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All sourcesNASA NTRSDOE OSTI
DOE OSTI2022

A High-Throughput MEMS-Based Differential Scanning Calorimeter for Direct Thermal Characterization of Antibodies

Calorimeters, which can be used for rapid thermal characterization of biomolecules, are getting intense attention in drug development. This paper presents a novel MEMS-based differential scanning calorimeter (DSC) for direct thermal characterization of protein samples. The DSC consisted of a pair of temperature sensors made by vanadium oxide (VOx) film with a temperature coefficient of resistivity of –0.025/K at 300 K, a microfluidic device with high thermal insulation (2.8 K/mW), and a Peltier heater for linear temperature scanning. The DSC exhibited high sensitivity (6.1 µV/µW), low noise (0.4 µW), high scanning rate (45 K/min), and low sample consumption volume (0.63 µL). The MEMS DSC was verified by measuring the temperature-induced denaturation of lysozyme at different pH, and then used to study the thermal stability of a monoclonal antibody (mAb), an antigen-binding fragment (Fab), and a dual variable domain immunoglobulin (DVD-Ig) at pH = 6. The results showed that lysozyme is a stable protein in the pH range of 4.0–8.0. The protein stability study revealed that the transition temperatures of the intact Fab fragment, mAb, and DVD proteins were comparable with conformational stability results obtained using conventional commercial DSC. These studies demonstrated that the MEMS DSC is an effective tool for directly understanding the thermal stability of antibodies in a high-throughput and low-cost manner compared to conventional calorimeters.

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CH↗
NASA NTRS1985

Addressable inverter matrix for process and device characterization

The addressable inverter matrix consists of 222 inverters each accessible with the aid of a shift register. The structure has proven useful in characterizing the variability of inverter transfer curves and in diagnosing processing faults. For good 3-micron CMOS bulk inverters investigated, the percent standard deviation of the inverter threshold voltage was less than one percent and the inverter gain (the slope of the inverter transfer curve at the inverter threshold vltage) was less than 3 percent. The average noise margin for the inverters was near 2 volts for a power supply voltage of 5 volts. The specific faults studied included undersize pull-down transistor widths and various open contacts in the matrix.

Buehler, M. G.↗
NASA NTRS1992

Multidisciplinary tailoring of hot composite structures

A computational simulation procedure is described for multidisciplinary analysis and tailoring of multilayered multimaterial hot composite engine structural components subjected to simultaneous multiple discipline-specific thermal, structural, vibration, and acoustic loadings including the effect of aggressive environments. The simulation is based on a 3D finite element analysis technique in conjunction with structural mechanics codes, thermal/acoustic analysis methods, and tailoring procedures. The integrated multidisciplinary simulation procedure is general-purpose including the coupled effects of nonlinearities in structure geometry, material, loading, and environmental complexities. The composite material behavior is assessed at all composite scales, i.e., the laminate/ply/constituents (fiber/matrix), via a nonlinear material characterization hygro-thermomechanical model. Sample tailoring cases exhibiting nonlinear material/loading/environmental behavior of aircraft engine fan blades, are presented. The various multidisciplinary loadings lead to different tailored designs, even those opposite of each other, as in the case of minimum material cost versus minimum structure weight and in the case of minimum vibration frequency versus minimum acoustic noise.

