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At least 1,297 records · Page 72

Development and fabrication of a graphite polyimide box beam

The state-of-the-art of graphite/polyimide structures was evaluated and key design and fabrication issues to be considered in future hardware programs are defined. The fabrication and testing at 500 F of a graphite/polyimide center wing box beam using OV-10A aircraft criteria was accomplished. The baseline design of this box was developed in a series of studies of other advanced composite materials: glass/epoxy, boron/epoxy, and boron/polyimide. The use of this basic design permits ready comparison of the performance of graphite/polyimide with these materials. Modifications to the baseline composite design were made only in those areas effected by the change of materials. Processing studies of graphite fiber polyimide resins systems resulted in the selection of a Modmor II/Gemon L material.

Nadler, M. A.↗

Elastomer mounted rotors - An alternative for smoother running turbomachinery

This paper describes the design of elastomeric bearing supports for a rotor built to simulate the power turbine of an advanced gas turbine engine which traverses two bending critical speeds. The elastomer dampers were constructed so as to minimize rotor dynamic response at the critical speeds. Results are presented of unbalance response tests performed with two different elastomer materials. These results showed that the resonances on the elastomer-mounted rotor were well damped for both elastomer materials and showed linear response to the unbalance weights used for response testing. Additional tests were performed using solid steel supports at either end (hand-mounted), which resulted in drastically increased sensitivity and nonlinear response, and with steel supports in one end of the rotor and the elastomer at the other, which yielded results which were between the soft- and hard-mounted cases. It is concluded that elastomeric supports are a viable alternative to other methods of mounting flexible rotors, that damping was well in excess of predictions and that elastomeric supports are tolerant of small rotor misalignments.

Tecza, J. A.↗

Precision laser tracking for global and polar motion

This paper provides an overview of the Goddard Laser Tracking Network (GLTN). GLTN station locations, equipment, possible improvements, and data flow are discussed. Locations of the other major laser tracking networks and their present or expected performance are also provided. The material includes a listing of the Lunar Laser Ranging Stations (LLRSs) and their actual or expected performance.

Shawe, M. E.↗

Effect of process conditions and chemical composition on the microstructure and properties of chemically vapor deposited SiC, Si, ZnSe, ZnS and ZnS(x)Se(1-x)

Subatmospheric pressure CVD processes have been developed to produce theoretically dense, highly pure, void-free and large area bulk materials, SiC, Si, ZnSe, ZnS and ZnS(x)Se(1-x). These materials are used for optical elements, such as mirrors, lenses and windows, over a wide spectral range from the VUV to the IR. We discuss the effect of CVD process conditions on the microstructure and properties of these materials, with emphasis on optical performance. In addition, we discuss the effect of chemical composition on the properties of the composite material ZnS(x)Se(1-x). We first present a general overview of the bulk CVD process and the relationship between process conditions, such as temperature, pressure, reactant gas concentration and growth rate, and the microstructure, morphology and properties of CVD-grown materials. Then we discuss specific results for CVD-grown SiC, Si, ZnSe, ZnS and ZnS(x)Se(1-x).

Pickering, Michael A.↗

A Comparison of Materials Issues for Cermet and Graphite-Based NTP Fuels

This paper compares material issues for cermet and graphite fuel elements. In particular, two issues in NTP fuel element performance are considered here: ductile to brittle transition in relation to crack propagation, and orificing individual coolant channels in fuel elements. Their relevance to fuel element performance is supported by considering material properties, experimental data, and results from multidisciplinary fluid/thermal/structural simulations. Ductile to brittle transition results in a fuel element region prone to brittle fracture under stress, while outside this region, stresses lead to deformation and resilience under stress. Poor coolant distribution between fuel element channels can increase stresses in certain channels. NERVA fuel element experimental results are consistent with this interpretation. An understanding of these mechanisms will help interpret fuel element testing results.

