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At least 1,297 records · Page 72

Materials processing in space; Proceedings of the Special Conference, Cincinnati, OH, May 4, 5, 1982

An international review of materials processing in space is provided, taking into account the NASA materials processing in space program, European activities in the field of microgravity research, and Japanese material processing tests in space. The subjects considered are related to materials processing in a microgravity environment, industrial and university applications and involvement, and challenges and prospectives of microgravity research in space. Attention is given to a review of the containerless processing technologies and facilities, glass research in space, bubble behavior in molten glass in a temperature gradient, semiconductor crystal growth and segregation problems on earth and space, seeded crystal growth of pseudobinary systems with large liquidus-solidus separation, avenues and incentives for commercial use of a low-gravity environment, and the Universities Space Research Association and its role in the materials processing in space program.

Dunbar, B. J.↗

Anode materials for electrochemical waste destruction

Electrochemical Oxidation (ECO) offers promise as a low-temperature, atmospheric pressure method for safe destruction of hazardous organic chemical wastes in water. Anode materials tend to suffer corrosion in the intensely oxidizing environment of the ECO cell. There is a need for cheaper, more resistant materials. In this experiment, a system is described for testing anode materials, with examples of several common anodes such as stainless steel, graphite, and platinized titanium. The ECO system is simple and safe to operate and the experiment can easily be expanded in scope to study the effects of different solutions, temperatures, and organic materials.

Molton, Peter M.↗

Microgravity acceleration measurement environment characterization

The Space Acceleration Measurement System (SAMS) is a general-purpose instrumentation system designed to measure the accelerations onboard the shuttle Orbiter and shuttle/Spacelab vehicles. These measurements are used to support microgravity experiments and investigations into the microgravity environment of the vehicle. Acceleration measurement can be made at locations remote from the SAMS main instrumentation unit by the use of up to three remote triaxial sensor heads. The SAMS was developed by NASA's Lewis Research Center (LeRC) in support of NASA's microgravity science programs. In the past, numerous acceleration measurement systems have flown on various space missions. These systems were tailored to measure accelerations for a narrow set of requirements and were limited in bandwidth, dynamic range, and recording capability. In addition, these systems were mission-peculiar and not easily modified for other applications or missions. The result has been an inability to accurately assess the expected microgravity environment prior to a mission for a particular experiment and/or location. The prime science objective for SAMS on the SL-J mission will be to measure the accelerations experienced by a multitude of experiments in the two racks of the Japanese First Materials Processing Test (FMPT). The FMPT consists of a variety of materials science and life science experiments contained in racks no. 7 and no. 10. The SAMS data will be made available to the FMPT principal investigators after the mission for their analysis with the FMPT data. A secondary science objective for SAMS will be the characterization of the acceleration environment of the Spacelab module. This will include an analysis of the acceleration transfer function of the Spacelab module which will utilize the FMPT acceleration measurement along with measurements at the rack no. 9 structure. Another analytical effort to be undertaken is a general characterization of the acceleration environment of the Spacelab as an orbiting laboratory. These analysis efforts will be in conjunction with similar measurements and analyses on other SAMS Spacelab missions.

Delombard, Richard↗

Design of a High Resolution Hexapod Positioning Mechanism

This paper describes the development of a high resolution, six-degree of freedom positioning mechanism. This mechanism, based on the Stewart platform concept, was designed for use with the Developmental Comparative Active Optics Telescope Testbed (DCATT), a ground-based technology testbed for the Next Generation Space Telescope (NGST). The mechanism provides active control to the DCATT telescope's segmented primary mirror. Emphasis is on design decisions and technical challenges. Significant issues include undesirable motion properties of PZT-inchworm actuators, testing difficulties, dimensional stability and use of advanced composite materials. Supporting test data from prototype mechanisms is presented.

Britt, Jamie↗

Design of a High Resolution Hexapod Positioning Mechanism

This paper describes the development of a high resolution, six-degree of freedom positioning mechanism. This mechanism, based on the Stewart platform concept, was designed for use with the Developmental Comparative Active Optics Telescope Testbed (DCATT), a ground-based technology testbed for the Next Generation Space Telescope (NGST). The mechanism provides active control to the DCATT telescope's segmented primary mirror. Emphasis is on design decisions and technical challenges. Significant issues include undesirable motion properties of PZT-inchworm actuators, testing difficulties, dimensional stability, and use of advanced composite materials. Supporting test data from prototype mechanisms is presented.

