Targetless characterization of optical blurring from microphysical scattering
Explore the source record for details and available documents.
Pattyn, Christian Alexander [Sandia National Labor↗
SEARCH · Engineering Papers
Results for “optical characterization”
Search indexed NASA NTRS and DOE OSTI research on propulsion, heat transfer, battery materials and energy systems. Follow report and document links to the original sources.
Quote a phrase for an exact phrase match. Source license links do not imply unrestricted reuse.
Facility for interferometric testing of 1.25-m mirrors at liquid helium temperatures
A concept is presented for a national cryogenic optics test facility capable of optical characterization of 1.25 m diameter optics having focal lengths up to 6.2 m at temperatures from 300 K to near 4 K. The facility will be comprised of a large Dewar with a phase shift interferometer, a two stage vacuum system employing a turbomolecular pump, and an integral vibration isolation system. The entire facility will be housed in a concrete site with a massive floor to assist in reducing vibration during optical tests. By providing interchangeable sections, the overall height of the Dewar can be adjusted to provide for testing of shorter focal length optics. The background for the facility is discussed along with the facility location, and the requirements and the performance considerations which drive the Dewar design with respect to the vibration isolation system, vacuum system, and optical interferometry.
Salerno, Louis J.↗
Facility for interferometric testing of 1.25-m mirrors at liquid helium temperatures
A concept is presented for a national cryogenic optics test facility capable of optical characterization of 1.25 m diameter optics having focal lengths up to 6.2 m at temperatures from 300 K to near 4 K. The facility will be comprised of a large Dewar with a phase shift interferometer, a two-stage vacuum system employing a turbomolecular pump, and an integral vibration isolation system. The entire facility will be housed in a concrete site with a massive floor to assist in reducing vibration during optical tests. By providing interchangeable sections, the overall height of the Dewar can be adjusted to provide for testing of shorter focal length optics. The background for the facility is discussed along with the facility location, and the requirements and the performance considerations which drive the Dewar design with respect to the vibration isolation system, vacuum system, and optical interferometry.
Salerno, Louis J.↗
A Custom High-Throughput Optical Mapping Instrument for Accelerated Stress Testing of PV Module Materials
The performance and integrity of photovoltaic (PV) modules and materials may be assessed through optical characterizations. We have developed a custom optical mapping instrument (OMI) to improve measurement throughput time, facilitate automated measurements, allow for localized specimen examination, obtain spatial information relative to commercial benchtop spectrophotometer instruments, and provide automated data analysis. Both the key components and the methods used to improve the measurements are described. The measurement precision for the OMI is benchmarked for hemispherical transmittance relative to a previous round-robin study for commercial spectrophotometers. In addition to the unique instrument developed in this study, new insights have emerged from the examination of specimens from previous experiments, including: the depletion of the UV absorber is revealed for specimens beyond a certain size after artificial ultraviolet (UV) weathering; an optical degradation by internal haze formation is confirmed following Damp Heat (85 °C/85% relative humidity) testing; the better uniformity of the wear pattern for falling sand abrasion is used to select the DIN 52348 fixture over the ASTM D968 fixture; and the greater local (in the order of millimeters) heterogeneity of surface contamination in the soiling-prone location of Dubai relative to Kuwait. The results of the UV study have already been used to improve the standardized weathering of encapsulants. The example for Damp Heat testing is given to increase awareness of a degradation believed to be ubiquitously occurring in safety and design-type qualification testing of PV modules.
14 SOLAR ENERGY↗
Optical Performance of Reflectivity Control Devices for Solar Sail Applications
Reflectivity control devices (RCDs) based on polymer dispersed liquid crystals were fabricated for Solar Cruiser, a SmallSat NASA Pathfinder Mission consisting of a 1653 square meter solar sail that would establish an artificial orbit sunward of the L1 Lagrange point for heliophysics observations. Here we describe the optical characterization of these birefringent electro-optic devices including thin film measurements and analysis, hyperspectral bidirectional reflectance distribution function measurements, and radiometric analysis. These measurements demonstrate the promise of RCDs for roll control and momentum management of solar sails.
Radiometry↗
Optical Performance of Reflectivity Control Devices (RCDs) for Solar Sail Applications
Reflectivity control devices (RCDs) based on polymer dispersed liquid crystals were fabricated for Solar Cruiser, a SmallSat NASA Pathfinder Mission consisting of a 1653 square meter solar sail that would establish an artificial orbit sunward of the L1 Lagrange point for heliophysics observations. Here we describe the optical characterization of these birefringent electro-optic devices including thin film measurements and analysis, hyperspectral bidirectional reflectance distribution function measurements, and radiometric analysis. These measurements demonstrate the promise of RCDs for roll control and momentum management of solar sails.
