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At least 1,279 records · Page 71

SERENA: Particle Instrument Suite for Determining the Sun-Mercury Interaction from BepiColombo

The ESA-JAXA BepiColombo mission to Mercury will provide simultaneous measurements from two spacecraft, offering an unprecedented opportunity to investigate magnetospheric and exospheric particle dynamics at Mercury as well as their interactions with solar wind, solar radiation, and interplanetary dust. The particle instrument suite SERENA (Search for Exospheric Refilling and Emitted Natural Abundances) is flying in space on-board the BepiColombo Mercury Planetary Orbiter (MPO) and is the only instrument for ion and neutral particle detection aboard the MPO. It comprises four independent sensors: ELENA for neutral particle flow detection, Strofio for neutral gas detection, PICAM for planetary ions observations, and MIPA, mostly for solar wind ion measurements. SERENA is managed by a System Control Unit located inside the ELENA box. In the present paper the scientific goals of this suite are described, and then the four units are detailed, as well as their major features and calibration results. Finally, the SERENA operational activities are shown during the orbital path around Mercury, with also some reference to the activities planned during the long cruise phase.

79 ASTRONOMY AND ASTROPHYSICS↗

Flying Cages in Traveling Wave Ion Mobility: Influence of the Instrumental Parameters on the Topology of the Host–Guest Complexes

Supramolecular mass spectrometry has emerged in the last decade as an orthogonal method to access, at the molecular level, the structures of noncovalent complexes extracted from the condensed phase to the rarefied gas phase using electrospray ionization. It is often considered that the soft nature of the ESI source confers to the method the capability to generate structural data comparable to those in the condensed phase. In the present paper, using the ammonium ion/cucurbituril combination as a model system, we investigate using ion mobility and computational chemistry the influence of the instrumental parameters on the topology, i.e., internal versus external association, of gaseous host/guest complex ions. MS and theoretical data are confronted to condensed phase data derived from nuclear magnetic resonance spectroscopy to assess whether the instrumental parameters can play an insidious role when trying to derive condensed phase data from mass spectrometry results. .

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

An overview of polarized neutron instruments and techniques in Asia Pacific

Polarized neutron scattering is an indispensable tool for exploring a vast range of scientific phenomena. With its dynamic scientific community and significant governmental support as well as the rapid economic growth, the Asia–Pacific region has become a key player in the worldwide neutron scattering arena. From traditional research reactors to cutting-edge spallation neutron sources, this region is home to a myriad of advanced instruments offering a wide range of polarized neutron capabilities. This review aims to provide a comprehensive overview of the development and current status of polarized neutron instruments and techniques in the Asia–Pacific region, emphasizing the important role of the Asia–Pacific region in shaping the landscape of global polarized neutron scattering development.

47 OTHER INSTRUMENTATION↗

Nuclear characterization of a general-purpose instrumentation and materials testing location in TREAT

The Transient Reactor Test facility (TREAT) was constructed in the late 1950s, provided thousands of transient irradiations before being placed in standby in 1994, and resumed operations in 2017 in order to reclaim its crucial role in nuclear-heated safety research. The latter half of TREAT’s historic operation was best known for integral-scale testing of fuel specimens under postulated reactor plant accident conditions, while TREAT’s earlier history included extensive simpler phenomena identification tests that elucidated fundamental behaviors and paved the way for these integral-scale tests. Advances in modern computational capabilities and a resurgence of interest in novel reactor technology have created an opportunity for emphasizing modernized science-based and separate effects test capabilities once again at TREAT. An innovative approach to this type of testing has been developed to leverage minor radioactivity built-in during brief TREAT irradiations in low activation hardware to facilitate handling for materials and instrumentation testing. This capability, termed the Minimal Activation Retrievable Capsule Holder (MARCH) irradiation vehicle system, will be used for inaugural fueled experiments in TREAT’s modern era as well as novel approaches to study materials undergoing neutron irradiation and instrumentation development and qualifications. This paper describes a comprehensive nuclear characterization, obtained via computational modeling, of the test position in the MARCH system. Though directly applicable to the MARCH system, the results also provide general quantification of the nuclear performance of the reactor and potential test materials, crucial for evaluating potential experiment design and response in TREAT. The neutron and photon flux environment was calculated via MCNP with ENDF/B-VII.1 nuclear data. Wire heating rate and DPA calculations were also performed and evaluated using historic TREAT test data. Furthermore, these calculations were performed to provide steady-state baseline reference values typical in both half- and full-slotted TREAT core configurations, enabling design scoping analysis prior to development of more specific design testing needs and transient testing experimentation.

