is associated with a sharp volume increase and the onset of liquid-like dynamics for sodium-cations (translational) and thiophosphate-polyanions (rotational) evident by inelastic neutron and Raman spectroscopies, as well as pair-distribution function and molecular dynamics analyses. Overall, these results shed light on the rich polymorphism of Na 3 PS 4 and are relevant for a range host of high-performance materials deriving from the Na 3 PS 4 structural archetype.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗

DOE OSTI2022

Exploring ENSO-Induced Anomalies over North America in Historical and Future Climate Simulations That Use HadGEM2-ESM Output to Drive WRF

Projected changes to the El Niño Southern Oscillation (ENSO) climate mode have been explored using global Earth system models (ESMs). Regional expressions of such changes have yet to be fully advanced and may require the use of regional downscaling. Here, we employ regional climate modeling (RCM) using the Weather Research and Forecasting (WRF) model at convection-permitting resolution and nested in output from the HadGEM2 ESM. We quantify ENSO teleconnections to temperature and precipitation anomalies in historical and future climate scenarios over eastern North America. Two paired simulations are run, a strong El Niño (positive ENSO phase) and a weak La Niña (negative ENSO phase), for the historical and future years. The HadGEM2 direct output and HadGEM2-WRF simulation output are compared to the anomalies derived from the NOAA ENSO Climate Normals dataset. The near-surface temperature and precipitation differences by ENSO phase, as represented by the HadGEM2-WRF historical simulations, show a poor degree of association with the NOAA ENSO Climate Normals, in part because of the large biases in the HadGEM2 model. Downscaling with the WRF model does improve the agreement with the observations, and large discrepancies remain. The model chain HadGEM2-WRF reverses the sign of the ENSO phase response over eastern North America under simulations of the future climate with high greenhouse gas forcing, but due to the poor agreement with the NOAA ENSO Climate Normals it is difficult to assign confidence to this prediction.

54 ENVIRONMENTAL SCIENCES↗

DOE OSTI2020

An extended/generalized phase-field finite element method for crack growth with global-local enrichment

In this paper, an extended/generalized finite element method (XFEM/GFEM) for simulating quasistatic crack growth based on a phase-field method is presented. The method relies on approximations to solutions associated with two different scales: a global scale, that is, structural and discretized with a coarse mesh, and a local scale encapsulating the fractured region, that is, discretized with a fine mesh. A stable XFEM/GFEM is employed to embed the displacement and damage fields at the global scale. The proposed method accommodates approximation spaces that evolve between load steps, while preserving a fixed background mesh for the structural problem. In addition, a prediction-correction algorithm is employed to facilitate the dynamic evolution of the confined crack regions within a load step. Several numerical examples of benchmark problems in two- and three-dimensional quasistatic fracture are provided to demonstrate the approach.

multiscale↗

NASA NTRS2003

Morphological Evidence for an Exclusively Inorganic Origin for Magnetite in Martian Meteorite ALH84001

The origin of magnetite crystals in Martian Meteorite ALH84001 is the focus of a debate about the possibility of past (and present) life on Mars. McKay et al. originally suggested that some of the magnetite crystals associated with carbonate globules in Martian Meteorite ALH84001 are biogenic in ori-gin, because they are single magnetic domain, free of crystalline defects, chemically pure, and coexist with other metastable phases in apparent disequilibrium. Thomas-Keprta et al. reported that a subpopulation of magnetite crystals (approx. 25%) associated with carbonate globules in ALH84001 and magnetite crystals produced by magnetotactic bacterial strain MV-1 have similar morphologies with crystal elongation along the [111] crystallographic axis that they describe as "truncated hexa-octahedral" ([111-THO]) magnetite. Along with several other properties, the [111]-THO morphology has been proposed to constitute a biomarker (i.e., formed only in biogenic processes), so that the presence of [111]-THO magnetite in ALH84001 may be evidence for past life on Mars.