Nuclear Propulsion↗

Cosmic Ray Exposure & Linear-Energy-Transfer Evaluations for the COBE Mission

Magnetospherically attenuated, orbit integrated, surface incident cosmic ray fluxes of galactic origin were determined for the COBE mission. All heavy ions up to Nickel (z=28) were considered in this, evaluation. In order to provide worst case approximations, estimates were based on solar minimum conditions. Transport and material shielding calculations were then performed for these vehicle encountered particles, for a simple spherical 3-D aluminum geometry, and the materially attenuated cosmic ray distributions emerging behind selected shield thicknesses were obtained. Finally, Linear-Energy-Transfer (LET) spectra were evaluated for the energy spectra of each ion specie and these were, in turn, integrated into the sum-total LET distribution contained in this report. The results are presented in tabular and graphical form for eight (8) different shield thicknesses from.01 to 10.0 gm/cm2 of aluminum. They show most conclusively, and not unexpectedly, that material shielding has virtually no 'effect on the final LET spectrum, at least not for aluminum shields. This was predictable. Please note that in the LET graphs, two curves were plotted. Of these, please ignore the one labeled "grazing" and use only the one labeled "normal". Again, it should be remembered that the end results contain contributions from all elements up to Nickel (z=28).

Stassinopoulos, E. G.↗

Overview of C/C-SiC Composite Development for the Orion Launch Abort System

Past and present efforts by the authors to further understanding of the ceramic matrix composite (CMC) material used in the valve components of the Orion Launch Abort System (LAS) Attitude Control Motor (ACM) will be presented. The LAS is designed to quickly lift the Orion Crew Exploration Vehicle (CEV) away from its launch vehicle in emergency abort scenarios. The ACM is a solid rocket motor which utilizes eight throttleable nozzles to maintain proper orientation of the CEV during abort operations. Launch abort systems have not been available for use by NASA on manned launches since the last Apollo ]Saturn launch in 1975. The CMC material, carbon-carbon/silicon-carbide (C/C-SiC), is manufactured by Fiber Materials, Inc. and consists of a rigid 4-directional carbon-fiber tow weave reinforced with a mixed carbon plus SiC matrix. Several valve and full system (8-valve) static motor tests have been conducted by the motor vendor. The culmination of these tests was the successful flight test of the Orion LAS Pad Abort One (PA ]1) vehicle on May 6, 2010. Due to the fast pace of the LAS development program, NASA Marshall Space Flight Center assisted the LAS community by performing a series of material and component evaluations using fired hardware from valve and full ]system development motor tests, and from the PA-1 flight ACM motor. Information will be presented on the structure of the C/C-SiC material, as well as the efficacy of various non ]destructive evaluation (NDE) techniques, including but not limited to: radiography, computed tomography, nanofocus computed tomography, and X-ray transmission microscopy. Examinations of the microstructure of the material via scanning electron microscopy and energy dispersive spectroscopy will also be discussed. The findings resulting from the subject effort are assisting the LAS Project in risk assessments and in possible modifications to the final ACM operational design.

Allen, Lee R.↗

The effect of sample holder material on ion mobility spectrometry reproducibility

When a positive detection of a narcotic occurs during the search of a vessel, a decision has to be made whether further intensive search is warranted. This decision is based in part on the results of a second sample collected from the same area. Therefore, the reproducibility of both sampling and instrumental analysis is critical in terms of justifying an in depth search. As reported at the 2nd Annual IMS Conference in Quebec City, the U.S. Coast Guard has determined that when paper is utilized as the sample desorption medium for the Barringer IONSCAN, the analytical results using standard reference samples are reproducible. A study was conducted utilizing papers of varying pore sizes and comparing their performance as a desorption material relative to the standard Barringer 50 micron Teflon. Nominal pore sizes ranged from 30 microns down to 2 microns. Results indicate that there is some peak instability in the first two to three windows during the analysis. The severity of the instability was observed to increase as the pore size of the paper is decreased. However, the observed peak instability does not create a situation that results in a decreased reliability or reproducibility in the analytical result.