Solar Sails↗
A Custom High-Throughput Optical Mapping Instrument (OMI) for Accelerated Stress Testing of PV Module Materials
The performance and integrity of photovoltaic (PV) modules and materials may be assessed through optical characterizations. We have developed a custom Optical Mapping Instrument (OMI) to improve measurement throughput time, facilitate automated measurements, and obtain spatial information relative to commercial benchtop spectrophotometer instruments. Both the key components and the methods used to improve the measurements are described. The measurement precision for the OMI is benchmarked for hemispherical transmittance relative to a previous round-robin study for commercial spectrophotometers. Example mapping measurements and their implications are given for specimens from other studies, including: (1) the depletion of the UV absorber is revealed for specimens beyond a certain size after standardized artificial ultraviolet (UV) weathering, (2) an optical degradation by internal haze formation is confirmed following Damp Heat (85°C/85% relative humidity) testing, (3) the better uniformity of the wear pattern for falling sand abrasion is used to select the DIN 52348 fixture over the ASTM D968 fixture, and (4) the local (millimeter-scale) heterogeneity of surface contamination in the soiling-prone location of Dubai relative to Kuwait. The results of the UV study have already been used to improve the standardized weathering of encapsulants. The example for Damp Heat testing is given to increase awareness of a degradation believed to be ubiquitously occurring in safety and design-type qualification testing of PV modules.
41 EE - Solar Energy Technologies Office (EE-4S)↗
A cryogenic white light absorption spectroscopy setup with in situ gamma irradiation and thermo-optical annealing for optical fiber radiation-induced attenuation characterization
Silica optical fiber sensors offer a fast, distributed measurement solution in various cryogenic and radiation environments, such as magnets for fusion power. Under these conditions, light-absorbing point defects limit lifetime via radiation-induced attenuation (RIA). To support RIA kinetics prediction, we present an in situ, broadband absorption spectroscopy setup combining gamma irradiation with liquid nitrogen cooling. The apparatus enables continuous monitoring of narrowband RIA levels and the use of secondary optical annealing light sources, alongside broadband spectrum measurements to characterize RIA defects through spectrum decomposition. Initial results confirm the inevitable photobleaching effect of the probe light source, which must be accounted for. In addition, we report RIA kinetics during cycles of gamma irradiation at 77 K and isochronal thermal annealing steps from liquid nitrogen to room temperature, showcasing the setup’s ability to replicate real fiber operation scenarios. These instruments form an ideal platform to further study the kinetics of RIA coupled with thermal and optical annealing.
Absorption spectroscopy↗
Spacecraft Glow and the Eisg/skirt Experiment
The objective of this experiment is to develop an understanding of the physical processes leading to spacecraft glow phenomena. The emphasis is to be on surface temperature and altitude effects. A complete understanding of the phenomena could be used to accomplish the following: (1) characterize optical instrument backgrounds; (2) provide guidelines for thermal insulations; (3) characterize material selection for flight optics and associated spacecraft; and (4) affect flight-operation altitude selection for relevant missions.
Swenson, Gary R.↗
Results of MODIS Band-to-Band Registration Characterization Using On-Orbit Lunar Observations
Since launch, lunar observations have been made regularly by both Terra and Aqua MODIS and used for a number of sensor calibration and characterization related applications, including radiometric stability monitoring, spatial characterization, optical leak and electronic cross-talk characterization, and calibration inter-comparison. MODIS has 36 spectral bands with a total of 490 individual detectors. They are located on four focal plane assemblies (FPA). This paper focuses on the use of MODIS lunar observations to characterize its band-to-band registration (BBR). In addition to BBR, the approach developed by the MODIS Characterization Support Team (MCST) can be used to characterize MODIS detector-to-detector registration (DDR). Long-term BBR results developed from this approach are presented and compared with that derived from a unique on-board calibrator (OBC). Results show that on-orbit changes of BBR have been very small for both Terra and Aqua MODIS and this approach can be applied to other remote sensing instruments.