Britt, Jamie↗

Three Dimensional Constraint Effects on the Estimated (Delta)CTOD during the Numerical Simulation of Different Fatigue Threshold Testing Techniques

Variation in constraint through the thickness of a specimen effects the cyclic crack-tip-opening displacement (DELTA CTOD). DELTA CTOD is a valuable measure of crack growth behavior, indicating closure development, constraint variations and load history effects. Fatigue loading with a continual load reduction was used to simulate the load history associated with fatigue crack growth threshold measurements. The constraint effect on the estimated DELTA CTOD is studied by carrying out three-dimensional elastic-plastic finite element simulations. The analysis involves numerical simulation of different standard fatigue threshold test schemes to determine how each test scheme affects DELTA CTOD. The American Society for Testing and Materials (ASTM) prescribes standard load reduction procedures for threshold testing using either the constant stress ratio (R) or constant maximum stress intensity (K(sub max)) methods. Different specimen types defined in the standard, namely the compact tension, C(T), and middle cracked tension, M(T), specimens were used in this simulation. The threshold simulations were conducted with different initial K(sub max) values to study its effect on estimated DELTA CTOD. During each simulation, the DELTA CTOD was estimated at every load increment during the load reduction procedure. Previous numerical simulation results indicate that the constant R load reduction method generates a plastic wake resulting in remote crack closure during unloading. Upon reloading, this remote contact location was observed to remain in contact well after the crack tip was fully open. The final region to open is located at the point at which the load reduction was initiated and at the free surface of the specimen. However, simulations carried out using the constant Kmax load reduction procedure did not indicate remote crack closure. Previous analysis results using various starting K(sub max) values and different load reduction rates have indicated DELTA CTOD is independent of specimen size. A study of the effect of specimen thickness and geometry on the measured DELTA CTOD for various load reduction procedures and its implication in the estimation of fatigue crack growth threshold values is discussed.

Seshadri, Banavara R.↗

Characterization of Lunar Polar Volatiles for Curation and ISRU - Executive Summary

The goal of this project is to support lunar exploration by simulating and characterizing ice and volatile-rich materials expected to be found at the lunar poles. These materials are highly sensitive to heating, which could significantly alter their composition and prevent scientific studies on lunar samples. During FY19, we obtained materials for and designed a simulated lunar environment, within which volatile-rich simulant could be made. We also refined the procedure for moderate-fidelity lunar simulants at cryogenic temperatures. In FY20, we completed our test setup, and we can now reach cryogenic temperatures and near-lunar pressures with active compositional monitoring of volatiles in the vapor phase. For FY21, we: 1) progressed towards developing sample storage temperature requirements for volatile-rich samples by completing storage testing, along with materials testing for Artemis geologic sampling, 2) obtained instrumentation for solid sample monitoring to characterize solid species, and 3) progressed towards water extraction testing for ISRU. Our test results will directly feed into Artemis science requirements, hardware designs for sample return, vehicle requirements (HLS, Gateway, Orion), and operations planning for lunar exploration activities.

Julie L Mitchell↗

Test Methodology to Evaluate the Safety of Materials Using Spark Incendivity

For many years scientists and engineers have been searching for the proper test method to evaluate an electrostatic risk for materials used in hazardous environments. A new test standard created by the International Electrotechnical Commission is a promising addition to conventional test methods used throughout industry. The purpose of this paper is to incorporate this test into a proposed new methodology for the evaluation of materials exposed to flammable environments. However, initial testing using this new standard has uncovered some unconventional behavior in materials that conventional test methods were thought to have reconciled. For example some materials tested at higher humidities were more susceptible to incendive discharges than at lower humidity even though the surface resistivity was lower.

Buhler, Charles↗

Zero Launch Mass Three Dimensional Print Head

NASA's strategic goal is to put humans on Mars in the 2030's. The NASA Human Spaceflight Architecture Team (HAT) and NASA Mars Design Reference Architecture (DRA) 5.0 has determined that in-situ resource utilization (ISRU) is an essential technology to accomplish this mission. Additive construction technology using in-situ materials from planetary surfaces will reduce launch mass, allow structures to be three dimensionally (3D) printed on demand, and will allow building designs to be transmitted digitally from Earth and printed in space. This will ultimately lead to elimination of reliance on structural materials launched from Earth (zero launch mass of construction consumables). The zero launch mass (ZLM) 3D print head project addressed this need by developing a system that 3D prints using a mixture of in-situ regolith and polymer as feedstock, determining the optimum mixture ratio and regolith particle size distribution, developing software to convert g-code into motion instructions for a FANUC robotic arm, printing test samples, performing materials testing, and printing a reduced scale habitable structure concept. This paper will focus on the ZLM 3D Print Head design, materials selection, software development, and lessons learned from operating the system in the NASA KSC Swamp Works Granular Mechanics & Regolith Operations (GMRO) Laboratory.