Singhal, Surendra N.↗
NASA NTRS1996

Advanced AE Techniques in Composite Materials Research

Advanced, waveform based acoustic emission (AE) techniques have been successfully used to evaluate damage mechanisms in laboratory testing of composite coupons. An example is presented in which the initiation of transverse matrix cracking was monitored. In these tests, broad band, high fidelity acoustic sensors were used to detect signals which were then digitized and stored for analysis. Analysis techniques were based on plate mode wave propagation characteristics. This approach, more recently referred to as Modal AE, provides an enhanced capability to discriminate and eliminate noise signals from those generated by damage mechanisms. This technique also allows much more precise source location than conventional, threshold crossing arrival time determination techniques. To apply Modal AE concepts to the interpretation of AE on larger composite specimens or structures, the effects of modal wave propagation over larger distances and through structural complexities must be well characterized and understood. To demonstrate these effects, measurements of the far field, peak amplitude attenuation of the extensional and flexural plate mode components of broad band simulated AE signals in large composite panels are discussed. These measurements demonstrated that the flexural mode attenuation is dominated by dispersion effects. Thus, it is significantly affected by the thickness of the composite plate. Furthermore, the flexural mode attenuation can be significantly larger than that of the extensional mode even though its peak amplitude consists of much lower frequency components.

Prosser, William H.↗
NASA NTRS2009

Three MMIC Amplifiers for the 120-to-200 GHz Frequency Band

Closely following the development reported in the immediately preceding article, three new monolithic microwave integrated circuit (MMIC) amplifiers that would operate in the 120-to-200-GHz frequency band have been designed and are under construction at this writing. The active devices in these amplifiers are InP high-electron-mobility transistors (HEMTs). These amplifiers (see figure) are denoted the LSLNA150, the LSA200, and the LSA185, respectively. Like the amplifiers reported in the immediately preceding article, the LSLNA150 (1) is intended to be a prototype of low-noise amplifiers (LNAs) to be incorporated into spaceborne instruments for sensing cosmic microwave background radiation and (2) has potential for terrestrial use in electronic test equipment, passive millimeter-wave imaging systems, radar receivers, communication receivers, and systems for detecting hidden weapons. The HEMTs in this amplifier were fabricated according to 0.08- m design rules of a commercial product line of InP HEMT MMICs at HRL Laboratories, LLC, with a gate geometry of 2 fingers, each 15 m wide. On the basis of computational simulations, this amplifier is designed to afford at least 15 dB of gain, with a noise figure of no more than about 6 dB, at frequencies from 120 to 160 GHz. The measured results of the amplifier are shown next to the chip photo, with a gain of 16 dB at 150 GHz. Noise figure work is ongoing. The LSA200 and the LSA185 are intended to be prototypes of transmitting power amplifiers for use at frequencies between about 180 and about 200 GHz. These amplifiers have also been fabricated according to rules of the aforesaid commercial product line of InP HEMT MMICs, except that the HEMTs in these amplifiers are characterized by a gate geometry of 4 fingers, each 37 m wide. The measured peak performance of the LSA200 is characterized by a gain of about 1.4 dB at a frequency of 190 GHz; the measured peak performance of the LSA185 is characterized by a gain of about 2.7 dB at a frequency of 181 GHz. The measured gain results of each chip are shown next to their respective photos.

Samoska, Lorene↗
NASA NTRS2011

Macro vs. Micro: Relating the Spectral Properties of Vesta and the HED Meteorite

We present the main results obtained comparing the visible-near infrared (VIS-NIR) spectra Vesta s surface with howardites, eucrites, diogenites (HED). HEDs are commonly associated with Vesta s composition based on spectral similarities. Because of such association, much effort is being made to merge the information from HEDs as well as Vestoids - with that from Vesta to characterize the lithologic diversity of the surface of this asteroid and to infer clues regarding its thermal history. However, while the HEDs are a class of meteorites well studied in the laboratory, the only spectral data available for Vesta until now were telescopic observations which are limited in terms of observation conditions, spatial resolution and Signal to Noise Ratio. The Dawn spacecraft, orbiting around Vesta since July 2011, is performing detailed observations of this body and thus improving our knowledge of its properties. Dawn s scientific payload includes an imaging spectrometer, VIR-MS, sensitive to the VIS-NIR spectral range. VIR-MS began acquiring spectra during the approach phase started in May 2011 and will continue its observations through July 2012 when the spacecraft will depart Vesta to travel to Ceres. The VIR-MS spatial resolution depends upon the mission phase (approach, survey, high altitude, low altitude). However, spectra acquired by VIR-MS have already exceeded the spatial resolution of ground-based telescopic observations, with resolution in the approach phase ranging from 2.5 up to 0.8 km/pixel. Moreover, the observations are uniformly distributed in latitude and longitude allowing us to have a global view of Vesta s crust spectral properties. Using the information provided by VIR spectra, we studied the distribution of the spectral heterogeneities on the surface and we used our findings to perform a comparison with HEDs spectra in the VIS-NIR spectral range searching for analogies and/or incompatibilities. In our analysis, we focused on a method to compare the results obtained at microscopic scale on HEDs samples and the one obtained at macroscopic scale on the surface of Vesta. Finally, we discuss our results in the context of vestan thermal history. The intent of this study is to improve our understanding of the connection between Vesta and the HED samples, which is one of the primary Dawn scientific objectives. This work is supported by an Italian Space Agency (ASI) grant and by NASA through the Dawn project and a Dawn at Vesta Participating Scientist grant.