Golden, D. C.↗

NASA NTRS1994

Multiscale low-frequency circulation modes in the global atmosphere

In this paper, fundamental multiscale circulation modes in the global atmosphere are identified with the objective of providing better understanding of atmospheric low-frequency variabilities over a wide range of spatial and temporal scales. With the use of a combination of rotated principal component technique, singular spectrum analysis, and phase space portraits, three categories of basic multiscale modes in the atmosphere are found. The first is the interannual-mode (IAM), which is dominated by time scales longer than a year and can be attributed to heating and circulation anomalies associated with the coupled tropical ocean-atmosphere, in particular the El Nino-Southern Oscillation. The second is a set of tropical intraseasonal modes consisting of three separate multiscale patterns (ISO-1, -2, -3) related to tropical heating that can be identified with the different phases of the Madden-Julian Oscillation (MJO), including its teleconnection to the extratropics. The ISO spatial and temporal patterns suggest that the extratropical wave train in the North Pacific and North America is related to heating over the Maritime Continent and that the evolution of the MJO around the equator may require forcing from the extratropics spawning convection over the Indian Ocean. The third category represents extratropical intraseasonal oscillations arising from internal dynamics of the basic-state circulation. In the Northern Hemisphere, there are two distinct circulation modes with multiple frequencies in this category: the Pacific/North America (PNA) and the North Atlantic/Eurasia (NAE). In the Southern Hemisphere, two phase-locked modes (PSA-1 and PSA-2) are found depicting an eastward propagating wave train from eastern Australia, via the Pacific South America to the South Atlantic. The extratropical modes exhibit temporal characteristics such as phase locking and harmonic oscillations possibly associated with quadratically nonlinear dynamical systems. Additionally, the observed monthly and seasonal anomalies arise from a complex interplay of the various multiscale low-frequency modes. The relative dominance of the different modes varies widely from month to month and from year to year. On the monthly time scale, while one or two mechanisms may dominate in one year, no single mechanism seems to dominate for all years. There are indications that when the IAM, that is, ENSO heating patterns are strong, the extratropical modes may be suppressed and vice versa. For the seasonal mean, the interannual mode tends to dominate and the contribution from the PNA remains quite significant.

Lau, K.-M.↗

NASA NTRS1989

Correlation of optical phase distortion with turbulent structure in a homogeneous shear flow

The relative importance of small-scale and large-scale turbulent structure to phase distortion in propagation through the homogeneous shear flow is the focus of this study. The importance of large-scale vortical structure and the associated scalar distribution to optical distortion induced by propagation through a turbulent shear flow has been established (Truman and Lee 1989). Phase errors induced in a coherent optical beam by these turbulent fluctuations are computed. This scalar field shows elongated regions of intense fluctuations which have an inclination with respect to the mean flow similar to that of the characteristic hairpin eddies. Long-term plans include an examination of the effects of inhomogeneity through consideration of direct numerical simulations of the channel flow, boundary layer or mixing layer.

Truman, C. Randall↗

NASA NTRS2007

Advances in Scanning Reflectarray Antennas Based on Ferroelectric Thin Film Phase Shifters for Deep Space Communications

Though there are a few examples of scanning phased array antennas that have flown successfully in space, the quest for low-cost, high-efficiency, large aperture microwave phased arrays continues. Fixed and mobile applications that may be part of a heterogeneous exploration communication architecture will benefit from the agile (rapid) beam steering and graceful degradation afforded by phased array antennas. The reflectarray promises greater efficiency and economy compared to directly-radiating varieties. Implementing a practical scanning version has proven elusive. The ferroelectric reflectarray, under development and described herein, involves phase shifters based on coupled microstrip patterned on Ba(x)Sr(1-x)TiO3 films, that were laser ablated onto LaAlO3 substrates. These devices outperform their semiconductor counterparts from X- through and K-band frequencies. There are special issues associated with the implementation of a scanning reflectarray antenna, especially one realized with thin film ferroelectric phase shifters. This paper will discuss these issues which include: relevance of phase shifter loss; modulo 2(pi) effects and phase shifter transient effects on bit error rate; scattering from the ground plane; presentation of a novel hybrid ferroelectric-semiconductor phase shifter; and the effect of mild radiation exposure on phase shifter performance.