3D print↗

Zero Launch Mass Three Dimensional Print Head

NASA's strategic goal is to put humans on Mars in the 2030s. The NASA Human Spaceflight Architecture Team (HAT) and NASA Mars Design Reference Architecture (DRA) 5.0 has determined that in-situ resource utilization (ISRU) is an essential technology to accomplish this mission. Additive construction technology using in-situ materials from planetary surfaces will reduce launch mass, allow structures to be three dimensionally (3D) printed on demand, and will allow building designs to be transmitted digitally from Earth and printed in space. This will ultimately lead to elimination of reliance on structural materials launched from Earth (zero launch mass of construction consumables). The zero launch mass (ZLM) 3D print head project addressed this need by developing a system that 3D prints using a mixture of in-situ regolith and polymer as feedstock, determining the optimum mixture ratio and regolith particle size distribution, developing software to convert g-code into motion instructions for a FANUC robotic arm, printing test samples, performing materials testing, and printing a reduced scale habitable structure concept. This paper will focus on the ZLM 3D Print Head design, materials selection, software development, and lessons learned from operating the system in the NASA KSC Swamp Works Granular Mechanics & Regolith Operations (GMRO) Laboratory.

Regolith↗

Similarity tests of turbine vanes, effects of ceramic thermal barrier coatings

The role of material thermal conductivity was analyzed for its effect on the thermal performance of air-cooled gas turbine components coated with a ceramic thermal barrier material when tested at reduced temperatures and pressures. It is shown that the thermal performance can be evaluated reliably at reduced gas and coolant conditions; however, thermal conductivity corrections are required for the data at reduced conditions. Corrections for a ceramic thermal barrier coated vane are significantly different than for an uncoated vane. Comparison of uncorrected test data, therefore, would show erroneously that the thermal barrier coating was ineffective. When thermal conductivity corrections are applied to the test data these data are then shown to be representative of engine data and also show that the thermal barrier coating increases the vane cooling effectiveness by 12.5 percent.

Gladden, H. J.↗

Similarity tests of turbine vanes - Effects of ceramic thermal barrier coatings

The role of material thermal conductivity was analyzed for its effect on the thermal performance of air-cooled gas turbine components coated with a ceramic thermal barrier material when tested at reduced temperatures and pressures. This study shows that the thermal performance can be evaluated reliably at reduced gas and coolant conditions. However, thermal conductivity corrections are required for the data at reduced conditions. These corrections for a ceramic thermal barrier coated vane are significantly different than the corrections for an uncoated vane. Comparison of uncorrected test data, therefore, would show erroneously that the thermal barrier coating was ineffective. When thermal conductivity corrections are applied to the test data these data are then shown to be representative of engine data and also show that the thermal barrier coating increases the vane cooling effectiveness by 12.5 precent.

Gladden, H. J.↗

Effects of atomic oxygen and ultraviolet radiation on candidate elastomeric materials for long duration missions. Test series no.1

Research was conducted at MSFC on the behavior of elastomeric materials after exposure to simulated space environment. Silicone S383 and Viton V747 samples were exposed to thermal vacuum, ultraviolet radiation, and atomic oxygen and then evaluated for changes in material properties. Characterization of the elastomeric materials included weight, hardness, optical inspection under normal and black light, spectrofluorescence, solar absorptance and emittance, Fourier transform infrared spectroscopy, and permeability. These results indicate a degree of sensitivity to exposure and provided some evidence of UV and atomic oxygen synergism.

