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Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.

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At least 1,261 records · Page 70
All sourcesNASA NTRSDOE OSTI
NASA NTRS1960

Halogen Containing Gases as Lubricants for Crystallized Glass Ceramic Metal Combinations at Temperatures to 1500 F

Pyroceram 9608 (a crystallized glass ceramic) has been considered for use in high-temperature bearing and seal applications. One of the problems encountered with Pyroceram is the lack of availability of lubricants for the temperature range in which this material becomes practical. Experiments were conducted with Pyroceram sliding on various nickel- and cobalt-base alloys using reactive halogen-containing gases as lubricants. Friction and wear data were obtained as a function of sliding velocity and temperature. Studies were made with a hemispherical rider (3/16-in. rad., Pyroceram 9608) sliding in a circumferential path on the flat surface of a rotating disk (2(1/2) in. diam., nickel- or cobalt-base alloys). The specimens were run in an atmosphere of the various gases with a load of 1200 grams, a sliding velocity of 3200 feet per minute, and temperatures from 75 to 1500 F. The gas CF2Br-CF2Br was found to be an effective lubricant for Pyroceram 9608 sliding on Hastelloy R-235 and Inconel X up to 1400 F. The gas CF2Cl-CF2Cl provided effective lubrication for Pyroceram sliding on various cobalt-base alloys at 1000 F.

Buckley, Donald H.↗
NASA NTRS1999

Production of Normal Mammalian Organ Culture Using a Medium Containing Mem-Alpha, Leibovitz L 15, Glucose Galactose Fructose

Normal mammalian tissue and the culturing process has been developed for the three groups of organ, structural and blood tissue. The cells are grown in vitro under micro- gravity culture conditions and form three dimensional cells aggregates with normal cell function. The microgravity culture conditions may be microgravity or simulated microgravity created in a horizontal rotating wall culture vessel. The medium used for culturing the cells, especially a mixture of epithelial and mesenchymal cells contains a mixture of Mem-alpha and Leibovits L15 supplemented with glucose, galactose and fructose.

Goodwin, Thomas J.↗
NASA NTRS1999

Dimensionally Stable Ether-Containing Polyimide Copolymers

Novel polyimide copolymers containing ether linkages were prepared by the reaction of an equimolar amount of dianhydride and a combination of diamines. The polyimide copolymers described herein possess the unique features of low moisture uptake, dimensional stability, good mechanical properties, and moderate glass transition temperatures. These materials have potential application as encapsulants and interlayer dielectrics.

Fay, Catharine C.↗
NASA NTRS1998

Synthesis of Polymers Containing Covalently Bonded NLO Chromophores

Polymers containing covalently bonded nonlinear optical (NLO) chromophores are expected to possess special properties such as greater stability, better mechanical processing, and easier film formation than their non-polymeric equivalent. For the present work, polymethylmethacrylate (PMMA) was selected as the basic polymer unit on which to incorporate different NLO chromophores. The NLO components were variations of DIVA {[2-methoxyphenyl methylidene]-propanedinitrile} which we prepared from vanillin derivatives and malononitrile. These were esterified with methacrylic acid and polymerized either directly or with methyl methacrylate to form homopolymers or copolymers respectively. Characterization of the polymers and NLO property studies are underway.

Denga, Xiao-Hua↗
NASA NTRS2001

Substituent and Solvent Effects on Excited State Charge Transfer Behavior of Highly Fluorescent Dyes Containing Thiophenylimidazole-Based Aldehydes

The excited state charge transfer for a series of highly fluorescent dyes containing thiophenylimidazole moiety was investigated. These systems follow the Twisted Intramolecular Charge Transfer (TICT) model. Dual fluorescence was observed for each substituted dye. X-ray structures analysis reveals a twisted ground state geometry for the donor substituted aryl on the 4 and 5 position at the imidazole ring. The excited state charge transfer was modeled by a linear solvation energy relationship using Taft's pi and Dimroth's E(sub T)(30) as solvent parameters. There is linear relation between the energy of the fluorescence transition and solvent polarity. The degree of stabilization of the excited state charge transfer was found to be consistent with the intramolecular molecular charge transfer. Excited dipole moment was studied by utilizing the solvatochromic shift method.

Santos, Javier↗
NASA NTRS1996

The Application of DFT to Systems Containing Metal Atoms

The application of density functional theory (DFT) to a series of metal containing systems will be described. The focus will be on the calculation of accurate bond energies, especially metal-ligand successive bond energies. The DFT results will be compared with experiment and other levels of theory. If time permits, metal clusters will also be discussed.