Ammannito, E.↗
NASA NTRS2012

Uniform Foam Crush Testing for Multi-Mission Earth Entry Vehicle Impact Attenuation

Multi-Mission Earth Entry Vehicles (MMEEVs) are blunt-body vehicles designed with the purpose of transporting payloads from outer space to the surface of the Earth. To achieve high-reliability and minimum weight, MMEEVs avoid use of limited-reliability systems, such as parachutes and retro-rockets, instead using built-in impact attenuators to absorb energy remaining at impact to meet landing loads requirements. The Multi-Mission Systems Analysis for Planetary Entry (M-SAPE) parametric design tool is used to facilitate the design of MMEEVs and develop the trade space. Testing was conducted to characterize the material properties of several candidate impact foam attenuators to enhance M-SAPE analysis. In the current effort, four different Rohacell foams are tested at three different, uniform, strain rates (approximately 0.17, approximately 100, approximately 13,600%/s). The primary data analysis method uses a global data smoothing technique in the frequency domain to remove noise and system natural frequencies. The results from the data indicate that the filter and smoothing technique are successful in identifying the foam crush event and removing aberrations. The effect of strain rate increases with increasing foam density. The 71-WF-HT foam may support Mars Sample Return requirements. Several recommendations to improve the drop tower test technique are identified.

Patterson, Byron W.↗
NASA NTRS2016

Single-Event Latchup Testing of the Micrel MIC4424 Dual Power MOSFET Driver

We conducted 47 exposures of four different MIC4424 devices and did not observe any SEL or high-current events. This included worst-case conditions with a LET of 81 MeV-sq cm/mg, applied voltage of 18.5 V, a case temperature greater than 120 C, and a final fluence of 1x10(exp 7)/sq cm. We also monitored both the outputs for the presence of SETs. While the period of the 1 MHz square wave was slightly altered in some cases, no pulses were added or deleted. 1. Purpose: The purpose of this testing is to characterize the BiCMOS/DMOS Micrel MIC4424 dual, non-inverting MOSFET driver for single-event latchup (SEL) susceptibility. These data will be used for flight lot evaluation purposes. 2. Devices Tested: The MIC4423/4424/4425 family are highly reliable BiCMOS/DMOS buffer/driver MOSFET drivers. They are higher output current versions of the MIC4426/4427/4428. They can survive up to 5V of noise spiking, of either polarity, on the ground pin. They can accept, without either damage or logic upset, up to half an amp of reverse current (either polarity) forced back into their outputs. Primarily intended for driving power MOSFETs, the MIC4423/4424/4425 drivers are suitable for driving other loads (capacitive, resistive, or inductive) which require low-impedance, high peak currents, and fast switching times. Heavily loaded clock lines, coaxial cables, or piezoelectric transducers are some examples. The only known limitation on loading is that total power dissipated in the driver must be kept within the maximum power dissipation limits of the package. Five (5) parts were provided for SEL testing. We prepared four parts for irradiation and reserved one piece as an un-irradiated control. More information about the devices can be found in Table 1. The parts were prepared for testing by removing the lid from the CDIP package to expose the target die. The parts were then soldered to small copper circuit adapter boards for easy handling. These parts are fabricated in a bulk BiCMOS/DMOS technology. Since we do not know the number of overlayers used in the fabrication processes, linear energy transfer calculations are determined based on the top-surface incident ion species and kinetic energy.