Linton, R. C.↗

Non-Contact Thermal Properties Measurement with Low-Power Laser and IR Camera System

As shown by the Phoenix Mars Lander's Thermal and Electrical Conductivity Probe (TECP), contact measurements of thermal conductivity and diffusivity (using a modified flux-plate or line-source heat-pulse method) are constrained by a number of factors. Robotic resources must be used to place the probe, making them unavailable for other operations for the duration of the measurement. The range of placement is also limited by mobility, particularly in the case of a lander. Placement is also subject to irregularities in contact quality, resulting in non-repeatable heat transfer to the material under test. Most important from a scientific perspective, the varieties of materials which can be measured are limited to unconsolidated or weakly-cohesive regolith materials, rocks, and ices being too hard for nominal insertion strengths. Accurately measuring thermal properties in the laboratory requires significant experimental finesse, involving sample preparation, controlled and repeatable procedures, and, practically, instrumentation much more voluminous than the sample being tested (heater plates, insulation, temperature sensors). Remote measurements (infrared images from orbiting spacecraft) can reveal composite properties like thermal inertia, but suffer both from a large footprint (low spatial resolution) and convolution of the thermal properties of a potentially layered medium. In situ measurement techniques (the Phoenix TECP is the only robotic measurement of thermal properties to date) suffer from problems of placement range, placement quality, occupation of robotic resources, and the ability to only measure materials of low mechanical strength. A spacecraft needs the ability to perform a non-contact thermal properties measurement in situ. Essential components include low power consumption, leveraging of existing or highly-developed flight technologies, and mechanical simplicity. This new in situ method, by virtue of its being non-contact, bypasses all of these problems. The use of photons to both excite and measure the thermal response of any surface material to a high resolution (estimated footprint = 10 square centimeters) is a generational leap in physical properties measurements. The proposed method consists of spot-heating the surface of a material with a low (less than 1 W) power laser. This produces a moderate (5-10 K) temperature increase in the material.

Hudson, Troy L.↗

Arcjet Testing of Micro-Meteoroid Impacted Thermal Protection Materials

There are several harsh space environments that could affect thermal protection systems and in turn pose risks to the atmospheric entry vehicles. These environments include micrometeoroid impact, extreme cold temperatures, and ionizing radiation during deep space cruise, all followed by atmospheric entry heating. To mitigate these risks, different thermal protection material samples were subjected to multiple tests, including hyper velocity impact, cold soak, irradiation, and arcjet testing, at various NASA facilities that simulated these environments. The materials included a variety of honeycomb packed ablative materials as well as carbon-based non-ablative thermal protection systems. The present paper describes the results of the multiple test campaign with a focus on arcjet testing of thermal protection materials. The tests showed promising results for ablative materials. However, the carbon-based non-ablative system presented some concerns regarding the potential risks to an entry vehicle. This study provides valuable information regarding the capability of various thermal protection materials to withstand harsh space environments, which is critical to sample return and planetary entry missions.

Agrawal, Parul↗

Reuseable lightweight modular multi-layer insulation for space shuttle

The adaptation of the Self Evacuating Multilayer Insulation System to the space shuttle orbiter liquid hydrogen tanks was investigated. Small scale material screening tests and subscale panel tests demonstrated the potential of the insulation to withstand the anticipated 100 flight cycles. The composition of the material and the process for producing the finished insulation are described. Results of the various tests to determine the durability of the material are presented.

Burr, K. F.↗

Fuel containment and damage tolerance in large composite primary aircraft structures. Phase 2: Testing

Technical issues associated with fuel containment and damage tolerance of composite wing structures for transport aircraft were investigated. Material evaluation tests were conducted on two toughened resin composites: Celion/HX1504 and Celion/5245. These consisted of impact, tension, compression, edge delamination, and double cantilever beam tests. Another test series was conducted on graphite/epoxy box beams simulating a wing cover to spar cap joint configuration of a pressurized fuel tank. These tests evaluated the effectiveness of sealing methods with various fastener types and spacings under fatigue loading and with pressurized fuel. Another test series evaluated the ability of the selected coatings, film, and materials to prevent fuel leakage through 32-ply AS4/2220-1 laminates at various impact energy levels. To verify the structural integrity of the technology demonstration article structural details, tests were conducted on blade stiffened panels and sections. Compression tests were performed on undamaged and impacted stiffened AS4/2220-1 panels and smaller element tests to evaluate stiffener pull-off, side load and failsafe properties. Compression tests were also performed on panels subjected to Zone 2 lightning strikes. All of these data were integrated into a demonstration article representing a moderately loaded area of a transport wing. This test combined lightning strike, pressurized fuel, impact, impact repair, fatigue and residual strength.

Sandifer, J. P.↗