Romanofsky, Robert R.↗

NASA NTRS1973

Theory of the phase anomaly in the thermosphere

Discussion of the temperature-density phase anomaly on the basis of a quasi-three-dimensional model in which the thermosphere dynamics associated with wind circulation is considered in a self-consistent form. Included in this analysis are the first three harmonics, which involve nonlinear coupling between diurnal and semidiurnal tides. It is shown that the phase anomaly with exospheric temperature peaks near 1600 LT and mass density peaks between 1400 and 1445 LT can be reproduced in a self-consistent theory without invoking ad hoc assumptions and boundary conditions that would mask the physical processes to be explored. A number of factors and processes are found to contribute to the phase anomaly, including the semidiurnal and particularly the terdiurnal components, heat advection, diffusion, and energy coupling with the lower atmosphere.

Mayr, H. G.↗

NASA NTRS1982

A reinvestigation of the rate of the C/+/ + H2 radiative association reaction

It is noted that new experimental results and statistical theories have prompted a reinvestigation of the rate coefficient of the interstellar reaction in which C(+) + H2 yields CH2(+) + h(nu) in the 10-100 K temperature range. The results presented here indicate a rate coefficient between 10 to the -16 and 10 to the -15 cu cm/s at all temperatures studied. In applying the modified thermal and phase space theories, it is expected that they will be as accurate as for radiative association as for three-body association, provided the ab initio value for the radiative decay rate is correct. It is expected that the calculated values of the rate coefficient will be accurate to within an order of magnitude and will have the correct temperature dependence.

Herbst, E.↗

NASA NTRS1973

Transient analysis of phase-locked tracking systems in the presence of noise.

This paper is concerned with the problem of obtaining time-dependent solutions to a class of Fokker-Planck equations that arise in the analysis and synthesis of a variety of first-order synchronization systems employing the phase-lock principle. These include the classical sinusoidal phase-locked loop, squaring and Costas loops, data-aided loops, hybrid loops, various symbol synchronizer mechanizations, and tunnel-diode oscillators. By analyzing the spectral properties of the associated time-dependent Fokker-Planck boundary value problem, eigenfunction expansions of the reduced modulo-2-pi phase-error-transition probability-density function are developed for a class of first-order synchronization systems.

La Frieda, J. R.↗

NASA NTRS1984

Application of signal analysis to cavitation

The diagnostic facilities of the cross power spectrum and the coherence function have been employed to enhance the identification of not only the inception of cavitation, but also its level. Two piezoelectric pressure transducers placed in the downstream chamber of a model spool valve undergoing various levels of cavitation allowed for the use of both functions - the phase angle of the complex cross spectrum and the dimensionless coherence function - to sense clearly the difference between noise levels associated with a noncavitating jet from those once cavitation inception is attained. The cavitation noise within the chamber exhibited quite a regular character in terms of the phase difference between instruments for limited cavitation. Varying cavitation levels clearly illustrated the effect of bubble size on the attendant frequency range for which there was an extremely high coherence or nearly perfect causality.

Martin, C. S.↗

NASA NTRS1988

Ariane 5 verification and associated test facilities

The philosophy of verification tests of the Ariane 5 launcher program is already established. It corresponds to the development and the ground and flight qualification phases for both unmanned and manned launches. The different types of test are outlined for the system, booster, main core and upper structures, allowing the identification of the associated test facilities which are described.

Vedrenne, M.↗

NASA NTRS1974

Satellite views of hurricane Camille

Three periods within the life cycle of Hurricane Camille (1969) are studied with radiometric and camera measurements from Nimbus-3 and camera information from ATS-3 in conjunction with conventional information. These periods are the deepening phase, the interaction of Camille with midlatitude westerlies, and the excessive rain producing period when the cyclone was over the central Appalachian Mountain. Just prior to significant deepening, the Nimbus-3 Medium Resolution Infrared Radiometer (MRIR) showed that a pronounced feeder band had formed southeast of the center which was associated with the rapid transport of moisture into the storm circulation. During the rapid deepening phase the MRIR measurements indicated the development of large scale subsidence throughout the troposphere northwest of the center. When Camille was over the lower Mississippi Valley it acted as an obstruction to the envrionmental wind. A region of widespread subsidence was created west and north of the cyclone center. Increased cloud-top elevations, back to the levels reached when Camille was an intense cyclone over the Gulf of Mexico, were estimated from the Nimbus-3 High Resolution Infrared Radiometer (HRIR) measurements on August 20, 1969, when Camille produced rains of major flood proportions near the east slopes of the Appalachians in central Virginia.