11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS↗

Benchmarking sensor fusion capabilities of an integrated instrumentation package

Quantifying and mitigating environmental risks introduced by marine energy conversion systems requires a variety of sensors (active acoustic, passive acoustic, and optical). The operation of these sensors must satisfy three directives to be effective: (1) do not alter the environment through operation of sensors; (2) capture rare events; and (3) do not accrue unmanageable volumes of low-value data. This requires integrating sensors into a single package, rather than operating them independently. The Adaptable Monitoring Package is an integrated instrumentation package that combines a multibeam sonar, acoustic camera, current profiler, optical cameras, and an array of hydrophones. The capabilities and limitations of the AMP sensors were benchmarked using cooperative targets, and real-time target tracking and detection was used to detect opportunistic targets (e.g., diving birds, seals). During an initial deployment, automatic detection of opportunistic targets achieved a 58% true positive rate and a 99% true negative rate (100% corresponding to an ideal system in both cases). In post-processing, target tracking data were used to evaluate automatic target classification capabilities using a k-nearest neighbor algorithm. Findings suggest that real-time target classification should be possible and enable integrated instrumentation systems to meet the monitoring needs of marine energy deployments.

16 TIDAL AND WAVE POWER↗

Simulation of differential die-away instrument’s response to asymmetrically burned spent nuclear fuel

Here, previous simulation studies of Differential Die–Away (DDA) instrument’s response to active interrogation of spent nuclear fuel from a pressurized water reactor (PWR) yielded promising results in terms of its capability to accurately measure or estimate basic spent fuel assembly (SFA) characteristics, such as multiplication, initial enrichment (IE) and burn-up (BU) as well as the total plutonium content. These studies were however performed only for a subset of idealized SFAs with a symmetric BU with respect to its longitudinal axis. Therefore, to complement the previous results, additional simulations have been performed of the DDA instrument’s response to interrogation of asymmetrically burned spent nuclear fuel in order to determine whether detailed assay of SFAs from all 4 sides will be necessary in real life applications or whether a cost and time saving single sided assay could be used to achieve results of similar quality as previously reported in case of symmetrically burned SFAs.

12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE W↗

Development and testing of a fission-like neutron field for dosimetry and instrument calibrations based on deuterium-tritium generator

For nearly five decades 252 Cf sources have been used for testing and calibration over a wide range of neutron detection devices used for nuclear safety and radiation protection. However, the vastly increased cost of 252 Cf sources, its short half-life, and concerns about future shortage have prompted nuclear facilities and radiological calibration laboratories that rely on high-intensity neutron sources to seek alternatives. There appear to be no other radionuclide neutron sources that would match “like-to-like” 252 Cf performance characteristics. Alternatives of producing a fission-like neutron spectrum based on commercially available deuterium-tritium (D-T) generators, and without any fissionable materials or beryllium, have been explored. This paper describes efforts of designing the spectrum shaping assembly, its construction and installation. The produced neutron field was evaluated both from the perspective of the neutron fluence spectrum and the resulting dosimetric outcome. Finally, it was tested for practical application by examining response of various health physics instruments and personal monitoring devices in comparison to the response of those devices when exposed to 252 Cf. In conclusion, the response of survey-type instruments tested within the prototype, surrogate fission, reference field are acceptably close to their response in the targeted 252 Cf field.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Recalibration of the Mars Science Laboratory ChemCam instrument with an expanded geochemical database

The ChemCam Laser-Induced Breakdown Spectroscopy (LIBS) instrument onboard the Mars Science Laboratory (MSL) rover Curiosity has obtained > 300,000 spectra of rock and soil analysis targets since landing at Gale Crater in 2012, and the spectra represent perhaps the largest publicly-available LIBS datasets. The compositions of the major elements, reported as oxides, have been re-calibrated using a laboratory LIBS instrument, Mars-like atmospheric conditions, and a much larger set of standards (408) that span a wider compositional range than previously employed. The new calibration uses a combination of partial least squares (PLS1) and Independent Component Analysis (ICA) algorithms, together with a calibration transfer matrix to minimize differences between the conditions under which the standards were analyzed in the laboratory and the conditions on Mars. While the previous model provided good results in the compositional range near the average Mars surface composition, the new model fits the extreme compositions far better. Examples are given for plagioclase feldspars, where silicon was previously significantly over-estimated, and for calcium-sulfate veins, where silicon compositions near zero were inaccurate. Here, the uncertainties of major element abundances are described as a function of the abundances, and are overall significantly lower than the previous model, enabling important new geochemical interpretations of the data.