Ricca, Alessandra↗
NASA NTRS2002

The Relative Humidity of the Atmosphere in the Encasements Containing the Declaration of Independence, the US Constitution (Pages 1 and 4), and the Bill of Rights

In 1951, the four pages of the US Constitution, the Letter of Transmittal, the Bill of Rights and the Declaration of Independence, collectively called the 'Charters of Freedom,' were hermetically sealed individually in glass encasements. The atmosphere in the encasements consisted of a mixture of helium with water vapor at a relative humidity between 25 and 35% at room temperature. In 1998, Margaret Kelly of the National Archives and Records Administration (NARA), contacted Dr. Joel S. Levine at NASA Langley Research Center (LaRC) to request assistance in determining the chemical composition of the atmosphere inside the encasements. Several different Langley learns were assembled to address that request. each using a different measurement technique. This report describes the method and results of one team's relative humidity measurements on encasements containing pages 1 and 4 of the US Constitution, the Bill of Rights, and the Declaration of Independence performed at NARA, College Park. Maryland, on July 23, 2001.

West, James W.↗
NASA NTRS2002

Oxidation of a Silica-Containing Material in a Mach 0.3 Burner Rig

A primarily silica-containing material with traces of organic compounds, as well as aluminum and calcium additions, was exposed to a Mach 0.3 burner rig at atmospheric pressure using jet fuel. The sample was exposed for 5 continuous hours at 1370 C. Post exposure x-ray diffraction analyses indicate formation of cristobalite, quartz, NiO and Spinel (Al(Ni)CR2O4). The rig hardware is composed of a nickel-based superalloy with traces of Fe. These elements are indicated in the energy dispersive spectroscopy (EDS) results. This material was studied as a candidate for high temperature applications under an engine technology program.

Nguyen, QuynhGiao N.↗
NASA NTRS1985

Self Contained Ecosystems

A self contained ecosystem developed at Jet Propulsion Laboratory is manufactured by Engineering and Research Associates. It is essentially a no-care aquarium which requires only natural or fluorescent light.

Source record↗
NASA NTRS2002

Polyimides Containing Pendent Phosphine Oxide Groups for Space Applications

As part of an ongoing materials development activity to produce high performance polymers that are durable to the space environment, phosphine oxide containing polyimides have been under investigation. A novel dianhydride was prepared from 2,5-dihydroxyphenyldiphenylphosphine oxide in good yield. The dianhydride was reacted with commercially available diamines, and a previously reported diamine was reacted with commercially available dianhydrides to prepare isomeric polyimides. The physical and mechanical properties, particularly thermal and optical properties, of the polymers were determined. One material exhibited a high glass transition temperature, high tensile properties, and low solar absorptivity. The chemistry, physical, and mechanical properties of these resins will be discussed.

Thompson, C. M.↗
NASA NTRS2003

Impact Resistance of Lightweight Hybrid Structures for Gas Turbine Engine Fan Containment Applications

The ballistic impact resistance of hybrid composite sandwich structures was evaluated with the ultimate goal of developing new materials or structures for potential gas turbine engine fan containment applications. The sandwich structures investigated consisted of GLARE-5 laminates as face sheets with lightweight cellular metallic materials such as honeycomb, foam, and lattice block as a core material. The impact resistance of these hybrid sandwich structures was compared to GLARE-5 laminates and 2024-T3 Al sheet, which were tested as a function of areal weight (material thickness). The GLARE-5 laminates exhibited comparable impact properties to that of 2024-T3 Al at low areal weights, even though there were significant differences in the static tensile properties of these materials. The GLARE-5, however, did have a greater ballistic limit than straight aluminum sheet at higher areal weights. Furthermore, there is up to a 25% advantage in ballistic limit for the GLARE-5/foam sandwich structures compared to straight 2024-T3 Al. But no advantage in ballistic limit was observed between any of the hybrid sandwich structures and thicker versions of GLARE-5. Recommendations for future work are provided, based on these preliminary data.

Hebsur, Mohan G.↗
NASA NTRS2002

Sub-millimeter Spectroscopy of Astrophysically Interesting Metal-Containing Molecules

With the advent of SOFIA and Herschel, new spectral windows will be opened for spectroscopy in the sub-millimeter region. To conduct science in this band, laboratory measurements must be carried out to provide accurate transition frequencies for molecular identification and physical interpretation. We are presently conducting such measurements using gas-phase submm direct absorption techniques. Of particular interest are simple molecules containing iron-peak elements, including carbides, and metal hydride ions (MH+), both which possess favorable transitions at submm wavelengths.