Jadamec, J. Richard↗

Reconfigurable Metasurface Optics at NASA LaRC Towards Space Image Sensing

Reconfigurable optical metasurfaces are rapidly emerging as a major frontier in photonics research, development, and applications. They promise compact, lightweight, and energy-efficient reconfigurable optical systems with unprecedented performance and functions that can be dynamically defined on-demand. Space applications represent an emerging area in which these characteristics are highly prized. The ability to dynamically tune optical functions through selective modulation of electromagnetic waves is crucial to the advancement of a variety of sensing applications, from imaging spectrometers to light detection and ranging (LiDAR). This presentation introduces a reconfigurable metasurface optic project led by a research team at NASA Langley Research Center (NASA LaRC) since 2019. It covers advances in phase change material-based reconfigurable optics, performance data on reliability enhancement of photonic devices, image sensing system architectures, and mission concepts enabled through these advances.

metasurface↗

Development of Polyimide Foam for Aircraft Sidewall Applications

In this paper, the use of polyimide foam as a lining in double panel applications is considered. It is being investigated here as a replacement for aircraft grade glass fiber and has a number of attractive functional attributes, not the least of which is its high fire resistance. The test configuration studied here consisted of two 1mm (0.04 in.) thick, flat aluminum panels separated by 12.7 cm (5.0 in.) with a 7.6 cm (3.0 in.) thick layer of foam centered in that space. Random incidence transmission loss measurements were conducted on this buildup, and conventional poro-elastic models were used to predict the performance of the lining material. Results from two densities of foam are considered. The Biot parameters of the foam were determined by a combination of direct measurement (for density, flow resistivity and Young s modulus) and inverse characterization procedures (for porosity, tortuosity, viscous and thermal characteristic length, Poisson s ratio and loss factor). The inverse characterization procedure involved matching normal incidence standing wave tube measurements of absorption coefficient and transmission loss of the isolated foam with finite element predictions. When the foam parameters determined in this way were used to predict the performance of the complete double panel system, reasonable agreement was obtained between the measured transmission loss and predictions made using a commercial statistical energy analysis code.

Silcox, Richard↗

Materials Research Capabilities

Lewis Research Center, in partnership with U.S. industry and academia, has long been a major force in developing advanced aerospace propulsion and power systems. One key aspect that made many of these systems possible has been the availability of high-performance, reliable, and long-life materials. To assure a continuing flow of new materials and processing concepts, basic understanding to guide such innovation, and technological support for development of major NASA systems, Lewis has supported a strong in-house materials research activity. Our researchers have discovered new alloys, polymers, metallic composites, ceramics, coatings, processing techniques, etc., which are now also in use by U.S. industry. This brochure highlights selected past accomplishments of our materials research and technology staff. It also provides many examples of the facilities available with which we can conduct materials research. The nation is now beginning to consider integrating technology for high-performance supersonic/hypersonic aircraft, nuclear space power systems, a space station, and new research areas such as materials processing in space. As we proceed, I am confident that our materials research staff will continue to provide important contributions which will help our nation maintain a strong technology position in these areas of growing world competition. Lewis Research Center, in partnership with U.S. industry and academia, has long been a major force in developing advanced aerospace propulsion and power systems. One key aspect that made many of these systems possible has been the availability of high-performance, reliable, and long-life materials. To assure a continuing flow of new materials and processing concepts, basic understanding to guide such innovation, and technological support for development of major NASA systems, Lewis has supported a strong in-house materials research activity. Our researchers have discovered new alloys, polymers, metallic composites, ceramics, coatings, processing techniques, etc., which are now also in use by U.S. industry. This brochure highlights selected past accomplishments of our materials research and technology staff. It also provides many examples of the facilities available with which we can conduct materials research. The nation is now beginning to consider integrating technology for high-performance supersonic/hypersonic aircraft, nuclear space power systems, a space station, and new research areas such as materials processing in space.

Stofan, Andrew J.↗

Impact wear of iron rich superalloys

The impact-sliding wear resistance of chill cast and aligned eutectic Fe-base superalloys against M42 and 17-4 PH steel counterface materials is examined. The aligned material tests were run with carbide fibers perpendicular to the counterface contact surface and the characterization focused on fracture processes as observed in the subsurface microstructure of the worn materials. Metallographic analyses were performed on specimens exposed to various numbers of repetitive impact load cycles, and for comparison, two other aligned composites were tested with the same fiber orientation under identical test conditions against hardened M42 tool steel. A strong improvement was found in wear resistance of an aligned eutectic structure as compared to the corresponding randomized chill cast structure. Experiments with the softer 17-4 counterface were characterized by transfer onto the Fe-base superalloy, and the cracks formed were oriented transverse to the relative sliding direction and occurred in a periodic fashion. Observations in subsurface regions of the worn materials indicated crack intergranularity with an occasional transgranular fracture of the M7C3 carbide phase.