47 OTHER INSTRUMENTATION↗

Analysis of the failures and corrective actions for the LHC cryogenics radiation tolerant electronics and its field instruments

The LHC cryogenic system radiation tolerant electronics and their associated field instruments have been in nominal conditions since before the commissioning of the first LHC beams in September 2008. This system is made of about 15’000 field instruments (thermometers, pressure sensors, liquid helium level gauges, electrical heaters and position switches), 7’500 electronic cards and 853 electronic crates. Since mid-2008 a software tool has been deployed, this allows an operator to report a problem and then lists the corrective actions. The tool is a great help in detecting recurrent problems that may be tackled by a hardware or software consolidation. The corrective actions range from simple resets, exchange of defective equipment, repair of electrical connectors, etc. However a recurrent problem that heals by itself is present on some channels. This type of fault is extremely difficult to diagnose and it appears as a temporary opening of an electrical circuit; its duration can range from a few minutes to several months. This paper presents the main type of problems encountered during the last four years, their evolution over time, the various hardware or software consolidations that have resulted and whether they have had an impact in the availability of the LHC beam.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Digital configurable instrument for emulation of signals from radiation detectors

The paper presents a digital instrument characterized by a specially designed architecture that is able to emulate in real time signals from a generic radiation detection system. The instrument is not a pulse generator of recorded shapes but a synthesizer of random pulses compliant to programmable statistics for height and starting time of events. Completely programmable procedures for emulation of noise, disturbances, and reference level variation are implemented.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

A thermal control system for long-term survival of scientific instruments on lunar surface

A thermal control system is being developed for scientific instruments placed on the lunar surface. This thermal control system, Lunar Mission Survival Module (MSM), was designed for scientific instruments that are planned to be operated for over a year in the future Japanese lunar landing mission SELENE-2. For the long-term operations, the lunar surface is a severe environment because the soil (regolith) temperature varies widely from nighttime −200 degC to daytime 100 degC approximately in which space electronics can hardly survive. The MSM has a tent of multi-layered insulators and performs a “regolith mound”. Temperature of internal devices is less variable just like in the lunar underground layers. The insulators retain heat in the regolith soil in the daylight, and it can keep the device warm in the night. We conducted the concept design of the lunar survival module, and estimated its potential by a thermal mathematical model on the assumption of using a lunar seismometer designed for SELENE-2. Thermal vacuum tests were also conducted by using a thermal evaluation model in order to estimate the validity of some thermal parameters assumed in the computed thermal model. The numerical and experimental results indicated a sufficient survivability potential of the concept of our thermal control system.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Magnetic and electric bulge-test instrument for the determination of coupling mechanical properties of functional free-standing films and flexible electronics

For the first time a novel multi-field bulge-test instrument which enables measurements of the biaxial mechanical properties and electro-magnetic-mechanical coupling effect of free-standing films in external magnetic/electric fields was proposed. The oil pressure was designed with two ranges, 0–1 MPa for elastic small deformation and 0–7 MPa for plastic/damage large deformation. A magnetic field that was horizontal and uniform in the film plane was supplied by a hollow cylindrical magnet. The magnitude could be changed from 0 to 10 000 Oe by adjusting the position of the testing film. Meanwhile, an electric field applied on the film was provided by a voltage source (Maximum voltage: 1000 V; Maximum current: 1 A). Various signals related to deformation, mechanical loading, magnetic field, and electric field could be measured simultaneously without mutual interference, which was confirmed by the coincidence of the measured P-H curves for titanium (Ti)/nickel (Ni) specimens with/without external fields. A hardening phenomenon under magnetic/electric fields was observed for Ni and lead zirconate titanate specimens. The multi-field bulge-test instrument will provide a powerful research tool to study the deformation mechanism of functional films and flexible electronics in the coupling field.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Development of pulsed neutron uranium logging instrument