Power MOSFET↗
NASA NTRS2020

Mitigating Fading in Cislunar Communications: Application to the Human Landing System

NASA’s human exploration program is currently working towards landing astronauts on the surface of the Moon by 2024, close the lunar South Pole. To guarantee astronaut safety and maximize science data return, NASA is in the process of defining the communication architecture that will support all astronaut activities from launch to surface operations. Of particular interest to this paper are links from the lunar surface back to Earth without any intermediate relays. We show that the system geometry is such that antennas on the landing system will need to be pointed at low elevation angles, thus potentially causing multi-path fading effects not typically encountered in space communications. This paper is organized in three parts. First, we characterize the multi-path fading effects expected in links between the lunar South Pole and Earth and show that for moderate data rates (less than 1 Mbps) the links suffer from slow fading. We then show that for this operations regime the performance of forward error correction schemes is significantly worse for traditional Additive White Gaussian Noise channels. Finally, we investigate multi-copy mechanisms to mitigate the effects of fading, most notably repetition schemes and Automatic Repeat Request.

Sanchez Net, Marc↗
NASA NTRSDate not supplied

Early Results From NOAA-21 (JPSS-2) VIIRS on-Orbit Calibration

Launched on November 10, 2022, the NOAA-21 (N-21) VIIRS has successfully completed its initial post-launch testing (PLT) and intensive calibration and validation (ICV) activities. It is now operated in its nominal configuration and characterized using measurements from its on-board calibrators (OBC) and lunar observations. In this paper, we provide a brief description of N-21 VIIRS on-orbit operation and calibration activities and present results derived from its early mission performance assessments, including examples of its OBC performance, spectral band responses, as well as detector signal to noise characteristics. As shown in this paper, the overall performance of N-21 VIIRS is better than that of its predecessor currently operated on the S-NPP and comparable to the one onboard the N-20, with an exception of relatively large changes in its SWIR band responses.

NOAA-21↗
DOE OSTI2025

Characterization of Peripheral Neurophotonic Systems for High-Performance Human-Computer Interfaces (CRADA Final Report)

As part of the Cyclotron Road program, Morphosis Inc. sought to investigate a non-invasive neuromuscular sensing approach for use as an intuitive and secure human–computer interface. These highly miniaturized, wearable neural interfaces were completely non-invasive and maintained stable, high-bandwidth, long-term access to a user’s actions, intent, and identity, while offering an exceptionally high signal-to-noise ratio compared to contemporary neural recording technologies. The widespread adoption of neural interfaces had the potential to reshape how people interact with technology, with profound societal impacts. Millions worldwide suffered from movement and/or speech disabilities, and these tools had the potential to democratize access to technology to enhance autonomy and quality of life. More broadly, interfaces capable of accurately conveying intentions and safeguarding identities could serve as a cornerstone for privacy, trust, and personal authenticity in digital environments. The use of thought-driven control of digitally enabled devices and governance of digital identities had the potential to revolutionize relationships with technology, transforming how people learn, communicate, and interact with the world.

42 ENGINEERING↗
NASA NTRS1989

Data structure characterization of miltispectral data using principal component and principal factor analysis

Both principal component analysis (PCA) and principal factor analysis (PFA) were used to analyze an experimental multispectral data structure in terms of common and unique variance. Only the common variance of the multispectral data was associated with the principal factor, while higher-order principal components were associated with both common and unique variance. The unique variance was found to represent small spectral variations within each cover type as well as noise vectors, and was most abundant in the lower-order principal components. The lower-order principal components can be useful in research designed to discriminate minor physical variations within features, and to highlight localized change when using multitemporal-multispectral data. Conversely, PFA of the multispectral data provided an insight into a great potential for discriminating basic land-cover types by excluding the unique variance which was related to the noise and minor spectral variations.