Xiong, Xiaoxiong↗
Analysis of Spacecraft Materials Discrimination Using Color Indices for Remote Sensing for Space Situational Awareness
The increasing number of space missions have resulted in an augmented density of artificial objects positioned in orbital domains near Earth. Knowing the material composition of the resident space object can be of value in object identification and risk assessment using remote sensing techniques. To perform this task, it is increasingly imperative to optically characterize spacecraft materials to identify unique material-specific spectroscopic markers. In this work, a variety of materials frequently utilized by the aerospace industry in spacecraft design and construction were analyzed using reflectance spectroscopy. The collected data provide a spectral characterization baseline for modern-day and historical spacecraft materials. The color index was computed for standard astronomical and suggested theoretical filter passbands and compared to each other in their capability to discriminate materials belonging to different classes. The color index was calculated from reflectance spectra of common spacecraft materials in their pristine, as-received conditions that fell under different family groupings. Different color-index combinations were studied using color-color diagrams. Visual and quantitative analysis of the color-color diagrams were used to evaluate the possibility of discriminating materials from one another by means of optical measurements. Results of the analysis show that polyimide and photovoltaic materials are most easy to discriminate from all other materials via color indices using different filter passbands evaluated in this study.
spectral reflectance↗
MeV ion-beam analysis of optical data storage films
Our objectives are threefold: (1) to accurately characterize optical data storage films by MeV ion-beam analysis (IBA) for ODSC collaborators; (2) to develop new and/or improved analysis techniques; and (3) to expand the capabilities of the IBA facility itself. Using H-1(+), He-4(+), and N-15(++) ion beams in the 1.5 MeV to 10 MeV energy range from a 5.5 MV Van de Graaff accelerator, film thickness (in atoms/sq cm), stoichiometry, impurity concentration profiles, and crystalline structure were determined by Rutherford backscattering (RBS), high-energy backscattering, channeling, nuclear reaction analysis (NRA) and proton induced X-ray emission (PIXE). Most of these techniques are discussed in detail in the ODSC Annual Report (February 17, 1987), p. 74. The PIXE technique is briefly discussed in the ODSC Annual Report (March 15, 1991), p. 23.
Leavitt, J. A.↗
Quantitative Infrared-to-Terahertz Nanospectroscopy of Semiconductors
Semiconductor technology now employs few-nanometer features, necessitating tools probing electronic properties on the same length scale. While the concentration of free charge carriers is routinely measured, the scattering rate remains challenging to access at the nanoscale. Here, we present ultrabroadband (5–50 THz) synchrotron infrared nanospectroscopy as a quantitative metrology tool for semiconductors. This technique can determine both the charge carrier concentration and scattering rate with percent-level accuracy, and it is inherently capable of ∼10 nm spatial resolution. We study silicon with different doping levels and confirm the method’s accuracy by statistical analysis and comparison with established far-field infrared spectroscopy. Near-field measurements systematically reveal charge-carrier concentrations ∼30% lower than far-field values, consistent with increased surface sensitivity and surface depletion. Our work establishes synchrotron infrared nanospectroscopy as a precise tool for quantitative nanoscale semiconductor characterization and paves the way toward all-optical characterization of surface depletion effects.
36 MATERIALS SCIENCE↗
Spectroscopic Behavior of Composite, Black Thermal Paint, Solar Cell, and Multi-layered Insulation Materials in a GEO Simulated Environment
Materials currently populating Earth orbital regimes can be distinguished by comparing remote observational data to that of optical material measurements obtained in the laboratory. Experimentation for this research primarily involved the acquisition of spectroscopic measurements on materials of interest to the telescopic observational community for enhanced space situational awareness. Common spacecraft materials worthy of preeminent analysis for this investigation include a carbon-carbon (c-c) matrix composite, various black thermal paints, a GPS solar cell and three different cover glass components. These materials were subjected to a simulated geosynchronous Earth orbit (GEO) space environment with the intent of observing material optical property behavior over quantitative exposure time. The aforementioned materials have been measured in their pristine and GEO simulated exposed conditions. A reflectance spectrometer and a bi-directional reflectance distribution function (BRDF) optical system have been operated to perform material characterization, optical property analysis, and to further compare such data to telescopic observational data acquired on equal materials.