Ziurys, L. M.↗
NASA NTRS2002

Initial Results on the Extraterrestrial Component of New Sediment Cores Containing Deposits of the Eltanin Impact Event

Background: The impact of the Eltanin asteroid into the Bellingshausen Sea (2.15 Ma) is the only known impact in a deep-ocean (approx. 5 km) basin. In 1995, Polarstern expedition ANT XII/4 made the first geological survey of the suspected impact region. Three sediment cores sampled around the San Martin seamounts (approx. 57.5 S, 91 W) contained well-preserved impact deposits. Sediments of Eocene age and younger were ripped up and redeposited by the impact. The depositional sequence produced by the impact has three units: a chaotic assemblage of sediment fragments up to 50 cm, followed by laminated sands deposited as a turbulent flow, and finally silts and clays that accumulated from dispersed sediments in the water column. The meteoritic impact ejecta, which is composed of shock-melted asteroidal materials and unmelted meteorites, settled through the water column and concentrated near the top of the laminated sands.

Kyte, Frank T.↗
NASA NTRS2003

The Synthesis of Beta-Peptides Containing Guanidino Groups

The synthesis of the beta-peptide 1 by the postsynthetic modification of the corresponding amino-containing peptide 3 is described. The potential of 1 to act as a template for the ligation of complementary negatively-charged peptides is discussed.

Wen, Ke↗
NASA NTRS1961

Residual Static Strength of ALuminum-Alloy Beams Containing Fatigue Cracks in the Tension Covers

Static tests were performed on 31 box beams containing fatigue cracks in order to determine their residual static strengths. The beams were constructed of 7075 and 2024 aluminum alloy according to several designs and employed stringers that were either bonded, riveted, or an integral part of the skin. skin (both aaterials) had the highest residual static strengths, whereas 7075 beams with integrally stiffened covers had the lowest residual static strengths. Except for the integrally stiffened beams, the skin material did not contribute to the residual static strength of the beams because the crack propagated across the skin before maximum load was reached. For the integrally stiffened beams, crack propagation and failure were synonymous. The test results are compared with predictions of the residual static strength. Fair agreement between predicted strength and actual strength was obtained for all beams tested.

Leybold, Herbert A.↗
NASA NTRS2004

Multiscale Modeling of Metallic Materials Containing Embedded Particles

Multiscale modeling at small length scales (10(exp -9) to 10(exp -3) m) is discussed for aluminum matrices with embedded particles. A configuration containing one particle surrounded by about 50 grains and subjected to uniform tension and lateral constraint is considered. The analyses are performed to better understand the effects of material configuration on the initiation and progression of debonding of the particles from the surrounding aluminum matrix. Configurational parameters considered include particle aspect ratio and orientation within the surrounding matrix. Both configurational parameters are shown to have a significant effect on the behavior of the materials as a whole. For elliptical particles with the major axis perpendicular to the direction of loading, a particle with a 1:1 aspect ratio completely debonds from the surrounding matrix at higher loads than particles with higher aspect ratios. As the particle major axis is aligned with the direction of the applied load, increasing amounts of load are required to completely debond the particles.

Phillips, Dawn R.↗
NASA NTRS2004

Effects of Subsurface Sampling & Processing on Martian Simulant Containing Varying Quantities of Water

The presence of water-ice in the Martian subsurface is a subject of much debate and excited speculation. Recent results from the gammaray spectrometer (GRS) on board NASA's Mars Odyssey spacecraft indicate the presence of large amounts of hydrogen in regions of predicted ice stability. The combination of chemistry, low gravitational field (3.71 m/s(exp 2)) and a surface pressure of about 6.36 mbar at the mean radius, place limits on the stability of H2O on the surface, however, results from the GRS indicate that the hydrogen rich phase may be present at a depth as shallow as one meter in some locations on Mars. The potential for water on Mars leads directly to the speculation that life may once have existed there, since liquid water is the unifying factor for environments known to support life on Earth. Lubricant-free drilling has been considered as a means of obtaining water-rich subsurface samples on Mars, and two recent white papers sponsored by the Mars Program have attempted to identify the problems associated with this goal. The two major issues identified were: the engineering challenges of drilling into a water-soil mixture where phase changes may occur; and the potential to compromise the integrity of in-situ scientific analysis due to contamination, volatilization, and mineralogical or chemical changes as a result of processing. This study is a first attempt to simulate lubricantfree drilling into JSC Mars-1 simulant containing up to 50% water by weight. The goal is to address the following: 1) Does sample processing cause reactions or changes in mineralogy which will compromise the interpretation of scientific measurements conducted on the surface? 2) Does the presence of water-ice in the sample complicate (1)? 3) Do lubricant-free drilling and processing leave trace contaminants which may compromise our understanding of sample composition? 4) How does the torque/power required for drilling change as a function of water content and does this lead to unexpected thermal effects?

Menard, J.↗