Lee, Jae K.↗
NASA NTRS2024

Large Interferometer For Exoplanets (LIFE) XIII. The value of Combining Thermal Emission and Reflected Light for the Characterization of Earth Twins

Context. Following the recommendations to NASA (in the Astro2020 Decadal survey) and ESA (through the Voyage2050 process), the search for life on exoplanets will be a priority in the next decades. Two concepts for direct imaging space missions are being developed for this purpose: the Habitable Worlds Observatory (HWO) and the Large Interferometer for Exoplanets (LIFE). These two concepts operate in different spectral regimes: HWO is focused on reflected light spectra in the ultraviolet, visible, and near-infrared (UV/VIS/NIR), while LIFE will operate in the mid-infrared (MIR) to capture the thermal emission of temperate exoplanets. Aims. In this study, we aim to assess the potential of HWO and LIFE to characterize a cloud-free Earth twin orbiting a Sun-like star at a distance of 10 pc, both as separate missions and in synergy with each other. We aim to quantify the increase in information that can be gathered by joint atmospheric retrievals on a habitable planet. Methods. We performed Bayesian retrievals on simulated data obtained by an HWO-like mission and a LIFE-like one separately, then jointly. We considered the baseline spectral resolutions currently assumed for these concepts and used two increasingly complex noise simulations, obtained using state-of-the-art noise simulators. Results. An HWO-like concept would allow one to strongly constrain H 2 O, O 2 , and O 3 in the atmosphere of a cloud-free Earth twin, while the atmospheric temperature profile is not well constrained (with an average uncertainty ≈100 K). LIFE-like observations would strongly constrain CO 2 , H 2 O, and O 3 and provide stronger constraints on the thermal atmospheric structure and surface temperature (down to ≈10 K uncertainty). For all the investigated scenarios, both missions would provide an upper limit on CH 4 . A joint retrieval on HWO and LIFE data would accurately define the atmospheric thermal profile and planetary parameters. It would decisively constrain CO 2 , H 2 O, O 2 , and O 3 and find weak constraints on CO and CH 4 . The significance of the detection is in all cases greater than or equal to the single-instrument retrievals. Conclusions. Both missions provide specific information that is relevant for the characterization of a terrestrial habitable exoplanet, but the scientific yield can be maximized by considering synergistic studies of UV/VIS/NIR+MIR observations. The use of HWO and LIFE together will provide stronger constraints on biosignatures and life indicators, with the potential to be transformative for the search for life in the Universe.

E Alei↗
DOE OSTI2024

Solution-phase sample-averaged single-particle spectroscopy of quantum emitters with femtosecond resolution

Here, the development of many optical quantum technologies depends on the availability of solid-state single quantum emitters with near-perfect optical coherence. However, a standing issue that limits systematic improvement is the significant sample heterogeneity and lack of mechanistic understanding of microscopic energy flow at the single emitter level and ultrafast timescales. Here we develop solution-phase single-particle pump-probe spectroscopy with photon correlation detection that captures sample-averaged dynamics in single molecules and/or defect states with unprecedented clarity at femtosecond resolution. We apply this technique to single quantum emitters in two-dimensional hexagonal boron nitride, which suffers from significant heterogeneity and low quantum efficiency. From millisecond to nanosecond timescales, the translation diffusion, metastable-state-related bunching shoulders, rotational dynamics, and antibunching features are disentangled by their distinct photon-correlation timescales, which collectively quantify the normalized two-photon emission quantum yield. Leveraging its femtosecond resolution, spectral selectivity and ultralow noise (two orders of magnitude improvement over solid-state methods), we visualize electron-phonon coupling in the time domain at the single defect level, and discover the acceleration of polaronic formation driven by multi-electron excitation. Corroborated with results from a theoretical polaron model, we show how this translates to sample-averaged photon fidelity characterization of cascaded emission efficiency and optical decoherence time. Our work provides a framework for ultrafast spectroscopy in single emitters, molecules, or defects prone to photoluminescence intermittency and heterogeneity, opening new avenues of extreme-scale characterization and synthetic improvements for quantum information applications.