Shenk, W. E.↗

DOE OSTI2024

Thermal Management of Discretized Heaters Using CuW Microchannel Heat Sinks and FC3283

Single-phase cooling using microchannel heat sinks (MCHS) has become a popular approach for overcoming the thermal challenges associated with high-powered microelectronic devices. Thermal management is one of the largest barriers to higher power densities in electronics and frequently limits overall device performance. The implementation of forced convective cooling via single-phase liquid cooling in MCHS reduces the thermal resistance resulting in lower device temperatures at high-power conditions, which can decrease the package size and extend the lifespan of devices. The goal of the work described in this article was to investigate practical cooling solutions for laser diode bars. This study examined the effectiveness of a copper tungsten (CuW) microchannel heat sink paired with a dielectric coolant (FC3283) for dissipating both discrete and uniform heat fluxes up to 600 W/cm2 across a 0.25-cm2 surface area through a numerical and experimental study. CuW was chosen as the MCHS material because it is thermal expansion matched to GaAs, which is a common laser diode substrate. FC3283 serves as a dielectric coolant that is compatible with power electronics cooling. The microchannels utilized in this work were approximately $365$ $μ$ m deep and $100$ $μ$ m wide resulting in a hydraulic diameter of $160$ $μ$ m. The study investigated the cooling performance across a variety of applied power loads and flow rates to determine optimal effectiveness. The resulting thermal resistance ranged from 0.15 cm2 K/W at the highest flow rate to 0.26 cm2 K/W at the lowest flow rate. Further, the resulting thermal performance from this study demonstrates the importance of considering discrete heat sources separately from uniform heat sources and proved that the unique combination of CuW microchannels with FC3283 can be a promising cooling option toward future advancements of laser diode bars and other high-power microelectronics.

42 ENGINEERING↗

DOE OSTI2022

Kuramoto synchronization of quantum tunneling polarons for describing the dynamic structure in cuprate superconductors

A major open topic in cuprates is the interplay between the lattice and electronic dynamics and the importance of their coupling to the mechanism of high-temperature superconductivity (HTSC). As evidenced by extended x-ray absorption fine structure (EXAFS) experiments, anharmonic structural effects are correlated with the charge dynamics and the transition to a superconducting phase in different HTSC compounds. Here, in this paper, we describe how structural anharmonic effects can be coupled to electronic and lattice dynamics in cuprate systems by performing the exact diagonalization of a prototype anharmonic many-body Hamiltonian on a relevant 6-atom cluster and show that the EXAFS results can be understood as a Kuramoto synchronization transition between coupled internal quantum tunneling of polarons associated with the two-site distribution of the copper–apical oxygen (Cu-O ap ) pair in the dynamic structure. The transition is driven by the anharmonicity of the lattice vibrations and promotes the pumping of charge, initially stored at the apical oxygen reservoirs, into the copper-oxide plane. Simultaneously, a finite projection of the internal quantum tunneling polaron extends to the copper–planar oxygen (Cu-O pl ) pair. All these findings allow an interpretation based on an effective quantum-mechanical triple-well potential associated with the oxygen sites of the 6-atom cluster, which accurately represents the phase synchronization of apical oxygens and lattice-assisted charge transfer to the CuO 2 plane.

75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND↗

NASA NTRS1984

Differential, integral, and momentum-transfer cross sections for elastic electron scattering by neon - 5 to 100 eV

Relative elastic-scattering differential cross sections were measured in the 5-100-eV impact energy and 10-145 deg angular ranges. Normalization of these cross sections was achieved by utilizing accurate total electron-scattering cross sections. A phase-shift analysis of the angular distributions in terms of real phase shifts has been carried out. From the differential cross sections, momentum-transfer cross sections were obtained and the values of the critical energy and angle were established (associated with the lowest value of the differential cross section) as 62.5 + or - 2.5 eV and 101.7 deg + or - 1.5 deg, respectively. The present phase shifts, the critical parameters, and differential, integral, and momentum-transfer cross sections are compared to previous experimental and theoretical results. The error associated with the present data is about 10 percent.