Wayne, S. F.↗

Electrochemical Impedance Spectroscopy of Alloys in a Simulated Space Shuttle Launch Environment

Type 304L stainless steel (304L SS) tubing is currently used in various supply lines that service the Orbiter at NASA's John F. Kennedy Space Center Launch Pads in Florida (USA). The atmosphere at the Space Shuffle launch site is very corrosive due to a combination of factors, such as the proximity of the Atlantic Ocean and the concentrated hydrochloric acid produced by the fuel combustion reaction in the solid rocket boosters. The acidic chloride environment is aggressive to most metals and causes severe pitting in many of the common stainless steel alloys such as 304L SS. Stainless steel tubing is susceptible to pitting corrosion that can cause cracking and rupture of both high-pressure gas and fluid systems. Outages in the systems where failures occur can impact the normal operation of the shuttle and launch schedules. The use of a more corrosion resistant tubing alloy for launch pad applications would greatly reduce the probability of failure, improve safety, lessen maintenance costs, and reduce downtime. A study which included ten alloys was undertaken to find a more corrosion resistant material to replace the existing 304L SS tubing. The study included atmospheric exposure at NASA's John F. Kennedy Space Center outdoor corrosion test site near the launch pads and electrochemical measurements in the laboratory which included DC techniques and electrochemical impedance spectroscopy (EIS). This paper presents the results from EIS measurements on three of the alloys: AL6XN (UN N08367), 254SMO (UNS S32l54), and 304L SS (UNS S30403). Type 304L SS was included in the study as a control. The alloys were tested in three electrolyte solutions which consisted of neutral 3.55% NaC1, 3.55% NaCl in O.1N HC1, and 3.55% NaCl in 1.ON HC1. The solutions were chosen to simulate environments that were expected to be less, similar, and more aggressive, respectively, than those present at the Space Shuttle launch pads. The results from the EIS measurements were analyzed to evaluate the corrosion susceptibility of the alloys and to predict the long-term corrosion performance of the subject materials. The results from the EIS measurements for the three alloys indicated that the higher-alloyed 254SMO and AL6XN exhibited a significantly improved resistance to corrosion than the 304L SS as the concentration of hydrochloric acid in the 3.55% NaC1 solution was increased. The polarization resistance values obtained from the EIS measurements were consistent with those from linear polarization measurements, and were indicative of the actual long-term corrosion performance of the alloys during a two-year atmospheric exposure study.

Calle, L. M.↗

Bubble behavior during solidification in low gravity

The trapping and behavior of gas bubbles were studied during low-gravity solidification of carbon tetrabromide, a transparent metal-model material. The experiment was performed during a NASA-sponsored sounding rocket flight and involved gradient freeze solidification of a gas-saturated melt. Gas bubbles were evolved at the solid-liquid interface during the low-gravity interval. No large-scale thermal migration of bubbles, bubble pushing by the solid-liquid interface, or bubble detachment from the interface were observed during the low-gravity experiment. A unique bubble motion-fluid flow event occurred in one specimen: a large bubble moved downward and caused some circulation of the melt. The gas bubbles that were trapped by the solid in commercial-purity material formed voids that had a cylindrical shape, in contrast to the spherical shape that had been observed in a prior low-gravity experiment. These shapes were not influenced by the gravity level (0.0001 g-0 vs g-0), but were dependent upon the initial temperature gradient. In higher purity material, however, the shape of the voids changed from cylindrical in 1g to spherical in low gravity.