36 MATERIALS SCIENCE↗
DOE OSTI2023

Coexistent quantum channel characterization using quantum process tomography with spectrally resolved detection

The coexistence of classical and quantum signals over the same optical fiber is critical for quantum networks operating within the existing communications infrastructure. Here, we characterize the quantum channel that results from distributing approximate single-photon polarization-encoded qubits simultaneously with classical light of varying intensities through a 25 km fiber-optic channel. We use spectrally resolved quantum process tomography with a newly developed Bayesian reconstruction method to estimate the quantum channel from experimental data, both with and without classical noise. Furthermore, we show that the coexistent fiber-based quantum channel has high process fidelity with an ideal depolarizing channel if the noise is dominated by Raman scattering. These results aid future development of quantum repeater designs and quantum error-correcting codes which benefit from realistic channel error models.

Chapman, Joseph↗
DOE OSTI2024

Superconducting nanowire single-photon detector enhanced near-infrared II portable confocal microscopy for tissue imaging with indocyanine green

In this Letter a novel, to our knowledge, approach for near-infrared (NIR) fluorescence portable confocal microscopy is introduced, aiming to enhance fluorescence imaging of biological samples in the NIR-II window. By integrating a superconducting nanowire single-photon detector (SNSPD) into a confocal microscopy, we have significantly leveraged the detection efficiency of the NIR-II fluorescence signal from indocyanine green (ICG), an FDA-approved dye known for its NIR-II fluorescence capabilities. The SNSPD, characterized by its extremely low dark count rate and optimized NIR system detection efficiency, enables the excitation of ICG with 1 mW and the capture of low-light fluorescence signals from deep regions (up to 512 µm). Consequently, our technique was able to produce high-resolution images of bio samples with a superior signal-to-noise ratio, making a substantial advancement in the field of fluorescence microscopy and offering a promising opportunity for future clinical study.

Liu, Yifan (ORCID:0000000328877704)↗
NASA NTRS1977

NASA Quiet, Clean General Aviation Turbofan /QCGAT/ program status

Emissions pollution studies, noise studies, and engine performance studies and their place in QCGAT developmental program status are reported. The Lycoming TFE 731 turbofan engine, the GE T700-GE-700 high bypass ratio turbofan, and the AVCO-Lycoming LTS 101 turboshaft engine are prominent candidates in the tests for urban quiet turbofan service. Two phases in the program are characterized. Engine quieting, polluting emissions abatement, and fuel economies are particularly important for the anticipated rise in number of jet propulsion craft using smaller airports adjacent to communities accustomed to low noise/pollution backgrounds.

Bresnahan, D. L.↗
NASA NTRS1989

Type of silicate feature in oxygen rich stellar envelopes

In many astronomical studies, the emissivity function derived from the Trapezium emission feature has been used. A statistical study of a large sample of objects is described that deals with the applicability of this function (hereafter TR). For comparison, another emissivity function derived for lunar silicate (LS) sample 14321 was used which has a maximum at 10.2 microns instead of at 9.7 microns as for TR. The IRAS low resolution spectra sources classified as 7n was used which has a silicate absorption feature without any atomic line emission. Most of these sources are likely to be oxygen rich stellar envelopes or hotspots in molecular clouds. The central source as assumed to emit a Plankian spectrum characterized by a temperature (t) and an absorbing envelope with an emissivity dependence of type TR or LS. Values of t and tau, the absorption optical depth were obtained by minimizing chi(exp 2) between the observed and fitted spectra in the 7 to 13 micron range. Values of reduced chi(exp 2) were obtained by taking the noise listed in the LRS Catalog as standard deviation. The tau values obtained correspond to 9.7 microns for TR and 10.2 for LS.

Iyengar, K. V. K.↗