This article introduces a development of pulsed neutron uranium logging instrument. By analyzing the temporal distribution of epithermal neutrons generated from the thermal fission of {sup 235}U, we propose a new method with a uranium-bearing index to calculate the uranium content in the formation. An instrument employing a D-T neutron generator and two epithermal neutron detectors has been developed. The logging response is studied using Monte Carlo simulation and experiments in calibration wells. The simulation and experimental results show that the uranium-bearing index is linearly correlated with the uranium content, and the porosity and thermal neutron lifetime of the formation can be acquired simultaneously.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Versatile common instrumentation for optical detection of pH and dissolved oxygen

The recent trend toward use of disposable and miniature bioreactors requires the use of appropriate sensors. pH and dissolved oxygen (DO) are often measured using optical chemical sensors due to their small form factor and convenience in use. These sensors are often interrogated using a specialized opto-electronic transducer that is designed around the optical sensor. In this contribution, we are presenting a new class of opto-electronic transducers that are usable with several different chemical sensors without the need to switch the optics or hardware when changing the type of the chemical sensor. This allows flexibility closer to the lab-grade devices while the size is closer to a dedicated sensor. This versatile instrumentation is capable of seamlessly switching between the pH and DO measurement modes and is capable of auto recognition of the sensor type. The principle of ratiometric fluorescence is used for pH measurements, and that of fluorescence lifetime for DO measurements. An approach to obtain identical calibrations between several devices is also presented. The described hardware constitutes common instrumentation for measuring either pH or DO and has been tested in actual bioprocesses. It has been found adequate for continuous bioprocess monitoring.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗

Development of electrical-erosion instrument for direct write micro-patterning on large area conductive thin films

We have developed a complete instrument to perform direct, dry, and cost-effective lithography on conductive materials, based on localized electrical discharges, which avoids using masks or chemicals typical of conventional photolithography. The technique is considered fully compatible with substrate transport based systems, like roll-to-roll technology. The prototype is based on two piezo nano-steppers coupled to three linear micro-stages to cover a large scale operation from micrometers to centimeters. The operation mode consists of a spring probe biased at low DC voltage with respect to a grounded conductive layer. The tip slides on the target layer keeping contact with the material in room conditions, allowing continuous electric monitoring of the process, and also real-time tilt correction via software. The sliding tip leaves an insulating path (limited by the tip diameter) along the material, enabling to draw electrically insulated tracks and pads. The physical principle of operation is based in the natural self-limitation of the discharge due to material removal or insulation. The so produced electrical discharges are very fast, in the range of μs, so features may be performed at speeds of few cm/s, enabling scalability to large areas. The instrument has been tested on different conducting materials as gold, indium tin oxide, and aluminum, allowing the fabrication of alphanumeric displays based on passive matrix of organic light emitting diodes without the use of masks or photoresists. We have verified that the highest potential is achieved on graphene, where no waste material is detected, producing excellent well defined edges. This allows manufacturing graphene micro-ribbons with a high aspect ratio up to 1200:1.

36 MATERIALS SCIENCE↗

An adaptable multiple power source for mass spectrometry and other scientific instruments

Power supplies are commonly used in the operation of many types of scientific equipment, including mass spectrometers and ancillary instrumentation. A generic modern mass spectrometer comprises an ionization source, such as electrospray ionization (ESI), ion transfer devices such as ion funnels and multipole ion guides, and ion signal detection apparatus. Very often such platforms include, or are interfaced with ancillary elements in order to manipulate samples before or after ionization. In order to operate such scientific instruments, numerous direct current (DC) channels and radio frequency (RF) signals are required, along with other controls such as temperature regulation. In particular, DC voltages in the range of ±400 V, along with MHz range RF signals with peak-to-peak amplitudes in the hundreds of volts range are commonly used to transfer ionized samples under vacuum. Additionally, an ESI source requires a high voltage (HV) DC source capable of producing several thousand volts and heaters capable of generating temperatures up to 300°C. All of these signals must be properly synchronized and managed in order to carry out ion trapping, accumulation and detection.

47 OTHER INSTRUMENTATION↗

An FPGA-based instrumentation platform for use at deep cryogenic temperatures

We describe the operation of a cryogenic instrumentation platform incorporating commercially available field-programmable gate arrays (FPGAs). The functionality of the FPGAs at temperatures approaching 4 K enables signal routing, multiplexing, and complex digital signal processing in close proximity to cooled devices or detectors within the cryostat. The performance of the FPGAs in a cryogenic environment is evaluated, including clock speed, error rates, and power consumption. Although constructed for the purpose of controlling and reading out quantum computing devices with low latency, the instrument is generic enough to be of broad use in a range of cryogenic applications.

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND ↗