Papazian, J. M.↗

Calibration Probe Uncertainty and Validation for the Hypersonic Material Environmental Test System

This paper presents an uncertainty analysis of the stagnation-point calibration probe surface predictions for conditions that span the performance envelope of the Hypersonic Materials Environmental Test System facility located at NASA Langley Research Center. A second-order stochastic expansion was constructed over 47 uncertain parameters to evaluate the sensitivities, identify the most significant uncertain variables, and quantify the uncertainty in the stagnation-point heat flux and pressure predictions of the calibration probe for a low- and high-enthalpy test condition. A sensitivity analysis showed that measurement bias uncertainty is the most significant contributor to the stagnation-point pressure and heat flux variance for the low-enthalpy condition. For the high-enthalpy condition, a paradigm shift in sensitivities revealed the computational fluid dynamics model input uncertainty as the main contributor. A comparison between the prediction and measurement of the stagnation-point conditions under uncertainty showed that there was evidence of statistical disagreement. A validation metric was proposed and applied to the prediction uncertainty to account for the statistical disagreement when compared to the possible stagnation-point heat flux and pressure measurements.

Brune, Andrew J.↗

High-Performance Thermoelectric Semiconductors

Figures of merit almost double current state-of-art thermoelectric materials. IrSb3 is semiconductor found to exhibit exceptional thermoelectric properties. CoSb3 and RhSb3 have same skutterudite crystallographic structure as IrSb3, and exhibit exceptional transport properties expected to contribute to high thermoelectric performance. These three compounds form solid solutions. Combination of properties offers potential for development of new high-performance thermoelectric materials for more efficient thermoelectric power generators, coolers, and detectors.

Fleurial, Jean-Pierre↗

Computational Materials Research

High temperature thermoplastic polyimide polymers are incorporated in engineering structures in the form of matrix materials in advanced fiber composites and adhesives in bonded joints. Developing analytical tools to predict long term performance and screen for final materials selection for polymers is the impetus for intensive studies at NASA and major industry based airframe developers. These fiber-reinforced polymeric composites (FRPCs) combine high strength with lightweight. In addition, they offer corrosion and fatigue resistance, a reduction in parts count, and new possibilities for control through aeroelastic tailoring and "smart" structures containing fully-integrated sensors and actuators. However, large-scale acceptance and use of polymer composites has historically been extremely slow. Reasons for this include a lack of familiarity of designers with the materials; the need for new tooling and new inspection and repair infrastructures; and high raw materials and fabrication costs.

Veazie, David R.↗

Experiment Evaluation of Bifurcation in Sands

The basic principles of bifurcation analysis have been established by several investigators, however several issues remain unresolved, specifically how do stress level, grain size distribution, and boundary conditions affect general bifurcation phenomena in pressure sensitive and dilatant materials. General geometrical and kinematics conditions for moving surfaces of discontinuity was derived and applied to problems of instability of solids. In 1962, the theoretical framework of bifurcation by studying the acceleration waves in elasto-plastic (J2) solids were presented. Bifurcation analysis for more specific forms of constitutive behavior was examined by studying localization in pressure-sensitive, dilatant materials, however, analyses were restricted to plane deformation states only. Bifurcation analyses were presented and applied to predict shear band formations in sand under plane strain condition. The properties of discontinuous bifurcation solutions for elastic-plastic solids under axisymmetric and plane strain loading conditions were studied. The study focused on theory, but also references and comparisons to experiments were made. The current paper includes a presentation of a summary of bifurcation analyses for biaxial and triaxial (axisymmetric) loading conditions. The Coulomb model is implemented using incremental piecewise scheme to predict the constitutive relations and shear band inclination angles. Then, a comprehensive evaluation of bifurcation phenomena is presented based on data from triaxial experiments performed under microgravity conditions aboard the Space Shuttle under very low effective confining pressure (0.05 to 1.30 kPa), in which very high peak friction angles (47 to 75 degrees) and dilatancy angles (30 to 31 degrees) were measured. The evaluation will be extended to include biaxial experiments performed on the same material under low (10 kPa) and moderate (100 kPa) confining pressures. A comparison between the behavior under biaxial and triaxial loading conditions will be presented, and related issues concerning influence of confining pressure will be discussed.

Alshibi, Khalid A.↗