Reyes, Jacqueline A.↗
Bio-Optical Properties of the Arabian Sea as Determined by In Situ and Sea WiFS Data
The overall objective of this work was to characterize optical and fluorescence properties in the euphotic zone during two British Ocean Flux Study (BOFS) Arabian Sea cruises. This was later expanded in 1995 to include three U.S. JGOFS Arabian Sea Cruises. The region was to be divided into one or more "bio-optical provinces," within each of which a single set of regression models was to be developed to relate the vertical distribution of irradiance attenuation and normalized fluorescence (SF and NF) to remote sensing reflectance and diffuse attenuation coefficient. The working hypothesis was that over relatively large spatial and temporal scales, the vertical profiles of bio-optical properties were predictable. The specific technical objectives were: (1) To characterize the vertical distribution of the inherent and apparent optical properties by measuring downwelling and upwelling irradiances, upwelling radiances, scalar irradiance of PAR, and beam transmissions at each station - from these data, spectral diffuse attenuation coefficients, irradiance reflectances, remote sensing reflectances, surface-leaving radiances and beam attenuation coefficients were determined; (2) To characterize the spectral absorption of total particulate, detrital, and dissolved organic material at each station from discrete water samples; (3) To describe the vertical distribution of photoadaptive properties in the water column by measuring profiles of stimulated (SF) and natural (NF) fluorescence and examining relationships between SF and NF as a function of diffuse optical depth, pigment biomass and primary productivity; and (4) To establish locally derived, in-water algorithms relating remote sensing reflectance spectra to diffuse attenuation coefficients, phytoplankton pigment concentrations and primary productivity, through intercomparisons with in situ measurements, for application to SeaWiFS data.
Trees, Charles C.↗
Optical Design and Characterization of 40-GHz Detector and Module for the BICEP Array
Families of cosmic inflation models predict a primordial gravitational-wave background that imprints B-mode polarization pattern in the cosmic microwave background (CMB). High-sensitivity instruments with wide frequency coverage and well-controlled systematic errors are needed to constrain the faint B-mode amplitude. We have developed antenna-coupled transition edge sensor arrays for high-sensitivity polarized CMB observations over a wide range of millimeter-wave bands. BICEP array, the latest phase of the BICEP/Keck experiment series, is a multi-receiver experiment designed to search for inflationary B-mode polarization to a precision σ(r) between 0.002 and 0.004 after 3 full years of observations, depending on foreground complexity and the degree of lensing removal. We describe the electromagnetic design and measured performance of BICEP array’s low-frequency 40-GHz detector, their packaging in focal plane modules, and optical characterization including efficiency and beam matching between polarization pairs. We summarize the design and simulated optical performance, including an approach to improve the optical efficiency due to mismatch losses. Here, we report the measured beam maps for a new broadband corrugation design to minimize beam differential ellipticity between polarization pairs caused by interactions with the module housing frame, which helps minimize polarized beam mismatch that converts CMB temperature to polarization (T→P) anisotropy in CMB maps.
47 OTHER INSTRUMENTATION↗
Characterization of mechanical deformation in aluminum by optical second harmonic generation
Second harmonic generation (SHG), a laser-based surface technique, was used to characterize near-surface defect evolution associated with mechanical deformation in 2024-T3 aluminum due to tensile loads. Electron backscatter diffraction (EBSD) measurements were also performed to determine the geometrically necessary dislocation density before and after tensile deformation. Comparison of the EBSD and SHG results found that dislocation density and SHG signal are inversely proportional; tensile deformation in the plastic regime led to an increase in dislocation density and a decrease in SHG response. A similar trend was seen in the SHG results on as-received (unpolished) Al samples; SHG response decreases with extent of plastic deformation. Furthermore, this study suggests that SHG has potential as a nondestructive evaluation technique.
36 MATERIALS SCIENCE↗
Fiber optic system for direct detection of CO 2 leakage in carbon storage wells (Abbreviated Final Report)
The feasibility study focused on the development of new fiber for distributed chemical sensing that will allow direct detection of CO2 leakages in the environment. This is particularly important for monitoring well integrity for carbon capture and storage (CSS), which can provide early warning for an incoming well failure and potential CO2 leaking through it. We proposed Raman or IR interrogation within gas-filled Holey Fibers (HoFs) interleaved with Fiber Bragg Grating (FBG) sections, so that the location and concentration of the gases would be provided simultaneously. The methodology would overcome current roadblocks to using fiber optics for CO2 (and other gases) detection in wells with direct in-situ measurements of concentration along with other important parameters such as temperature and pressure. We were able to assess commercially available IR/Raman hollow core fiber and demonstrated detection of CO2 through them in our controlled environment setups at various pressure conditions. We have also established the ability of drilling precisely with fs-lases side holes to enable penetration of CO2 into the hollow core fiber and reduce diffusion rates. Open joint collars were also explored with double functionality: to obtain splice to solid core fiber critical for field deployment and create gas ingress locations. Both diffusion-only and pressurized fiber system have been constructed following COMSOL based semi-hybrid optical /fluidodynamics models. FBGs have been identified and procured and characterized. Along the work we leveraged internal modeling/design, photonics/laser characterization, optical fiber fabrication, and AM lab capabilities to design, develop and test in-house components or assemblies. Our results indicate the potential of HoF for CO2 downhole direct detection.
25 ENERGY STORAGE↗